CN107200553A - One kind contains rare earth element porcelain and its preparation technology - Google Patents

One kind contains rare earth element porcelain and its preparation technology Download PDF

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Publication number
CN107200553A
CN107200553A CN201710507485.7A CN201710507485A CN107200553A CN 107200553 A CN107200553 A CN 107200553A CN 201710507485 A CN201710507485 A CN 201710507485A CN 107200553 A CN107200553 A CN 107200553A
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China
Prior art keywords
parts
porcelain
rare earth
earth element
lucium
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CN201710507485.7A
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Chinese (zh)
Inventor
闵海龙
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Suzhou Porcelain Gas Epoch Cleaning Equipment Co Ltd
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Suzhou Porcelain Gas Epoch Cleaning Equipment Co Ltd
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Priority to CN201710507485.7A priority Critical patent/CN107200553A/en
Publication of CN107200553A publication Critical patent/CN107200553A/en
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    • C—CHEMISTRY; METALLURGY
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    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/02—Preparing or treating the raw materials individually or as batches
    • C04B33/13—Compounding ingredients
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B33/00—Clay-wares
    • C04B33/32—Burning methods
    • C04B33/34—Burning methods combined with glazing
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/009—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone characterised by the material treated
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/45—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements
    • C04B41/50—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials
    • C04B41/5022—Coating or impregnating, e.g. injection in masonry, partial coating of green or fired ceramics, organic coating compositions for adhering together two concrete elements with inorganic materials with vitreous materials
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B41/00—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone
    • C04B41/80—After-treatment of mortars, concrete, artificial stone or ceramics; Treatment of natural stone of only ceramics
    • C04B41/81—Coating or impregnation
    • C04B41/85—Coating or impregnation with inorganic materials
    • C04B41/86—Glazes; Cold glazes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3225—Yttrium oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
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    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3224—Rare earth oxide or oxide forming salts thereof, e.g. scandium oxide
    • C04B2235/3227—Lanthanum oxide or oxide-forming salts thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/32—Metal oxides, mixed metal oxides, or oxide-forming salts thereof, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3262—Manganese oxides, manganates, rhenium oxides or oxide-forming salts thereof, e.g. MnO
    • C04B2235/3267—MnO2
    • C—CHEMISTRY; METALLURGY
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3418—Silicon oxide, silicic acids, or oxide forming salts thereof, e.g. silica sol, fused silica, silica fume, cristobalite, quartz or flint
    • C—CHEMISTRY; METALLURGY
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    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/30—Constituents and secondary phases not being of a fibrous nature
    • C04B2235/34—Non-metal oxides, non-metal mixed oxides, or salts thereof that form the non-metal oxides upon heating, e.g. carbonates, nitrates, (oxy)hydroxides, chlorides
    • C04B2235/3427—Silicates other than clay, e.g. water glass
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/02—Composition of constituents of the starting material or of secondary phases of the final product
    • C04B2235/50—Constituents or additives of the starting mixture chosen for their shape or used because of their shape or their physical appearance
    • C04B2235/54—Particle size related information
    • C04B2235/5418—Particle size related information expressed by the size of the particles or aggregates thereof
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B2235/00—Aspects relating to ceramic starting mixtures or sintered ceramic products
    • C04B2235/65—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes
    • C04B2235/656—Aspects relating to heat treatments of ceramic bodies such as green ceramics or pre-sintered ceramics, e.g. burning, sintering or melting processes characterised by specific heating conditions during heat treatment
    • C04B2235/6567—Treatment time

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  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Ceramic Engineering (AREA)
  • Materials Engineering (AREA)
  • Structural Engineering (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Compositions Of Oxide Ceramics (AREA)

Abstract

One kind of the present invention contains rare earth element porcelain, it is characterised in that the porcelain includes the raw material of following parts by weight：Lucium：0.5 2.5 parts；Clay：28 40 parts；Calcined kaolin：10 18 parts；Suzhou soil：8 15 parts；Sepiolite：13 parts；Medical stone：13 parts；Manganese dioxide：17 parts；Quartz sand：38 parts.One kind that the present invention is provided contains rare earth element porcelain, added with lucium so that the porcelain surface burnt out is more fine and smooth penetrating, improves the overall aesthetic property of porcelain, and technique is simple, it is easy to accomplish.

