CN107188469A - A kind of fire-resistant waterproof insulation material and preparation method thereof - Google Patents
A kind of fire-resistant waterproof insulation material and preparation method thereof Download PDFInfo
- Publication number
- CN107188469A CN107188469A CN201710429336.3A CN201710429336A CN107188469A CN 107188469 A CN107188469 A CN 107188469A CN 201710429336 A CN201710429336 A CN 201710429336A CN 107188469 A CN107188469 A CN 107188469A
- Authority
- CN
- China
- Prior art keywords
- parts
- fire
- insulation material
- mixture
- resistant waterproof
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B28/00—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements
- C04B28/24—Compositions of mortars, concrete or artificial stone, containing inorganic binders or the reaction product of an inorganic and an organic binder, e.g. polycarboxylate cements containing alkyl, ammonium or metal silicates; containing silica sols
- C04B28/26—Silicates of the alkali metals
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/00017—Aspects relating to the protection of the environment
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/27—Water resistance, i.e. waterproof or water-repellent materials
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2111/00—Mortars, concrete or artificial stone or mixtures to prepare them, characterised by specific function, property or use
- C04B2111/20—Resistance against chemical, physical or biological attack
- C04B2111/28—Fire resistance, i.e. materials resistant to accidental fires or high temperatures
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B2201/00—Mortars, concrete or artificial stone characterised by specific physical values
- C04B2201/30—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values
- C04B2201/32—Mortars, concrete or artificial stone characterised by specific physical values for heat transfer properties such as thermal insulation values, e.g. R-values for the thermal conductivity, e.g. K-factors
Abstract
The invention discloses a kind of fire-resistant waterproof insulation material, include the raw material of following parts by weight：Native 10 16 parts of the filler of 15 25 parts of polyvinyl alcohol, 12 25 parts of lightweight sierozem power, 8 18 parts of hydroxymethyl cellulose, 37 parts of hydrophober, 8 12 parts of negative ion powder for building, mineral, 8 14 parts of fire retardant, 6 12 parts of reinforcing fibre, 7 15 parts of inorganic binder, 35 45 parts of water.The insulation material of the present invention has relatively low water absorption rate and thermal conductivity factor, and insulation, fire prevention, stability are good, there is stronger mechanical strength, it is rub resistance, corrosion-resistant, service life is longer, additionally can persistently discharge the pollutant in anion and absorption air, reaches the effect of purification air；The raw material components of the present invention are safe and reliable simultaneously, environmental sound, and raw material is easy to get, and cost is relatively low, and technique is concise, with higher practical value and good application prospect.
Description
Technical field
The present invention relates to water-proof heat-insulation material technical field, and in particular to a kind of fire-resistant waterproof insulation material and its preparation side
Method.
Background technology
State's heat insulating material for external industry has had very long history, and building energy conservation accounts for the overwhelming majority, such as U.S. with insulation material
Building thermal insulation material accounts for eighty per cant or so of all insulation materials since 1987, the Western European countries such as Sweden and Finland most probably with
On asbestos product be used for building energy conservation.The heat-insulation material that China is used for building energy conservation is then relatively fewer.At present, country just
Relevant policies are being put into effect, building energy conservation are being widelyd popularize, this will be greatly promoted application of the heat-insulation material in architectural engineering.
The expense of China every year for building heat preservation is just in cumulative year after year, but most of the insulation material used or single varieties, work(
The single product of energy, directly results in substantial amounts of energy consumption.
Country also requires that more and more stricter to the security of the insulation material used in building, it is ensured that the requirement of health and
The requirement of personal safety, material must be nontoxic, harmless, pollution-free and must prevent fires, almost completely without anti-in organic material
Fiery ability, some, which even meet fire, can discharge toxic gas.With continuing deeply for national propulsion energy-saving environmental protection, building energy conservation method
There is wide market development space in the implementation of rule, future architecture energy-saving and heat-insulating material.Now, the positive court of global heat preserving and insulating material
Efficiently, energy-conservation, thin layer, shield integration direction is developed outside heat-insulated, waterproof, in Development of Novel heat preserving and insulating material and meets structure
Energy-saving insulating technique is emphasized targetedly to use heat-insulation material simultaneously, more, by standard criterion design and construction, makes great efforts to improve
Insulating efficiency and reduce cost.Inorganic heat insulation material constitutes not aging, with will not thermal expansion, cold events, cracking resistance, peel
Etc. good self-characteristic.Compared with general insulation material, there is oneself special performance superiority, being can not in construction material
The performance characteristics of replacement, and cost is relatively low, can save lot of materials, cost of labor.But presently commercially available inorganic heat insulation material is general
Store-through causes substantial amounts of energy consumption the problem of the coefficient of heat conduction is big.
