CN107189594A - A kind of novel aqueous waterproof heat insulating decorative coating and its preparation technology - Google Patents

A kind of novel aqueous waterproof heat insulating decorative coating and its preparation technology Download PDF

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Publication number
CN107189594A
CN107189594A CN201710576124.8A CN201710576124A CN107189594A CN 107189594 A CN107189594 A CN 107189594A CN 201710576124 A CN201710576124 A CN 201710576124A CN 107189594 A CN107189594 A CN 107189594A
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heat insulating
insulating decorative
decorative coating
waterproof heat
agent
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徐兰
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Bo Nuo Environmental Protection Technology Co Ltd Of Ma'an Mountain
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Bo Nuo Environmental Protection Technology Co Ltd Of Ma'an Mountain
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D133/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D125/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by an aromatic carbocyclic ring; Coating compositions based on derivatives of such polymers
    • C09D125/02Homopolymers or copolymers of hydrocarbons
    • C09D125/04Homopolymers or copolymers of styrene
    • C09D125/08Copolymers of styrene
    • C09D125/14Copolymers of styrene with unsaturated esters
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D143/00Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing boron, silicon, phosphorus, selenium, tellurium, or a metal; Coating compositions based on derivatives of such polymers
    • C09D143/04Homopolymers or copolymers of monomers containing silicon
    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/004Reflecting paints; Signal paints
    • CCHEMISTRY; METALLURGY
    • C08ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08LCOMPOSITIONS OF MACROMOLECULAR COMPOUNDS
    • C08L2205/00Polymer mixtures characterised by other features
    • C08L2205/03Polymer mixtures characterised by other features containing three or more polymers in a blend

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Paints Or Removers (AREA)

Abstract

The invention discloses a kind of novel aqueous waterproof heat insulating decorative coating and its preparation technology, belong to building coating field.The coating includes each component of following percentage by weight:Water soluble acrylic acid olefine resin 30% 60%, watery water-proofing agent 2% 10%, aqueous color paste 15% 35%, heat-insulation functional material 3% 12%, auxiliary agent 2% 9%, surplus is deionized water.The technique mainly includes two steps, and hydrate colour mill base is prepared first, then adds hydrate colour mill base in the preparation of coating, you can obtain Waterproof heat insulating decorative coating.The present invention can be applied to the ornamental water-proof heat-insulating paint of decorative tile, building wall, multi-color system required by sheet metal surface, high glaze by using by compound constitute of the aqueous color paste containing infrared external reflection nano dye, solar reflectivity is up to 87%, and it is low 15 DEG C with reference to model temperature that heat insulating temperature difference testing result scribbles Waterproof heat insulating decorative coating model temperature ratio;The sample ageing-resistant time is up to 1500h and colour-fast, not efflorescence.

