CN107201161A - A kind of anti-skid intensifier for smooth brick masonry surface and preparation method thereof - Google Patents
A kind of anti-skid intensifier for smooth brick masonry surface and preparation method thereof Download PDFInfo
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- CN107201161A CN107201161A CN201710504705.0A CN201710504705A CN107201161A CN 107201161 A CN107201161 A CN 107201161A CN 201710504705 A CN201710504705 A CN 201710504705A CN 107201161 A CN107201161 A CN 107201161A
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- intensifier
- skid
- brick masonry
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
- C09D175/08—Polyurethanes from polyethers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K3/00—Materials not provided for elsewhere
- C09K3/14—Anti-slip materials; Abrasives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/18—Oxygen-containing compounds, e.g. metal carbonyls
- C08K3/20—Oxides; Hydroxides
- C08K3/22—Oxides; Hydroxides of metals
- C08K2003/2237—Oxides; Hydroxides of metals of titanium
- C08K2003/2241—Titanium dioxide
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/30—Sulfur-, selenium- or tellurium-containing compounds
- C08K2003/3045—Sulfates
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K7/00—Use of ingredients characterised by shape
- C08K7/22—Expanded, porous or hollow particles
- C08K7/24—Expanded, porous or hollow particles inorganic
- C08K7/26—Silicon- containing compounds
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Curing Cements, Concrete, And Artificial Stone (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
The invention discloses a kind of anti-skid intensifier for smooth brick masonry surface, include the raw material of following percentage by weight：Inorganic acid 1~12%, Glycolic acid 0.5~10%, diisocyanate 3~8%, trimethylolpropane 1~5%, modified starch 8~15%, extender 15~25%, anion surfactant 2~6%, age resister 1~3%, polyoxypropyleneglycol 2~6%, surplus are water.A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, it is the liquid of outward appearance clear, it is nonpoisonous and tasteless, with superpower penetrating power, can effectively strengthen the coefficient of friction of smooth brick masonry surface, play good, lasting skidproof effect, and it is more notable to meet skidproof effect after water, chance oil, for smooth brick masonry surface, any change will not be produced to the outward appearance of masonry, its preparation method is simple, reaction condition is gentle, is worthy to be popularized.
Description
Technical field
The present invention relates to daily-use chemical industry technical field, more particularly to a kind of anti-skid intensifier for smooth brick masonry surface and its preparation
Method.
Background technology
With the continuous improvement of people's level, people to the performance and appearance requirement of daily life household articles also increasingly
It is high.Existing building decoration earth material is more and more high-grade, attractive in appearance, but is due to that the ground such as the ceramic tile of hard, marble are smooth
Degree is high, causes its coefficient of friction low, and walking smooth, tumble injury event, especially floor tile easily occurs and meets water, meets after oil, easily occurs
It is smooth.In actual life, often occur much to fall down because ground is wet and slippery, tumble injury, or even the thing disabled gives people to cause
Infliction of body and property loss.Ship-and-galley tile is easily occurred in that on the market now, and the surface for which reducing floor tile is smooth
Degree, the anti-skidding of floor tile is increased using ridge design by a small margin is designed in tile surface.However, in practical application, Wo Menhui
It was found that such ship-and-galley tile meets water, meets smooth probability after oil and remain unchanged very high, such as hotel guest-room or the shower floor of family bathroom space
With doorway floor tile, because pin or slippers carry water, smooth probability is significantly increased, if old man and child can make us very much load
The heart；And the ground such as hotel eatery, chafing dish restaurant and kitchen, the problem of drinks, soup, beverage are trickled down inevitably occurs, goes out
Existing personnel are thrilling, and smooth phenomenon happens occasionally, and the ground such as stair, passageway of market, supermarket and office building of handling official business, run into it is rainy,
When snowing, the people for sliding into tumble injury is quite a few.Based on above statement, the present invention proposes a kind of anti-skid intensifier for smooth brick masonry surface
And preparation method thereof.
The content of the invention
The invention aims to solve shortcoming present in prior art, and a kind of smooth brick masonry surface proposed is prevented
Sliding reinforcing agent and preparation method thereof.
A kind of anti-skid intensifier for smooth brick masonry surface, includes the raw material of following percentage by weight：Inorganic acid 1~12%, glycol
Acid 0.5~10%, diisocyanate 3~8%, trimethylolpropane 1~5%, modified starch 8~15%, extender 15~25%, the moon
Ionic surface active agent 2~6%, age resister 1~3%, polyoxypropyleneglycol 2~6%, surplus are water.
