CN107201443A - A kind of automatic leaching device - Google Patents

A kind of automatic leaching device Download PDF

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Publication number
CN107201443A
CN107201443A CN201710487819.9A CN201710487819A CN107201443A CN 107201443 A CN107201443 A CN 107201443A CN 201710487819 A CN201710487819 A CN 201710487819A CN 107201443 A CN107201443 A CN 107201443A
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CN
China
Prior art keywords
leaching
plate
guide shell
leaching tanks
soda acid
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Granted
Application number
CN201710487819.9A
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Chinese (zh)
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CN107201443B (en
Inventor
唐立婧
苏建财
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Xiamen Huanzi Mining Technology Co.,Ltd.
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Xiamen Rim Mining Polytron Technologies Inc
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Priority to CN201710487819.9A priority Critical patent/CN107201443B/en
Publication of CN107201443A publication Critical patent/CN107201443A/en
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    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/04Extraction of metal compounds from ores or concentrates by wet processes by leaching
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22BPRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00Extraction of metal compounds from ores or concentrates by wet processes
    • C22B3/02Apparatus therefor
    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02PCLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P10/00Technologies related to metal processing
    • Y02P10/20Recycling

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  • Engineering & Computer Science (AREA)
  • Chemical & Material Sciences (AREA)
  • Manufacturing & Machinery (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

The present invention discloses a kind of automatic leaching device, guide shell and distribution drum are arranged in leaching tanks, the lower end of distribution drum is arranged on the bottom of leaching tanks, the upper end of distribution drum is connected by the lower end of conically shaped and guide shell, the upper end material guide port of guide shell and the notch of leaching tanks are kept at a distance, and the lower end of guide shell opens up feeding mouth;The agitating shaft of mixer is stretched into distribution drum through guide shell and conically shaped, and the stirring that agitating shaft lower end is installed is located in distribution drum with impeller;Soda acid entrance is opened up above the side wall of leaching tanks and ore pulp enters confession connection soda acid feeding pipe and ore pulp feeding pipe, corrosion-resistant mozzle is located in leaching tanks, the upper end connection soda acid entrance of mozzle and ore pulp entrance and lower end are connected to below the feeding mouth of guide shell, the side wall of leaching tanks and open up gape for connection ore discharge pipe;Control system control soda acid feeding pipe, ore pulp feeding pipe and valve and the head of mixer on ore discharge pipe.The present invention can reduce cost of labor, and safe operation improves leaching efficiency.