Description

A kind of novel aqueous waterproof heat insulating decorative coating and its preparation technology
Technical field
Decorative tile, building wall, sheet metal are can be applied to the invention belongs to building coating field, more particularly to one kind The waterproof heat insulating decorative coating and its preparation technology on surface.
Background technology
According to statistics, building energy consumption accounts for the 30% of whole society's total energy consumption, and China's building energy consumption is 2-4 times of developed country.Carry High constructure thermal and insulating performance, improve building using function, it is energy-saving that to be that current building selection design is another important examine Worry factor.Insulating moulding coating can be to wavelength in 400nm-2500nm scopes solar infrared and ultraviolet reflect, it is to avoid The heat of the sun carries out accumulation heating in body surface, plays heat-insulated effect, meanwhile, heat radiation can be carried out automatically again and reached The purpose of radiating, reduces the temperature of object, also still possesses above-mentioned functions even in cloudy day and night coating, also can radiant heat Amount, so as to reduce the temperature of object.Water-repellent paint is that a class is coated on formation densification after the body surface protected or decorated The protective coating of film, has increasing application in engineering construction field.In use, only the coating with single performance is past Toward it is impossible to meet use demand.When for being painted with crackle and when needing heat-insulated object, it is necessary to coating have concurrently waterproof with Every thermal property, at this moment common single insulating moulding coating or water-repellent paint cannot meet above-mentioned requirements.
And for decoration functions, defencive function and livability improve function building coating for, energy-saving and environmental protection and Safety is particularly important, is also the effective measures that various countries' target for energy-saving and emission-reduction is implemented.A series of energy-conserving and environment-protective building coatings meet the tendency of and It is raw, wherein most typically white roof paint and white or light wall covering, can significantly reduce temperature in building, So as to realize building energy conservation requirement.But for the building surface of some chromatic colour decorative effects, this waterproof and heat-insulating effect is just It is unobvious, and there is fading decolourization phenomenon.
The content of the invention
In order to overcome the defect that above prior art is present, make the anti-of coating system it is an object of the invention to provide a kind of Water heat insulating function is further strengthened, can be applied to decorative tile, building wall, the water-proof heat-insulating paint of sheet metal surface and its Preparation technology.
The purpose of the present invention can be achieved through the following technical solutions:
A kind of novel aqueous waterproof heat insulating decorative coating, it includes each component of following percentage by weight:Aqueous acrylamide Sour olefine resin 30%-60%, watery water-proofing agent 2%-10%, aqueous color paste 15%-35%, heat-insulation functional material 3%-12%, Auxiliary agent 2%-9%, surplus are deionized water.
Further, described water soluble acrylic acid olefine resin is acrylic elastic emulsion, pure acrylic acid microemulsion, the breast of silicon third One or two kinds of combinations of liquid, acrylate and vinyl acetate emulsion or styrene-acrylic emulsion.
Further, described watery water-proofing agent is waterproofing agent of organosilicon, and waterproofing agent of organosilicon is aqueous, solvent-free uses With the silicone-modified polysiloxane emulsion of functional group.
Further, described aqueous color paste includes each component of following percentage by weight:Infrared reflective pigment 25%- 45%th, defoamer 1.5%-6.0%, wetting agent 1.5%-3.0%, dispersant 6.0%-15%, 1.5%-4.5% thickener, Surplus is deionized water.
Further, described infrared reflective pigment is the Ti-Y-Mo (5.5-6.45 of yellow:2.0-3.0:1.0- 1.6) nano dye, red Ti-Fe-Cr (4.5-6.4:1.3-1.8:0.4-1.2) nano dye, the Ti-Zn-Co of green (4.8-6.6:1.8-2.8:1.4-2.2) Ti-Mn-Nd (the 5.5-7.4 of nano dye, purple:1.1-1.9:0.3-0.9) nanometer One or both of pigment is combined.
Further, the heat-insulation functional material is hollow ceramic microspheres, hollow glass micropearl, floating bead, closed-cell expanded treasure One kind in Zhu Yan Void-rich materials.
Further, described auxiliary agent is defoamer 0.2%-1.3%, coalescents 0.5%-2.5%, dispersant 0.3%-2.0%, levelling agent 0.1%-0.5%, thickener 0.3%-2.0%, preservative 0.1%-0.5%.
Further, described auxiliary agent also includes the 0.5%-1.5% kind sour zinc of lubricant Pork and beans, and the kind sour zinc of Pork and beans has Stronger adhesive force, lubricity is good, can improve coating fouling precipitation phenomenon.
A kind of preparation technology of novel aqueous waterproof heat insulating decorative coating, is specifically carried out according to the following steps:
1) preparation of aqueous color paste
A, prepare infrared reflective nano dye