On the other hand, the insulation material of market today circulation, performance is not perfect enough, and fire protecting performance difference is, it is necessary to which bonding agent, is applied
Work is bothered, solid, firm performance relative reduction, cuts consumption resource greatly, structure waits optimization.Such as (polystyrene foam plate,
Polyurathamc) though with relatively low water absorption rate and heat conductivility, do not prevent fires；Using cement as the inorganic heat preservation of bonding agent
Heat-barrier material, (such as foamed cement material, cement base perlite material, concrete-based polyphenylene granule putty) water absorption rate and heat conduction system
The higher, energy-saving effect of number is bad；The warming plate complex manufacturing technology of other inorganic material (such as foam glass, floating bead) production,
Fragility is big, and difficulty of construction is big, and cost is high.
The content of the invention
For the defect of prior art, it is an object of the invention to provide a kind of fire-resistant waterproof insulation material, the insulation material
With relatively low water absorption rate and thermal conductivity factor, insulation, fire prevention, stability are good, there is a stronger mechanical strength, rub resistance, corrosion-resistant,
Service life is longer, additionally can persistently discharge the pollutant in anion and absorption air, reaches the effect of purification air
Really；The raw material components of the present invention are safe and reliable simultaneously, environmental sound, and raw material is easy to get, and cost is relatively low, and technique is concise, has
Higher practical value and good application prospect.
The present invention solves technical problem and adopted the following technical scheme that：
The invention provides a kind of fire-resistant waterproof insulation material, include the raw material of following parts by weight：
It is 15-25 parts of polyvinyl alcohol, 12-25 parts of lightweight sierozem power, 8-18 parts of hydroxymethyl cellulose, 3-7 parts of hydrophober, for building
Native 10-16 parts of the filler of 8-12 parts of negative ion powder, mineral, 8-14 parts of fire retardant, 6-12 parts of reinforcing fibre, inorganic binder 7-15
Part, 35-45 parts of water.
Preferably, the fire-resistant waterproof insulation material includes the raw material of following parts by weight：
20 parts of polyvinyl alcohol, 18 parts of lightweight sierozem power, 13 parts of hydroxymethyl cellulose, hydrophober 5,10 parts of negative ion powder for building,
13 parts of filler of mineral soil, 11 parts of fire retardant, 9 parts of reinforcing fibre, 11 parts of inorganic binder, 40 parts of water.
Preferably, the hydrophober is calcium stearate, aluminum stearate or sodium methyl silicate, compares 2 according to weight:1:1 composition
Mixture.
Preferably, the negative ion powder for building is that tourmaline powder, neodymia, terbium peroxide compare 5 according to weight:1:
The mixture of 1 composition.
Preferably, the native filler of the mineral is bentonite, kaolin, attapulgite according to 2:1:The mixture of 1 composition, institute
State bentonite, kaolin, attapulgite to calcine 1 hour in the case where temperature is 700-750 DEG C, 0.5 hour is incubated, after natural cooling
Discharging, is finally made the powder that particle mean size is below 500nm by the bentonite after calcining, kaolin, attapulgite.
Preferably, the fire retardant is graphite, magnesium hydroxide, aluminium hydroxide and halogenated phosphate, compares 2 according to weight:1:
2:The mixture of 1 composition.
Preferably, the reinforcing fibre is glass fibre, silicon nitride fiber and alumina silicate fibre according to weight ratio 3:1:2 groups
Into mixture.
Preferably, the inorganic binder is one kind in waterglass, aluminium hydroxide or zinc oxide.
The present invention also provides a kind of preparation method of fire-resistant waterproof insulation material, comprises the following steps：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, 10-20 points of stirring
Clock, speed of agitator 200-300r/min, adds water, is warming up to 45-65 DEG C, continues to stir 15-25 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 300-
400 r/min, are stirred 15-25 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir
45-65 minutes, obtain mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed in the case where hydraulic press pressure is 40-60MPa, will
Dried in feedstock module feeding baking oven after shaping, drying temperature is 100-120 DEG C, and drying time is 1-3 hours, natural cooling
The fire-resistant waterproof insulation material invented.
Preferably, the preparation process of the fire-resistant waterproof insulation material is：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, stir 15 minutes,
Speed of agitator 250r/min, adds water, is warming up to 55 DEG C, continues to stir 20 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 350r/
Min, is stirred 20 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir 55 minutes, obtains
Mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed, will be molded in the case where hydraulic press pressure is 50MPa
Dried in feedstock module feeding baking oven afterwards, drying temperature is 110 DEG C, and drying time is 2 hours, what natural cooling was invented
Fire-resistant waterproof insulation material.