Description

One kind contains rare earth element porcelain and its preparation technology
Technical field
Contain rare earth element porcelain and its preparation technology the present invention relates to one kind.
Background technology
Porcelain is unique creation of Chinese people, and the long civilization of China is represent with its unique national cultural feature, Nowadays, porcelain has goed deep into the life of people as the higher technique of artistic value and commodity.But traditional porcelain is The need for it can not meet people, it is therefore desirable to which a kind of new porcelain replaces.
The content of the invention
To solve above-mentioned problem, contain rare earth element porcelain it is an object of the invention to provide one kind.It is described to contain There is rare earth element porcelain, added with lucium so that the porcelain surface burnt out is more fine and smooth penetrating, improves porcelain whole The aesthetic property of body, and technique is simple, it is easy to accomplish.
To reach above-mentioned purpose, the technical scheme is that：
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：0.5-2.5 parts； Clay：28-40 parts；Calcined kaolin：10-18 parts；Suzhou soil：8-15 parts；Sepiolite：1-3 parts；Medical stone：1-3 parts；Dioxy Change manganese：1-7 parts；Quartz sand：3-8 parts.
Further, the porcelain includes the raw material of following parts by weight：Lucium：1-2 parts；Clay：34-40 Part；Calcined kaolin：10-15 parts；Suzhou soil：11-15 parts；Sepiolite：1-2 parts；Medical stone：1-2 parts；Manganese dioxide：3-7 Part；Quartz sand：5-8 parts.
Further, the porcelain includes the raw material of following parts by weight：Lucium：1.5 part；Clay：38 parts；Forge Burn kaolin：13 parts；Suzhou soil：12 parts；Sepiolite：1.8 part；Medical stone：1.2 part；Manganese dioxide：5 parts；Quartz sand：5.5 Part.
Further, the lucium be at least two of lanthanum rare earth or yttrium element or lanthanum rare earth or yttrium element with On.
Further, the particle diameter of the calcined kaolin is 200 ~ 300 mesh.
A kind of preparation technology containing rare earth element porcelain, comprises the following steps：
（1）It is in proportion that calcined kaolin, Suzhou soil, sepiolite, medical stone, manganese dioxide, quartz is well mixed, wear into fineness For the powder of 100-150 mesh, lucium and clay are added, training mud is prepared, by kiln-firing, system after training mud shaping and drying Obtain plain embryo；
（2）Inside and outside glaze is uniformly wrapped using glaze method is swung in ceramic idiosome inner and outer surfaces, carries out glaze firing, firing must be containing rare earth member Bique device.
Further, the step（1）The concrete operations of middle firing are：650 ~ 700 DEG C of 0.5 ~ 1.5h of calcining are first warming up to, 800 ~ 900 DEG C of 1 ~ 2h of calcining are continuously heating to, then are warming up to 1100 ~ 1180 DEG C of 5 ~ 8h of calcining.
The beneficial effects of the present invention are：
One kind that the present invention is provided contains rare earth element porcelain, added with lucium so that the porcelain surface burnt out is more Refinement is greasy penetrating, improves the overall aesthetic property of porcelain, and technique is simple, it is easy to accomplish.
Embodiment
In order to make the purpose , technical scheme and advantage of the present invention be clearer, it is further detailed with reference to embodiments Describe in detail bright.
Embodiment 1
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：0.5 part；It is viscous Soil：28 parts；Calcined kaolin：10 parts；Suzhou soil：15 parts；Sepiolite：1 part；Medical stone：3 parts；Manganese dioxide：2 parts；Quartz Sand：3 parts.
Embodiment 2
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：1 part；Clay： 30 parts；Calcined kaolin：12 parts；Suzhou soil：11 parts；Sepiolite：1 part；Medical stone：3 parts；Manganese dioxide：7 parts；Quartz sand：6 Part.
Embodiment 3
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：1.5 part；It is viscous Soil：38 parts；Calcined kaolin：13 parts；Suzhou soil：12 parts；Sepiolite：1.8 part；Medical stone：1.2 part；Manganese dioxide：5 parts；Stone Sand：5.5 part.
Embodiment 4
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：1 part；Clay： 35 parts；Calcined kaolin：18 parts；Suzhou soil：8 parts；Sepiolite：2 parts；Medical stone：2 parts；Manganese dioxide：1 part；Quartz sand：8 Part.
Embodiment 5
One kind contains rare earth element porcelain, and the porcelain includes the raw material of following parts by weight：Lucium：2.5 part；It is viscous Soil：40 parts；Calcined kaolin：15 parts；Suzhou soil：12 parts；Sepiolite：2 parts；Medical stone：1 part；Manganese dioxide：3 parts；Quartz Sand：7 parts.
The lucium is more than at least two of lanthanum rare earth or yttrium element or lanthanum rare earth or yttrium element.
A kind of preparation technology containing rare earth element porcelain, comprises the following steps：
（1）It is in proportion that calcined kaolin, Suzhou soil, sepiolite, medical stone, manganese dioxide, quartz is well mixed, wear into fineness For the powder of 100-150 mesh, lucium and clay are added, training mud is prepared, kiln-firing after mud shaping and drying will be trained, first 650 ~ 700 DEG C of 0.5 ~ 1.5h of calcining are warming up to, 800 ~ 900 DEG C of 1 ~ 2h of calcining are continuously heating to, then be warming up to 1100 ~ 1180 DEG C and forge 5 ~ 8h is burnt, element embryo is made；
（2）Inside and outside glaze is uniformly wrapped using glaze method is swung in ceramic idiosome inner and outer surfaces, carries out glaze firing, firing must be containing rare earth member Bique device.
One kind that the present invention is provided contains rare earth element porcelain, added with lucium so that the porcelain table burnt out Face is more fine and smooth penetrating, improves the overall aesthetic property of porcelain, and technique is simple, it is easy to accomplish.
It should be noted that the above embodiments are merely illustrative of the technical solutions of the present invention and it is unrestricted.Although with reference to compared with The present invention is described in detail good embodiment, it will be understood by those within the art that, can be to the technology of invention Scheme is modified or equivalent substitution, and without departing from the scope of technical solution of the present invention, it all should cover the power in the present invention In sharp claimed range.