Pigment is mixed 1 hour in ethanol medium using ball mill grinding in specific proportions, by the precursor powder It is placed in Muffle furnace, at 1000 DEG C, insulation is calcined for 3 hours, and furnace cooling obtains infrared reflective nano dye;
B, in high speed dispersor dispersion tank add component amount deionized water, start dispersion machine, rotating speed is adjusted to 1100r/min, sequentially adds defoamer, wetting agent, dispersant, thickener, and rotating speed is carried to 1400r/min, disperses 5-10min; Rotating speed is down to 1100r/min, and infrared reflective pigment is slowly added at agitating shaft, disperses 30min- after having fed at a high speed 60min;Add after defoamer, with 200r/min froth breaking 10min, shut down;Further ground 1 hour on three-roller, use ammoniacal liquor PH value is adjusted to 7.8~9.0, aqueous color paste is filtered to obtain;
2) preparation of Waterproof heat insulating decorative coating
Water soluble acrylic acid olefine resin, deionized water, defoamer and the dispersant for sequentially adding component amount are scattered to dispersion machine In tank, rotating speed is adjusted to 300r/min, aqueous color paste is slowly added to, then dispersion mixing 40-60min sequentially adds thereto Waterproofing agent of organosilicon, hollow ceramic microspheres, finally add defoamer, coalescents, levelling agent, thickener, anti-corrosion thereto again Agent is filtrated to get Waterproof heat insulating decorative coating after 10 minutes with 500r/min dispersion mixings.
Beneficial effects of the present invention:
Compared with prior art, advantage is that the present invention is compound by using the aqueous color paste containing infrared external reflection nano dye Constitute can be applied to decorative tile, building wall, multi-color system, the ornamental waterproof of high glaze required by sheet metal surface every Hot coating, because this infrared external reflection nano dye reflectivity itself may be up to 96%, obtained waterproof heat insulating decorative is applied Material solar reflectivity is up to 87%, and heat insulating temperature difference testing result scribbles the reference of Waterproof heat insulating decorative coating model temperature ratio Model temperature is low 15 DEG C;The ageing-resistant time of sample is up to 1500h and colour-fast, not efflorescence;Impermeability, low temperature flexibility, drawing The water resistancees such as intensity clothes are stretched to reach《Polymer emulsion building water-proof paint》(JC/T864-2008) II classes product index requirement. With high-weatherability, waterproof and the multifunctional integrated water-borne heat-insulating environmental protection coating material of insulation, its heat-proof quality, water resistance, Decoration performance, workability and environmental-protecting performance all reach concerned countries or Industry code requirements.
Embodiment
Technical scheme is clearly and completely described below in conjunction with embodiment, it is clear that described reality It is only a part of embodiment of the invention to apply example, rather than whole embodiments.Based on the embodiment in the present invention, this area is general All other embodiment that logical technical staff is obtained under the premise of creative work is not made, belongs to what the present invention was protected Scope.
Embodiment 1
A kind of novel aqueous waterproof heat insulating decorative Paint preparation technology, is specifically carried out according to the following steps:
1) preparation of aqueous color paste
A, the Ti-Y-Mo nano dyes for preparing yellow
The molybdenum oxide of 30kg titanium dioxide, 12kg yittrium oxide and 5kg is utilized into ball mill grinding in ethanol medium Mixing 1 hour, the precursor powder is placed in Muffle furnace, and at 1000 DEG C, insulation is calcined for 3 hours, and furnace cooling is produced To the Ti-Y-Mo nano dyes of yellow, infrared reflectivity 91-94%, average grain diameter 180nm;
B, in high speed dispersor dispersion tank add 43kg deionized water, start dispersion machine, rotating speed is adjusted to 1100r/ Min, sequentially adds 1kg defoamers, 2kg wetting agents, 9kg dispersants, and 3kg thickeners, rotating speed is carried to 1400r/min, disperses 8min;Rotating speed is down to 1100r/min, and 40kg yellow Ti-Y-Mo nano dyes are slowly added at agitating shaft, after having fed at a high speed Scattered 30min;Add after 2kg defoamers, with 200r/min froth breaking 10min, shut down;Further ground 1 hour on three-roller, PH value is adjusted to 8.0 with ammoniacal liquor, filters to obtain aqueous yellow pulp;
2) preparation of Waterproof heat insulating decorative coating
30kg acrylic elastic emulsion, 20kg deionized water, 2kg defoamer and dispersant 0.5kg are added and divided Dissipate in machine dispersion tank, rotating speed is adjusted to 300r/min, be slowly added to 35kg aqueous yellow pulp, dispersion mixing 40-60min, so Add 3.5kg waterproofing agent of organosilicon, 7kg hollow ceramic microspheres thereto afterwards, finally add the kind sour zinc of Pork and beans thereto again 0.5kg, defoamer 0.3kg, coalescents 2.5kg, levelling agent 0.1kg, thickener 0.3kg, preservative 0.1kg are with 500r/min Dispersion mixing is filtrated to get Waterproof heat insulating decorative coating after 10 minutes.
Embodiment 2
1) preparation of aqueous color paste
A, the Ti-Fe-Cr nano dyes for preparing red