Compared with prior art, the present invention has following beneficial effect：
（1）The negative ion powder for building added in a kind of fire-resistant waterproof insulation material of the present invention, predominantly tourmaline powder, oxygen
Change neodymium, terbium peroxide composition mixture, its enable to prepare insulation material persistently discharge anion, anion
With anti-oxidant (reproducibility) and anti-aging outstanding role, the feature of environmental protection of material is effectively increased.
（2）A kind of fire-resistant waterproof insulation material of the present invention employs the native filler of mineral, predominantly bentonite, kaolin,
Attapulgite, the bentonite, kaolin, attapulgite are the powdered thing of grinding title Nano grade after calcining at high temperature
Body, considerably increases its specific surface area, can be good at the pollutant in absorption air, such as formaldehyde, benzene harmful substance, significantly
Add the function of the purification air of insulation material.
（3）A kind of fire-resistant waterproof insulation material of the present invention is using polyvinyl alcohol as material of main part, auxiliary addition inorganic bond
Agent and hydroxymethyl cellulose, substantially increase the compactness and slickness of material surface, effectively enhance the waterproof thermal-insulated of material
Performance.
（4）The fire retardant that a kind of fire-resistant waterproof insulation material of the present invention is used includes graphite, magnesium hydroxide, aluminium hydroxide
And halogenated phosphate, it can be that the insulation material prepared has good fire resistant flame retardant performance.
（5）A kind of fire-resistant waterproof insulation material of the present invention has relatively low water absorption rate and a thermal conductivity factor, insulation, fire prevention,
Stability is good, there is a stronger mechanical strength, rub resistance, corrosion-resistant, and service life is longer, additionally can persistently discharge anion
And the pollutant in absorption air, reach the effect of purification air；The raw material components of the present invention are safe and reliable simultaneously, to environment
It is harmless, and raw material is easy to get, cost is relatively low, and technique is concise, with higher practical value and good application prospect.
Embodiment
With reference to specific embodiment, the technical scheme in the embodiment of the present invention is clearly and completely described, shown
So, described embodiment is only a part of embodiment of the invention, rather than whole embodiments.Based on the reality in the present invention
Example is applied, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made all belongs to
In the scope of protection of the invention.
Embodiment 1.
A kind of fire-resistant waterproof insulation material of the present embodiment, includes the raw material of following parts by weight：
25 parts of polyvinyl alcohol, 25 parts of lightweight sierozem power, 18 parts of hydroxymethyl cellulose, 7 parts of hydrophober, negative ion powder for building 12
Part, native 16 parts of the filler of mineral, 14 parts of fire retardant, 12 parts of reinforcing fibre, 15 parts of inorganic binder, 45 parts of water.
Hydrophober in the present embodiment is calcium stearate, aluminum stearate or sodium methyl silicate, compares 2 according to weight:1:1 composition
Mixture.
Negative ion powder for building in the present embodiment is tourmaline powder, neodymia, terbium peroxide compare 5 according to weight:
1:The mixture of 1 composition.
The native filler of mineral in the present embodiment is bentonite, kaolin, attapulgite according to 2:1:The mixture of 1 composition,
The bentonite, kaolin, attapulgite are calcined 1 hour in the case where temperature is 750 DEG C, are incubated 0.5 hour, are gone out after natural cooling
Material, is finally made the powder that particle mean size is below 500nm by the bentonite after calcining, kaolin, attapulgite.
Fire retardant in the present embodiment is graphite, magnesium hydroxide, aluminium hydroxide and halogenated phosphate, compares 2 according to weight:1:
2:The mixture of 1 composition.
Reinforcing fibre in the present embodiment is glass fibre, silicon nitride fiber and alumina silicate fibre according to weight ratio 3:1:2
The mixture of composition.
Inorganic binder in the present embodiment is aluminium hydroxide.
A kind of preparation method of fire-resistant waterproof insulation material of the present embodiment, comprises the following steps：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, stir 20 minutes,
Speed of agitator 300r/min, adds water, is warming up to 65 DEG C, continues to stir 25 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober are added in mixer, and rotating speed is 400 r/
Min, is stirred 25 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir 65 minutes, obtains
Mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed, will be molded in the case where hydraulic press pressure is 60MPa
Dried in feedstock module feeding baking oven afterwards, drying temperature is 120 DEG C, and drying time is 3 hours, what natural cooling was invented
Fire-resistant waterproof insulation material.
Embodiment 2.