It is preferred that, a kind of described anti-skid intensifier for smooth brick masonry surface includes the raw material of following percentage by weight：It is inorganic
Acid 2~10%, Glycolic acid 1~8%, diisocyanate 4~7%, trimethylolpropane 2~4%, modified starch 10~14%, extender
18~22%, anion surfactant 3~5%, age resister 1.5~2.5%, polyoxypropyleneglycol 3~5%, surplus are water.
It is preferred that, a kind of described anti-skid intensifier for smooth brick masonry surface includes the raw material of following percentage by weight：It is inorganic
Acid 6%, Glycolic acid 5%, diisocyanate 5%, trimethylolpropane 3%, modified starch 12%, extender 20%, anionic surface are lived
Property agent 4%, age resister 2%, polyoxypropyleneglycol 4%, surplus be water.
It is preferred that, the modified starch is CMS or acetic starch.
It is preferred that, the extender is one in blanc fixe, talcum powder, wollastonite in powder, titanium dioxide and molecular sieve powder
Plant or arbitrary composition.
It is preferred that, the anion surfactant is neopelex, alkyl glyceryl ether sulfonate, aliphatic acid
One kind in sulfoalkyl ester, sulphosuccinates or alpha-sulfo monocarboxylate.
The invention also provides a kind of preparation method of anti-skid intensifier for smooth brick masonry surface, comprise the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Extender, 18~30min of ultrasonic disperse obtains mixing liquid A；
S2, the trimethylolpropane of the percentage by weight, diisocyanate, age resister and anion surfactant added
Enter high-speed mixer, at 78~98 DEG C, with 280~320r/min rotating speed, 12~18min of high-speed stirred obtains mixed liquid B；
S3, the modified starch and water of the percentage by weight be added in oscillator, at 48~65 DEG C, concussion mixing 15~
25min, is well mixed to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 1~3h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, it is the liquid of outward appearance clear, nontoxic nothing
Taste, with superpower penetrating power, can effectively strengthen the coefficient of friction of smooth brick masonry surface, play good, lasting anti-skidding
Skidproof effect is more notable after effect, and chance water, chance oil, anti-skid intensifier for smooth brick masonry surface proposed by the present invention, for light
Sliding brick masonry surface, will not produce any change to the outward appearance of masonry, increase the invention also provides a kind of smooth brick masonry surface is anti-skidding
The preparation method of strong agent, respectively by extender ultrasonic disperse in the mixed liquor of inorganic acid, Glycolic acid and polyoxypropyleneglycol；
By trimethylolpropane, diisocyanate, age resister and anion surfactant hybrid reaction；Modified starch is dissolved in water
In, the mixture ground and mixed of above-mentioned three step is produced finally by liquid honing machine, its preparation method is simple, reaction condition temperature
With, raw materials used penetrating power is good, safety non-toxic, the anti-skid intensifier good antiskid effect of preparation and persistently, can be widely applied to
The anti-skidding enhancing of the masonries such as ceramic tile, marble, granite, is worthy to be popularized.
Embodiment
The present invention is made with reference to specific embodiment further to explain.
Embodiment one
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, includes the raw material of following percentage by weight：Inorganic acid
10%th, Glycolic acid 5%, diisocyanate 4%, trimethylolpropane 2%, CMS 12%, wollastonite in powder and molecular sieve powder
Composition 18%, sulphosuccinates 4%, age resister 2%, polyoxypropyleneglycol 4%, surplus are water.
Its preparation method, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Wollastonite in powder and molecular sieve powder composition, ultrasonic disperse 20min obtains mixing liquid A；
S2, by the trimethylolpropane of the percentage by weight, diisocyanate, age resister and sulphosuccinates add
High-speed mixer, at 85 DEG C, with 300r/min rotating speed, high-speed stirred 15min obtains mixed liquid B；
S3, the CMS and water of the percentage by weight be added in oscillator, at 50 DEG C, concussion mixing 20min is mixed
Conjunction is uniform to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 2h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
Embodiment two
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, includes the raw material of following percentage by weight：Inorganic acid 5%,
Glycolic acid 3%, diisocyanate 7%, trimethylolpropane 1%, acetic starch 8%, the composition 25% of blanc fixe and talcum powder,
Alkyl glyceryl ether sulfonate 3%, age resister 1.5%, polyoxypropyleneglycol 2%, surplus are water.