30kg titanium dioxide, 7.5kg iron oxide and 0.5kg chromium oxide are mixed in ethanol medium using ball mill grinding Close 1 hour, the precursor powder is placed in Muffle furnace, insulation is calcined for 3 hours at 1000 DEG C, and furnace cooling obtains Red Ti-Fe-Cr nano dyes, infrared reflectivity 92-95%, average grain diameter 165nm;
B, the Ti-Zn-Co nano dyes for preparing green
25kg titanium dioxide, 1kg zinc oxide and 1kg cobalt oxides are mixed 1 in ethanol medium using ball mill grinding Hour, the precursor powder is placed in Muffle furnace, at 1000 DEG C, insulation is calcined for 3 hours, and furnace cooling obtains green Ti-Zn-Co nano dyes, infrared reflectivity 90-94%, average grain diameter 190nm;
C, in high speed dispersor dispersion tank add 44kg deionized water, start dispersion machine, rotating speed is adjusted to 1100r/ Min, sequentially adds 0.8kg defoamers, 3.0kg wetting agents, 9kg dispersants, 3kg thickeners, and rotating speed is carried to 1400r/min, point Dissipate 10min;Rotating speed is down to 1100r/min, be slowly added to successively at agitating shaft 19kg red Ti-Fe-Cr nano dyes and 19kg green Ti-Zn-Co nano dyes, disperse at a high speed 40min after having fed;Add after 2.2kg defoamers, with 200r/ Min froth breaking 10min, shut down;Further ground 1 hour on three-roller, pH value is adjusted to 8.2 with ammoniacal liquor;Filter to obtain aqueous palm fibre Mill base;
2) preparation of Waterproof heat insulating decorative coating
The pure acrylic acid microemulsion of 35kg styrene-acrylic emulsions and 25kg, 5kg deionized water, 0.2kg will be sequentially added to disappear Infusion and dispersant 0.6kg are added in dispersion machine dispersion tank, and rotating speed is adjusted into 300r/min, 21kg aqueous brown is slowly added to Then slurry, dispersion mixing 40-60min adds 3.8kg waterproofing agent of organosilicon, 6.2kg hollow glass micropearl, most thereto Add the kind sour zinc 0.8kg of Pork and beans, defoamer 0.3kg, coalescents 1.6kg, levelling agent 0.2kg, thickener thereto again afterwards 0.4kg, preservative 0.3kg are filtrated to get Waterproof heat insulating decorative coating after 10 minutes with 500r/min dispersion mixings.
Embodiment 3
1) preparation of aqueous color paste
A, the Ti-Fe-Cr nano dyes for preparing red
30kg titanium dioxide, 7.5kg iron oxide and 0.5kg chromium oxide are mixed in ethanol medium using ball mill grinding Close 1 hour, the precursor powder is placed in Muffle furnace, insulation is calcined for 3 hours at 1000 DEG C, and furnace cooling obtains Red Ti-Fe-Cr nano dyes, infrared reflectivity 92-95%, average grain diameter 165nm;
B, the Ti-Mn-Nd nano dyes for preparing purple
30kg titanium dioxide, 8.0kg manganese chlorides and 0.4kg neodymia are mixed in ethanol medium using ball mill grinding Close 1 hour, the precursor powder is placed in Muffle furnace, insulation is calcined for 3 hours at 1000 DEG C, and furnace cooling obtains Red Ti-Fe-Cr nano dyes, infrared reflectivity 92-96%, average grain diameter 175nm;
C, in high speed dispersor dispersion tank add 45kg deionized water, start dispersion machine, rotating speed is adjusted to 1100r/ Min, sequentially adds defoamer 0.8kg, 3.0kg wetting agent, 10kg dispersants, 3kg thickeners, and rotating speed is carried to 1400r/min, point Dissipate 5-10min;Rotating speed is down to 1100r/min, is slowly added to 20kg red Ti-Fe-Cr nano dyes successively at agitating shaft With the Ti-Mn-Nd nano dyes of 16kg purples, disperse 60min after having fed at a high speed;Add after 2.2kg defoamers, with 200r/ Min froth breaking 10min, shut down;Further ground 1 hour on three-roller, pH value is adjusted to 7.9 with ammoniacal liquor;Filter to obtain aqueous purple Red mill base;
2) preparation of Waterproof heat insulating decorative coating
To sequentially add 30kg silicone acrylic emulsion, 15kg acrylate and vinyl acetate emulsions, 10kg deionized water, 0.3kg defoamer and Dispersant 0.8kg is added in dispersion machine dispersion tank, and rotating speed is adjusted into 300r/min, 31kg aqueous aubergine color is slowly added to Then slurry, dispersion mixing 40-60min adds 3.3kg waterproofing agent of organosilicon, 5.7kg closed-cell expanded perlite thereto, Finally add the kind sour zinc 1.5kg of Pork and beans, defoamer 0.4kg, coalescents 1.0kg, levelling agent 0.3kg, thickener thereto again 0.5kg, preservative 0.2kg are filtrated to get Waterproof heat insulating decorative coating after 10 minutes with 500r/min dispersion mixings.
According to relevant national standard, to the basic performance of Waterproof heat insulating decorative coating, the test result such as institute of table 1 Show.
The basic performance test result of the Waterproof heat insulating decorative coating of table 1
Present invention disclosed above preferred embodiment is only intended to help and illustrates the present invention.Preferred embodiment is not detailed All details of narration, it is only described embodiment that the invention is not limited yet.Obviously, according to the content of this specification, It can make many modifications and variations.This specification is chosen and specifically describes these embodiments, is to preferably explain the present invention Principle and practical application so that skilled artisan can be best understood by and utilize the present invention.The present invention is only Limited by claims and its four corner and equivalent.