Description

A kind of automatic leaching device
Technical field
It is especially relevant with a kind of structure of automatic leaching device the present invention relates to the technical field of hydrometallurgy, ore dressing etc..
Background technology
In the prior art, had by the way of immersion, mixing, dissolving to remove in ore.But, acid used Alkali all have stronger corrosivity, to equipment construct requirement it is higher, there is presently no exclusively with automatic control device, It can only be leached by manually controlling to realize, cost of labor is high, and operation is dangerous, and leaching efficiency is low.
The content of the invention
It is an object of the invention to provide a kind of automatic leaching device, cost of labor is reduced, safer, raising leaching is operated Efficiency.
To achieve these goals, technical scheme is as follows:
A kind of automatic leaching device, including leaching tanks, guide shell, distribution drum, mixer and control system;Corrosion resistant guide shell It is arranged on distribution drum in corrosion resistant leaching tanks, the barrel dliameter of guide shell is less than the barrel dliameter of distribution drum, and distribution drum is by some distribution Plate is surrounded, and gap is kept between adjacent distribution plate, and the lower end of distribution drum is arranged on the bottom of leaching tanks, and the upper end of distribution drum leads to The lower end for crossing corrosion resistant conically shaped and guide shell is connected, and the upper end material guide port of guide shell and the notch of leaching tanks are kept at a distance, The lower end of guide shell opens up feeding mouth;The head of mixer is arranged on the top of leaching tanks, and the corrosion resistant agitating shaft of mixer is worn Cross guide shell and conically shaped is stretched into distribution drum, the stirring that agitating shaft lower end is installed is located in distribution drum with corrosion resistant impeller; Soda acid entrance is opened up above the side wall of leaching tanks and ore pulp enters confession connection soda acid feeding pipe and ore pulp feeding pipe, corrosion-resistant water conservancy diversion Pipe is located in leaching tanks, and the upper end of mozzle connection soda acid entrance and ore pulp entrance and lower end are connected to the feeding mouth of guide shell, Gape is opened up below the side wall of leaching tanks for connection ore discharge pipe;Control system outside leaching tanks and soda acid feeding pipe, Valve on ore pulp feeding pipe and ore discharge pipe connects and controls on and off, and the head of control system and mixer connects and controls work Make.
Flowmeter, control system and the stream on soda acid feeding pipe and ore discharge pipe are installed on the soda acid feeding pipe and ore discharge pipe Gauge is connected, and the information transmitted according to flowmeter controls the valve on and off on soda acid feeding pipe and ore discharge pipe.
The ore pulp entrance is located at the top of soda acid entrance.
Liquid level gauge is installed, liquid level gauge outer cladding resistant material, control system is connected with liquid level gauge in the leaching tanks, and The valve on and off on information control soda acid feeding pipe, ore pulp feeding pipe and ore discharge pipe transmitted according to liquid level gauge.
Install and cover resistance on the circular ultrasonic echography plate of bottom formula, bottom formula circle ultrasonic echography plate in the bottom of the leaching tanks Corrosion material, the lower end of distribution drum is arranged on the circular ultrasonic echography plate of bottom formula, the vibration of bottom formula circle ultrasonic echography plate Movement is connected with control system and controls time of vibration and vibration frequency.
Installation side formula plate shape is ultrasonic in the way of it can slide up and down lifting in the side wall formation chute of the leaching tanks, chute Ripple ultrasound plate, side formula plate shape ultrasonic echography plate outer cladding resistant material, side formula plate shape ultrasonic echography plate is arranged on lifting The lower end of rope, the upper end of halliard is connected transmission, small machine and side formula plate shape ultrasound with the small machine at the top of leaching tanks The vibration movement of ripple ultrasound plate is connected with control system, and when controlling the vibration of side formula plate shape ultrasonic echography plate by control system Between and vibration frequency, by control system control small machine work, by halliard drive side formula plate shape ultrasonic echography plate stretch into Under the liquid level of leaching tanks.
The leaching tanks are made of stainless steel material.
The guide shell, distribution drum, conically shaped and mozzle are made of polytetrafluoroethylmaterial material.