Its preparation method, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Blanc fixe and talcum powder composition, ultrasonic disperse 18min obtains mixing liquid A；
S2, the trimethylolpropane of the percentage by weight, diisocyanate, age resister and alkyl glyceryl ether sulfonate added
Enter high-speed mixer, at 78 DEG C, with 280r/min rotating speed, high-speed stirred 12min obtains mixed liquid B；
S3, the acetic starch and water of the percentage by weight be added in oscillator, at 58 DEG C, concussion mixing 22min, mixing
It is uniform to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 1.5h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
Embodiment three
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, includes the raw material of following percentage by weight：Inorganic acid 1%,
Glycolic acid 0.5%, diisocyanate 5%, trimethylolpropane 4%, CMS 10%, the combination of titanium dioxide and molecular sieve powder
Thing 15%, alpha-sulfo monocarboxylate 5%, age resister 1%, polyoxypropyleneglycol 5%, surplus are water.
Its preparation method, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Titanium dioxide and molecular sieve powder composition, ultrasonic disperse 25min obtains mixing liquid A；
S2, by the trimethylolpropane of the percentage by weight, diisocyanate, age resister and alpha-sulfo monocarboxylate add
High-speed mixer, at 92 DEG C, with 320r/min rotating speed, high-speed stirred 18min obtains mixed liquid B；
S3, the CMS and water of the percentage by weight be added in oscillator, at 65 DEG C, concussion mixing 18min is mixed
Conjunction is uniform to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 3h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
Example IV
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, includes the raw material of following percentage by weight：Inorganic acid
12%th, the composition of Glycolic acid 8%, diisocyanate 3%, trimethylolpropane 5%, acetic starch 15%, talcum powder and titanium dioxide
20%th, aliphatic acid sulfoalkyl ester 2%, age resister 3%, polyoxypropyleneglycol 3%, surplus are water.
Its preparation method, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Talcum powder and titanium dioxide composition, ultrasonic disperse 30min obtains mixing liquid A；
S2, by the trimethylolpropane of the percentage by weight, diisocyanate, age resister and aliphatic acid sulfoalkyl ester add
High-speed mixer, at 98 DEG C, with 310r/min rotating speed, high-speed stirred 14min obtains mixed liquid B；
S3, the acetic starch and water of the percentage by weight be added in oscillator, at 60 DEG C, concussion mixing 25min, mixing
It is uniform to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 1h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
Embodiment five
A kind of anti-skid intensifier for smooth brick masonry surface proposed by the present invention, includes the raw material of following percentage by weight：Inorganic acid 8%,
Glycolic acid 10%, diisocyanate 8%, trimethylolpropane 3%, CMS 13%, the group of blanc fixe and molecular sieve powder
Compound 22%, neopelex 6%, age resister 2.5%, polyoxypropyleneglycol 6%, surplus are water.
Its preparation method, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Blanc fixe and molecular sieve powder composition, ultrasonic disperse 22min obtains mixing liquid A；
S2, the trimethylolpropane of the percentage by weight, diisocyanate, age resister and neopelex added
Enter high-speed mixer, at 95 DEG C, with 290r/min rotating speed, high-speed stirred 16min obtains mixed liquid B；
S3, the CMS and water of the percentage by weight be added in oscillator, at 48 DEG C, concussion mixing 15min is mixed
Conjunction is uniform to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 2.5h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
Test uses the brick masonry surface friction after sliding brick masonry surface anti-skid intensifier in the embodiment of the present invention one~five respectively
Coefficient and common masonry skin-friction coefficient, draw following data：
| Skin-friction coefficient | |
| Embodiment one | 1.3 |
| Embodiment two | 0.9 |
| Embodiment three | 1.0 |
| Example IV | 1.2 |
| Embodiment five | 1.1 |
| Common masonry | 0.3 |
The foregoing is only a preferred embodiment of the present invention, but protection scope of the present invention be not limited thereto, it is any
Those familiar with the art the invention discloses technical scope in, technique according to the invention scheme and its invention
Design is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (7)
1. a kind of anti-skid intensifier for smooth brick masonry surface, it is characterised in that include the raw material of following percentage by weight：Inorganic acid 1
~12%, Glycolic acid 0.5~10%, diisocyanate 3~8%, trimethylolpropane 1~5%, modified starch 8~15%, increasing
Measure agent 15~25%, anion surfactant 2~6%, age resister 1~3%, polyoxypropyleneglycol 2~6%, surplus
For water.
2. a kind of anti-skid intensifier for smooth brick masonry surface according to claim 1, it is characterised in that including following weight hundred
Divide the raw material of ratio：Inorganic acid 2~10%, Glycolic acid 1~8%, diisocyanate 4~7%, trimethylolpropane 2~4%, change
Property starch 10~14%, extender 18~22%, anion surfactant 3~5%, age resister 1.5~2.5%, polyoxy
It is water to change propylene glycol 3~5%, surplus.