Claims (9)

1. a kind of novel aqueous waterproof heat insulating decorative coating, it is characterised in that it includes each component of following percentage by weight: Water soluble acrylic acid olefine resin 30%-60%, watery water-proofing agent 2%-10%, aqueous color paste 15%-35%, heat-insulation functional material 3%-12%, auxiliary agent 2%-9%, surplus are deionized water.
2. Waterproof heat insulating decorative coating according to claim 1, it is characterised in that described water soluble acrylic acid alkene Resin is selected from acrylic elastic emulsion, pure acrylic acid microemulsion, silicone acrylic emulsion, the one or two of acrylate and vinyl acetate emulsion or styrene-acrylic emulsion Mixing.
3. Waterproof heat insulating decorative coating according to claim 1, it is characterised in that described watery water-proofing agent is Waterproofing agent of organosilicon.
4. Waterproof heat insulating decorative coating according to claim 1, it is characterised in that described aqueous color paste is included The each component of following percentage by weight:Infrared reflective pigment 25%-45%, defoamer 1.5%-6.0%, wetting agent 1.5%- 3.0%th, dispersant 6.0%-15%, 1.5%-4.5% thickeners, surplus are deionized water.
5. Waterproof heat insulating decorative coating according to claim 4, it is characterised in that described infrared reflective face Expect the Ti-Y-Mo nano dyes for yellow, red Ti-Fe-Cr nano dyes, the Ti-Zn-Co nano dyes of green, purple Ti-Mn-Nd nano dyes one or two kinds of mixing.
6. Waterproof heat insulating decorative coating according to claim 1, it is characterised in that the heat-insulation functional material is One of which in hollow ceramic microspheres, hollow glass micropearl, floating bead, closed-cell expanded perlite Void-rich material.
7. Waterproof heat insulating decorative coating according to claim 1, it is characterised in that described auxiliary agent is defoamer 0.2%-1.3%, coalescents 0.5%-2.5%, dispersant 0.3%-2.0%, levelling agent 0.1%-0.5%, thickener 0.3%-2.0%, preservative 0.1%-0.5%.
8. Waterproof heat insulating decorative coating according to claim 7, it is characterised in that described auxiliary agent also includes The 0.5%-1.5% kind sour zinc of lubricant Pork and beans.
9. a kind of preparation technology of novel aqueous waterproof heat insulating decorative coating, it is characterised in that specifically carry out according to the following steps:
1) preparation of aqueous color paste
A, prepare infrared reflective nano dye
Pigment is mixed 1 hour in ethanol medium using ball mill grinding in specific proportions, the precursor powder is placed in In Muffle furnace, at 1000 DEG C, insulation is calcined for 3 hours, and furnace cooling obtains infrared reflective nano dye;
B, in high speed dispersor dispersion tank add component amount deionized water, start dispersion machine, rotating speed is adjusted to 1100r/ Min, sequentially adds defoamer, wetting agent, dispersant, thickener, and rotating speed is carried to 1400r/min, disperses 5-10min;Rotating speed drops To 1100r/min, infrared reflective pigment is slowly added at agitating shaft, disperses 30min-60min after having fed at a high speed;Add After defoamer, with 200r/min froth breaking 10min, shut down;Further on three-roller grind 1 hour, with ammoniacal liquor adjust pH value to 7.8~9.0, filter to obtain aqueous color paste;
2) preparation of Waterproof heat insulating decorative coating
Sequentially add component amount enters dispersion machine dispersion tank by water soluble acrylic acid olefine resin, deionized water, defoamer and dispersant In, rotating speed is adjusted to 300r/min, aqueous color paste is slowly added to, then dispersion mixing 40-60min has sequentially added thereto Machine silicon waterproofing agent, hollow ceramic microvesicle, finally add defoamer, coalescents, levelling agent, thickener, preservative thereto again Waterproof heat insulating decorative coating is filtrated to get after 10 minutes with 500r/min dispersion mixings.
CN201710576124.8A 2017-07-14 2017-07-14 A kind of novel aqueous waterproof heat insulating decorative coating and its preparation technology Pending CN107189594A (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107892849A (en) * 2017-11-22 2018-04-10 江门市水星涂料科技有限公司 A kind of reflective heat-insulation paint and preparation method thereof
CN108360294A (en) * 2018-02-08 2018-08-03 深圳市能驭生态化工科技有限公司 A kind of fire protection flame retarding water paint and preparation method thereof for paper product
CN108893023A (en) * 2018-08-16 2018-11-27 李晟隆 A kind of building exterior wall heat preserving coating and preparation method thereof
CN109054569A (en) * 2018-07-05 2018-12-21 吕莉 A kind of dedicated plank water-repellent paint in bathroom
CN109207066A (en) * 2018-08-08 2019-01-15 佛山科学技术学院 A kind of aquosity heat insulating heat preserving paint and preparation method thereof
CN109796802A (en) * 2018-12-07 2019-05-24 浙江传化涂料有限公司 A kind of preparation method and applications of the hollow carbosphere of carbon coating titanium dioxide
CN110452570A (en) * 2019-08-12 2019-11-15 中山爱因新材料有限公司 A kind of heat-reflecting heat-insulating water-repellent paint
CN112266670A (en) * 2020-10-28 2021-01-26 石家庄日加精细矿物制品有限公司 Coating for improving pollution resistance of particles
CN113388268A (en) * 2021-06-18 2021-09-14 浙江华源颜料股份有限公司 Iron oxide black pigment with near-infrared reflection function and preparation method thereof
CN116120066A (en) * 2023-01-18 2023-05-16 中稀(凉山)稀土有限公司 Molybdenum-titanate rare earth cold pigment and preparation method thereof