After such scheme, the present invention is imported leaching agent soda acid and ore pulp in guide shell by mozzle, soda acid and ore deposit Slurry is contacted in mozzle to be pre-mixed, then is produced radial flow by the impeller rotation of mixer and axially flowed, and is formed in distribution drum Negative pressure, in the presence of guide shell, changes radial flow so that ore pulp is projected from the feeding mouth of guide shell, and conically shaped, which has, to be oriented to Effect, makes ore pulp discharge more smooth, and under the lower use of distribution plate so that ore pulp is discharged rapidly from the gap of distribution plate, ore pulp leads to Cross after distribution plate and rise, the upper end material guide port to guide shell enters guide shell, form a circulation, be conducive to ore pulp and soda acid to fill Divide stirring contact, improve leaching effect.
The present invention can be fully utilized control system and be controlled, and greatly reduce cost of labor, operate safer.
Below in conjunction with the drawings and specific embodiments, the invention will be further described.
Brief description of the drawings
Fig. 1 is the structural representation of the present invention;
Fig. 2 is guide shell and the schematic perspective view of distribution drum.
Label declaration
Leaching tanks 1, notch 11, soda acid entrance 12, soda acid feeding pipe 121, valve 122, flowmeter 123, ore pulp entrance 13, ore pulp Feeding pipe 131, valve 132, gape 14, ore discharge pipe 141, valve 142, flowmeter 143, chute 15;
Guide shell 2, material guide port 21, feeding mouth 22;
Distribution drum 3, gap 31, distribution plate 32;
The head 4 of mixer, agitating shaft 41, impeller 42;
Conically shaped 5;
Mozzle 6;
Liquid level gauge 7;
The circular ultrasonic echography plate 8 of bottom formula;
Side formula plate shape ultrasonic echography plate 9, halliard 91, small machine 92.
Embodiment
As depicted in figs. 1 and 2, a kind of automatic leaching device that the present invention is disclosed, including leaching tanks 1, guide shell 2, distribution Cylinder 3, mixer and control system(Ordinary elements, as long as the control purpose of the present invention can be realized, not shown in figure).
Guide shell 2 and distribution drum 3 are arranged in leaching tanks 1, and the barrel dliameter of guide shell 2 is less than the barrel dliameter of distribution drum 3, distribution drum 3 are surrounded by some distribution plates 32, and gap 31 is kept between adjacent distribution plate 32, and the lower end of distribution drum 3 is arranged on leaching tanks 1 Bottom, the upper end of distribution drum 3 is connected by conically shaped 5 with the lower end of guide shell 2, and the upper end of guide shell 2 is material guide port 21, guide The notch 11 of mouth 21 and leaching tanks 1 keeps sufficient distance, and the lower end of guide shell 2 opens up feeding mouth 22.
The head 4 of mixer is arranged on the top of leaching tanks 1, and the agitating shaft 41 of mixer passes through guide shell 2 and conically shaped 5 Stretch into distribution drum 3, the stirring that the lower end of agitating shaft 41 is installed is located in distribution drum 3 with impeller 42.
The soda acid feeding pipe 121 that soda acid entrance 12 and ore pulp entrance 13 supply outside respectively is opened up above the side wall of leaching tanks 1 Connected with ore pulp feeding pipe 131, mozzle 6 is located in leaching tanks 1, the upper end connection soda acid entrance 12 and ore pulp of mozzle 6 enter Mouthfuls 13 inner side and lower end are connected to below the feeding mouth 22 of guide shell 2, the side wall of leaching tanks 1 and open up gape 14 for outside Ore discharge pipe 141 is connected.In order to be conducive to soda acid and ore pulp to be pre-mixed, to reduce the concentration of soda acid, ore pulp entrance 13 is designed to Positioned at the top of soda acid entrance 12, make soda acid upon entering mozzle 6 at once by slurry dilution, reduce corrosion.
Control system is arranged on outside leaching tanks 1, control system and the valve 122 on soda acid feeding pipe 121, ore pulp feeding pipe The valve 142 on valve 132 and ore discharge pipe 141 on 131 connects and controls on and off, the head 4 of control system and mixer Connect and control work.
Operation and leaching effect are leached in order to better control over, the present invention pacifies on soda acid feeding pipe 121 and ore discharge pipe 141 Flowmeter 123 and 143 is filled, control system is connected with flowmeter 123 and 143, and the information transmitted according to flowmeter 123 and 143 Valve 122 and 142 on control soda acid feeding pipe 121 and ore discharge pipe 141 is opened or closed.Liquid level gauge 7, liquid are also installed in leaching tanks 1 Position 7 outer cladding resistant materials of meter, control system is connected with liquid level gauge 7, and the information control soda acid transmitted according to liquid level gauge 7 enters The on and off of valve 122,132,142 on expects pipe 121, ore pulp feeding pipe 131 and ore discharge pipe 141.