3. a kind of anti-skid intensifier for smooth brick masonry surface according to claim 1, it is characterised in that including following weight hundred
Divide the raw material of ratio：Inorganic acid 6%, Glycolic acid 5%, diisocyanate 5%, trimethylolpropane 3%, modified starch 12%, increasing
Amount agent 20%, anion surfactant 4%, age resister 2%, polyoxypropyleneglycol 4%, surplus are water.
4. a kind of anti-skid intensifier for smooth brick masonry surface according to claim 1, it is characterised in that the modified starch is
CMS or acetic starch.
5. a kind of anti-skid intensifier for smooth brick masonry surface according to claim 1, it is characterised in that the extender is attached most importance to
One kind or arbitrary composition in spar powder, talcum powder, wollastonite in powder, titanium dioxide and molecular sieve powder.
6. a kind of anti-skid intensifier for smooth brick masonry surface according to claim 1, it is characterised in that the anionic surface
Activating agent is neopelex, alkyl glyceryl ether sulfonate, aliphatic acid sulfoalkyl ester, sulphosuccinates or α-sulphur
One kind in base monocarboxylate.
7. a kind of preparation method of anti-skid intensifier for smooth brick masonry surface according to any one of claim 1-6, its
It is characterised by, comprises the following steps：
S1, inorganic acid, Glycolic acid and the polyoxypropyleneglycol mixing by the percentage by weight, add the percentage by weight
Extender, 18~30min of ultrasonic disperse obtains mixing liquid A；
S2, the trimethylolpropane of the percentage by weight, diisocyanate, age resister and anion surfactant added
Enter high-speed mixer, at 78~98 DEG C, with 280~320r/min rotating speed, 12~18min of high-speed stirred obtains mixed liquid B；
S3, the modified starch and water of the percentage by weight be added in oscillator, at 48~65 DEG C, concussion mixing 15~
25min, is well mixed to obtain mixed liquor C；
S4, the mixed liquor C obtained by the mixed liquor A obtained by step S1, the mixed liquid B obtained by step S2 and step S3 is added to liquid
In body grinder, 1~3h is fully ground, required anti-skid intensifier for smooth brick masonry surface is produced.
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710504705.0A CN107201161A (en) | 2017-06-28 | 2017-06-28 | A kind of anti-skid intensifier for smooth brick masonry surface and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710504705.0A CN107201161A (en) | 2017-06-28 | 2017-06-28 | A kind of anti-skid intensifier for smooth brick masonry surface and preparation method thereof |
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| CN201710504705.0A Pending CN107201161A (en) | 2017-06-28 | 2017-06-28 | A kind of anti-skid intensifier for smooth brick masonry surface and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107880847A (en) * | 2017-10-18 | 2018-04-06 | 安徽爱弥儿环境科技有限公司 | A kind of floor tile antilubricant and preparation method thereof |
| CN108300414A (en) * | 2018-02-09 | 2018-07-20 | 佛山市大幸新材料有限公司 | A kind of anti-skidding nano material and preparation method thereof |
| CN108949107A (en) * | 2018-09-05 | 2018-12-07 | 上海世卿防滑防护科技有限公司 | A kind of ground anti-skid preparation manufacture craft |
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| CN1699289A (en) * | 2005-05-10 | 2005-11-23 | 山东师范大学 | Anti-skid intensifier for smooth brick masonry surface and method for preparing same |
| CN105238201A (en) * | 2015-11-06 | 2016-01-13 | 深圳市彩虹精细化工股份有限公司 | Aerosol tile antiskid coating and preparation method thereof |
| CN105647360A (en) * | 2016-04-11 | 2016-06-08 | 长沙友胜建材科技有限公司 | Surface antiskid treating agent |
| CN106118456A (en) * | 2016-06-17 | 2016-11-16 | 广东纳德新材料有限公司 | A kind of ceramic tile antilubricant and its preparation method and application |
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| CN1075976A (en) * | 1993-03-19 | 1993-09-08 | 张梧 | Slipproofing agent |
| CN1374361A (en) * | 2001-03-09 | 2002-10-16 | 蔡先贤 | Anti-skid agent |
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|---|---|---|---|---|
| CN107880847A (en) * | 2017-10-18 | 2018-04-06 | 安徽爱弥儿环境科技有限公司 | A kind of floor tile antilubricant and preparation method thereof |
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Application publication date: 20170926 |