Claims (7)

1. one kind contains rare earth element porcelain, it is characterised in that the porcelain includes the raw material of following parts by weight：Rare earth is mixed Thing：0.5-2.5 parts；Clay：28-40 parts；Calcined kaolin：10-18 parts；Suzhou soil：8-15 parts；Sepiolite：1-3 parts；Wheat meal Stone：1-3 parts；Manganese dioxide：1-7 parts；Quartz sand：3-8 parts.
2. one kind according to claim 1 contains rare earth element porcelain, it is characterised in that the porcelain includes following weight The raw material of number：Lucium：1-2 parts；Clay：34-40 parts；Calcined kaolin：10-15 parts；Suzhou soil：11-15 parts；Sea Afrodite：1-2 parts；Medical stone：1-2 parts；Manganese dioxide：3-7 parts；Quartz sand：5-8 parts.
3. one kind according to claim 1 contains rare earth element porcelain, it is characterised in that the porcelain includes following weight The raw material of number：Lucium：1.5 part；Clay：38 parts；Calcined kaolin：13 parts；Suzhou soil：12 parts；Sepiolite：1.8 Part；Medical stone：1.2 part；Manganese dioxide：5 parts；Quartz sand：5.5 part.
4. one kind according to claim 1 contains rare earth element porcelain, it is characterised in that the lucium is that lanthanum is dilute More than at least two of soil or yttrium element or lanthanum rare earth or yttrium element.
5. one kind according to claim 1 contains rare earth element porcelain, it is characterised in that the particle diameter of the calcined kaolin For 200 ~ 300 mesh.
6. a kind of preparation technology containing rare earth element porcelain as claimed in claim 1, it is characterised in that including following step Suddenly：
（1）It is in proportion that calcined kaolin, Suzhou soil, sepiolite, medical stone, manganese dioxide, quartz is well mixed, wear into fineness For the powder of 100-150 mesh, lucium and clay are added, training mud is prepared, by kiln-firing, system after training mud shaping and drying Obtain plain embryo；
（2）Inside and outside glaze is uniformly wrapped using glaze method is swung in ceramic idiosome inner and outer surfaces, carries out glaze firing, firing must be containing rare earth member Bique device.
7. one kind according to claim 6 contains rare earth element porcelain, it is characterised in that the step（1）Middle firing Concrete operations are：650 ~ 700 DEG C of 0.5 ~ 1.5h of calcining are first warming up to, 800 ~ 900 DEG C of 1 ~ 2h of calcining are continuously heating to, then be warming up to 1100 ~ 1180 DEG C of 5 ~ 8h of calcining.
CN201710507485.7A 2017-06-28 2017-06-28 One kind contains rare earth element porcelain and its preparation technology Pending CN107200553A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110746176A (en) * 2018-07-23 2020-02-04 安徽省绩溪旭龙山庄四宝文化有限公司 Chengni inkstone and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001253760A (en) * 2000-03-08 2001-09-18 Toto Ltd China and porcelain
CN105036810A (en) * 2015-07-24 2015-11-11 郏县神前传奇陶瓷钧瓷厂 Black-base mottled composite Tang jun glaze and process for preparing jun porcelain through black-base mottled composite Tang jun glaze

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2001253760A (en) * 2000-03-08 2001-09-18 Toto Ltd China and porcelain
CN105036810A (en) * 2015-07-24 2015-11-11 郏县神前传奇陶瓷钧瓷厂 Black-base mottled composite Tang jun glaze and process for preparing jun porcelain through black-base mottled composite Tang jun glaze

Non-Patent Citations (3)

* Cited by examiner, † Cited by third party
Title
WEIDONG LI等: "The white porcelains from Dehua kiln site of China: Part I. Chemical compositions and the evolution regularity", 《CERAMICS INTERNATIONAL》 *
唐志阳: "稀土元素在陶瓷中的应用", 《陶瓷》 *
姚丽等: "稀土氧化物在陶瓷工业中的应用", 《硅酸盐通报》 *

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110746176A (en) * 2018-07-23 2020-02-04 安徽省绩溪旭龙山庄四宝文化有限公司 Chengni inkstone and preparation method thereof

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Application publication date: 20170926