In order to promote leaching effect, leaching efficiency is improved, the present invention installs formula circular ultrasonic wave in bottom in the bottom of leaching tanks 1 Resistant material is covered on ultrasonic plate 8, bottom formula circle ultrasonic echography plate 8, the lower end of distribution drum 3 is arranged on the circular ultrasound of bottom formula On ripple ultrasound plate 8, the vibration movement of bottom formula circle ultrasonic echography plate 8 is connected with control system and controls time of vibration and vibration Frequency.In addition, in the side wall formation chute 15 of leaching tanks 1, chute 15 in the way of it can slide up and down lifting installation side formula plate shape Ultrasonic echography plate 9, the outer cladding resistant material of side formula plate shape ultrasonic echography plate 9, side formula plate shape ultrasonic echography plate 9 is installed In the lower end of halliard 91, the upper end of halliard 91 is connected transmission, small machine 92 with the small machine 92 installed in the top of leaching tanks 1 It is connected with the vibration movement of side formula plate shape ultrasonic echography plate 9 with control system, and formula plate shape ultrasound in side is controlled by control system The time of vibration and vibration frequency of ripple ultrasound plate 9, are worked by control system control small machine 92, side formula are driven by halliard 91 Plate shape ultrasonic echography plate 9 stretches under the liquid levels of leaching tanks 1 or is lifted off liquid level.
All components contacted with soda acid of the present invention are all made of resistant material.Such as, leaching tanks 1 are using corrosion-resistant Material is made, and can be specifically stainless steel material, or inexpensive carbon steel material.Guide shell 2, distribution drum 3, conically shaped 5, water conservancy diversion Pipe 6 and the circular ultrasonic echography plate 8 of liquid level gauge 7, bottom formula, the surface of side formula plate shape ultrasonic echography plate 9 use corrosion-resistant material Material is made, and can be specifically polytetrafluoroethylmaterial material.The agitating shaft 41 and impeller 42 of mixer are also made of resistant material, It can be specifically stainless steel material.
During present invention work, control system control valve 142 is closed, and control valve 122 and 132 is opened, while by flowing Gauge 123 controls the addition of soda acid, and control valve 122 is closed when reaching setting value, is set when liquid level gauge 7 detects liquid level and reached During definite value, control system control valve 132 is closed, then by control system control mixer work.Leaching agent soda acid and ore pulp by Mozzle 6 is imported in guide shell 2, and soda acid and ore pulp are contacted in mozzle 2 and be pre-mixed, then are rotated by the impeller 42 of mixer Produce radial flow and axially flow, negative pressure is formed in distribution drum 3, in the presence of guide shell 2, change radial flow so that ore pulp Projected from the feeding mouth 21 of guide shell 2, speed increase, conically shaped 5 has guide effect, make ore pulp discharge more smooth, in distribution Under the lower use of plate 3 so that ore pulp is discharged rapidly from the gap 31 of distribution plate 3, because speed is larger, is washed away bottom particles, is prevented Deep gouge;Ore pulp enters guide shell 2 by rising after distribution plate 3 to upper end material guide port 21, forms a circulation, is conducive to ore pulp Contact is sufficiently and uniformly stirred with soda acid, not the problems such as not resulting in " ore pulp short circuit ", leaching effect is higher.In leaching process, control System processed also controls the vibration movement work of the circular ultrasonic echography plate 8 of bottom formula and side formula plate shape ultrasonic echography plate 9, generation Ultrasonic wave can make to produce sound wave cavitation between soda acid and ore pulp, cause the formation, growth and burst pressure of bubble in solution Contracting, so that ore is scattered, the contact area of increase ore and soda acid leaching agent improves object and is transferred to liquid phase from solid phase Mass transfer rate, shortens extraction time, and Strengthen education improves leaching efficiency.The circular ultrasonic echography plate 8 of bottom formula and side wall installation side Formula plate shape ultrasonic echography plate 9 can set automatic spacing to work, it is to avoid work long hours, desired effects, side can be reached again Formula plate shape ultrasonic echography plate 9 can operationally be driven by halliard 91 and is put under liquid level, it is not necessary to when, then by halliard 91 are lifted on liquid level, prevent from contacting and being corroded with soda acid for a long time.
The present invention can realize Automated condtrol, reduce in cost of labor, the extraction process for being widely used in various ores, Lift leaching efficiency.
One embodiment of the present of invention is the foregoing is only, the limitation not designed this case, all designs according to this case are closed The equivalent variations that key is done, each fall within the protection domain of this case.