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102643587A (en) * 2012-03-21 2012-08-22 深圳市嘉达节能环保科技有限公司 Water-in water type colorful thermal insulation coating and preparation method thereof
CN103725124A (en) * 2013-08-02 2014-04-16 太仓派欧技术咨询服务有限公司 High-radiation heat-insulated coating

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102643587A (en) * 2012-03-21 2012-08-22 深圳市嘉达节能环保科技有限公司 Water-in water type colorful thermal insulation coating and preparation method thereof
CN103725124A (en) * 2013-08-02 2014-04-16 太仓派欧技术咨询服务有限公司 High-radiation heat-insulated coating

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107892849A (en) * 2017-11-22 2018-04-10 江门市水星涂料科技有限公司 A kind of reflective heat-insulation paint and preparation method thereof
CN108360294A (en) * 2018-02-08 2018-08-03 深圳市能驭生态化工科技有限公司 A kind of fire protection flame retarding water paint and preparation method thereof for paper product
CN108360294B (en) * 2018-02-08 2021-02-12 深圳市能驭生态化工科技有限公司 Fireproof flame-retardant water-based paint for paper products and preparation method thereof
CN109054569A (en) * 2018-07-05 2018-12-21 吕莉 A kind of dedicated plank water-repellent paint in bathroom
CN109207066A (en) * 2018-08-08 2019-01-15 佛山科学技术学院 A kind of aquosity heat insulating heat preserving paint and preparation method thereof
CN108893023A (en) * 2018-08-16 2018-11-27 李晟隆 A kind of building exterior wall heat preserving coating and preparation method thereof
CN109796802A (en) * 2018-12-07 2019-05-24 浙江传化涂料有限公司 A kind of preparation method and applications of the hollow carbosphere of carbon coating titanium dioxide
CN110452570A (en) * 2019-08-12 2019-11-15 中山爱因新材料有限公司 A kind of heat-reflecting heat-insulating water-repellent paint
CN112266670A (en) * 2020-10-28 2021-01-26 石家庄日加精细矿物制品有限公司 Coating for improving pollution resistance of particles
CN113388268A (en) * 2021-06-18 2021-09-14 浙江华源颜料股份有限公司 Iron oxide black pigment with near-infrared reflection function and preparation method thereof
CN116120066A (en) * 2023-01-18 2023-05-16 中稀(凉山)稀土有限公司 Molybdenum-titanate rare earth cold pigment and preparation method thereof
CN116120066B (en) * 2023-01-18 2024-04-26 中稀(凉山)稀土有限公司 Molybdenum-titanate rare earth cold pigment and preparation method thereof

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Application publication date: 20170922