Claims (8)

1. a kind of automatic leaching device, it is characterised in that:Including leaching tanks, guide shell, distribution drum, mixer and control system; Corrosion resistant guide shell and distribution drum are arranged in corrosion resistant leaching tanks, and the barrel dliameter of guide shell is less than the barrel dliameter of distribution drum, point Surrounded with cylinder by some distribution plates, gap kept between adjacent distribution plate, the lower end of distribution drum is arranged on the bottom of leaching tanks, The upper end of distribution drum is connected by the lower end of corrosion resistant conically shaped and guide shell, the upper end material guide port of guide shell and leaching tanks Notch is kept at a distance, and the lower end of guide shell opens up feeding mouth;The head of mixer is arranged on the top of leaching tanks, mixer corrosion resistant The agitating shaft of erosion is stretched into distribution drum through guide shell and conically shaped, the stirring that agitating shaft lower end is installed corrosion resistant impeller position In distribution drum;Soda acid entrance is opened up above the side wall of leaching tanks and ore pulp enters confession connection soda acid feeding pipe and ore pulp pan feeding Pipe, corrosion-resistant mozzle is located in leaching tanks, and the upper end of mozzle connects soda acid entrance and ore pulp entrance and lower end is connected to and led Gape is opened up below the feeding mouth of flow cartridge, the side wall of leaching tanks for connection ore discharge pipe;Control system outside leaching tanks It is connected with the valve on soda acid feeding pipe, ore pulp feeding pipe and ore discharge pipe and controls on and off, the machine of control system and mixer Head connects and controls work.
2. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The bottom of the leaching tanks is installed by bottom formula circle Resistant material is covered on shape ultrasonic echography plate, bottom formula circle ultrasonic echography plate, the lower end of distribution drum is justified installed in bottom formula On shape ultrasonic echography plate, the vibration movement of bottom formula circle ultrasonic echography plate be connected with control system and control time of vibration and Vibration frequency.
3. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The side wall formation chute of the leaching tanks, In chute in the way of it can slide up and down lifting installation side formula plate shape ultrasonic echography plate, side formula plate shape ultrasonic echography plate outsourcing Resistant material is covered, side formula plate shape ultrasonic echography plate is arranged on the lower end of halliard, and the upper end of halliard is leached with being arranged on The vibration movement of small machine connection transmission at the top of groove, small machine and side formula plate shape ultrasonic echography plate is connected with control system, And the time of vibration and vibration frequency of side formula plate shape ultrasonic echography plate are controlled by control system, small machine is controlled by control system Work, drives side formula plate shape ultrasonic echography plate to stretch under the liquid level of leaching tanks by halliard.
4. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The soda acid feeding pipe and ore discharge Guan Shangan Flowmeter is filled, control system is connected with the flowmeter on soda acid feeding pipe and ore discharge pipe, and the information control transmitted according to flowmeter Valve on and off on relieving haperacidity alkali feeding pipe and ore discharge pipe.
5. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The ore pulp entrance is located at soda acid entrance Top.
6. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:Liquid level gauge, liquid are installed in the leaching tanks Position meter outer cladding resistant material, control system is connected with liquid level gauge, and the information transmitted according to liquid level gauge controls soda acid pan feeding Valve on and off on pipe, ore pulp feeding pipe and ore discharge pipe.
7. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The leaching tanks use stainless steel material system Into.
8. a kind of automatic leaching device as claimed in claim 1, it is characterised in that:The guide shell, distribution drum, conically shaped and Mozzle is made of polytetrafluoroethylmaterial material.
CN201710487819.9A 2017-06-23 2017-06-23 A kind of automatic leaching device Active CN107201443B (en)

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Application Number Priority Date Filing Date Title
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CN107201443B CN107201443B (en) 2019-05-10

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111389597A (en) * 2020-01-22 2020-07-10 中国矿业大学 Polar mixed reagent for low-rank coal flotation and flotation process
CN111748705A (en) * 2020-06-30 2020-10-09 长沙矿冶研究院有限责任公司 Method for extracting rare earth elements from deep sea sediments
CN114934193A (en) * 2022-05-24 2022-08-23 浙江伽能环境工程有限责任公司 Method for enhancing normal-pressure acid leaching efficiency of nickel anode mud desulfurization slag
US11920246B2 (en) 2021-10-18 2024-03-05 The Regents Of The University Of California Seawater electrolysis enables Mg(OH)2 production and CO2 mineralization

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111389597A (en) * 2020-01-22 2020-07-10 中国矿业大学 Polar mixed reagent for low-rank coal flotation and flotation process
CN111748705A (en) * 2020-06-30 2020-10-09 长沙矿冶研究院有限责任公司 Method for extracting rare earth elements from deep sea sediments
CN111748705B (en) * 2020-06-30 2024-07-02 长沙矿冶研究院有限责任公司 Method for extracting rare earth element from deep sea sediment
US11920246B2 (en) 2021-10-18 2024-03-05 The Regents Of The University Of California Seawater electrolysis enables Mg(OH)2 production and CO2 mineralization
CN114934193A (en) * 2022-05-24 2022-08-23 浙江伽能环境工程有限责任公司 Method for enhancing normal-pressure acid leaching efficiency of nickel anode mud desulfurization slag

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Inventor after: Tang Lijing

Inventor after: Su Jiancai

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Address after: 361000 2505, No. 96-1, Lujiang Road, Siming District, Xiamen, Fujian

Patentee after: Xiamen Huanzi Mining Technology Co.,Ltd.

Address before: 361000 2505, No. 96-1, Lujiang Road, Siming District, Xiamen, Fujian

Patentee before: XIAMEN HUANZI MINING TECHNOLOGY Inc.

PE01 Entry into force of the registration of the contract for pledge of patent right
PE01 Entry into force of the registration of the contract for pledge of patent right

Denomination of invention: An automatic leaching device

Effective date of registration: 20231221

Granted publication date: 20190510

Pledgee: China Co. truction Bank Corp Xiamen branch

Pledgor: Xiamen Huanzi Mining Technology Co.,Ltd.

Registration number: Y2023980072673