A kind of fire-resistant waterproof insulation material of the present embodiment, includes the raw material of following parts by weight：
15 parts of polyvinyl alcohol, 12 parts of lightweight sierozem power, 8 parts of hydroxymethyl cellulose, 3 parts of hydrophober, 8 parts of negative ion powder for building,
10 parts of filler of mineral soil, 8 parts of fire retardant, 6 parts of reinforcing fibre, 7 parts of inorganic binder, 35 parts of water.
Hydrophober in the present embodiment is calcium stearate, aluminum stearate or sodium methyl silicate, compares 2 according to weight:1:1 composition
Mixture.
Negative ion powder for building in the present embodiment is tourmaline powder, neodymia, terbium peroxide compare 5 according to weight:
1:The mixture of 1 composition.
The native filler of mineral in the present embodiment is bentonite, kaolin, attapulgite according to 2:1:The mixture of 1 composition,
The bentonite, kaolin, attapulgite are calcined 1 hour in the case where temperature is 700 DEG C, are incubated 0.5 hour, are gone out after natural cooling
Material, is finally made the powder that particle mean size is below 500nm by the bentonite after calcining, kaolin, attapulgite.
Fire retardant in the present embodiment is graphite, magnesium hydroxide, aluminium hydroxide and halogenated phosphate, compares 2 according to weight:1:
2:The mixture of 1 composition.
Reinforcing fibre in the present embodiment is glass fibre, silicon nitride fiber and alumina silicate fibre according to weight ratio 3:1:2
The mixture of composition.
Inorganic binder in the present embodiment is waterglass.
A kind of preparation method of fire-resistant waterproof insulation material of the present embodiment, comprises the following steps：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, stir 10 minutes,
Speed of agitator 200r/min, adds water, is warming up to 45 DEG C, continues to stir 15 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 300r/
Min, is stirred 15 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir 45 minutes, obtains
Mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed, will be molded in the case where hydraulic press pressure is 40MPa
Dried in feedstock module feeding baking oven afterwards, drying temperature is 100 DEG C, and drying time is 1 hour, what natural cooling was invented
Fire-resistant waterproof insulation material.
Embodiment 3.
A kind of fire-resistant waterproof insulation material of the present embodiment, includes the raw material of following parts by weight：
20 parts of polyvinyl alcohol, 18 parts of lightweight sierozem power, 13 parts of hydroxymethyl cellulose, hydrophober 5,10 parts of negative ion powder for building,
13 parts of filler of mineral soil, 11 parts of fire retardant, 9 parts of reinforcing fibre, 11 parts of inorganic binder, 40 parts of water.
Hydrophober in the present embodiment is calcium stearate, aluminum stearate or sodium methyl silicate, compares 2 according to weight:1:1 composition
Mixture.
Negative ion powder for building in the present embodiment is tourmaline powder, neodymia, terbium peroxide compare 5 according to weight:
1:The mixture of 1 composition.
The native filler of mineral in the present embodiment is bentonite, kaolin, attapulgite according to 2:1:The mixture of 1 composition,
The bentonite, kaolin, attapulgite are to be calcined 1 hour in the case where temperature is 730 DEG C, 0.5 hour are incubated, after natural cooling
Discharging, is finally made the powder that particle mean size is below 500nm by the bentonite after calcining, kaolin, attapulgite.
Fire retardant in the present embodiment is graphite, magnesium hydroxide, aluminium hydroxide and halogenated phosphate, compares 2 according to weight:1:
2:The mixture of 1 composition.
Reinforcing fibre in the present embodiment is glass fibre, silicon nitride fiber and alumina silicate fibre according to weight ratio 3:1:2
The mixture of composition.
Inorganic binder in the present embodiment is zinc oxide.
A kind of preparation method of fire-resistant waterproof insulation material of the present embodiment, comprises the following steps：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, stir 15 minutes,
Speed of agitator 250r/min, adds water, is warming up to 55 DEG C, continues to stir 20 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 350r/
Min, is stirred 20 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir 55 minutes, obtains
Mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed, will be molded in the case where hydraulic press pressure is 50MPa
Dried in feedstock module feeding baking oven afterwards, drying temperature is 110 DEG C, and drying time is 2 hours, what natural cooling was invented
Fire-resistant waterproof insulation material.
The performance test results of the fire-resistant waterproof insulation material prepared in various embodiments above are as follows：
| Thermal conductivity factor W/（m·k） | Water absorption rate % | Fire protecting performance | Anion-generating capacity/cm3 | |
| Embodiment 1 | 0.024 | 2.4 | B1 | 654 |
| Embodiment 2 | 0.031 | 1.8 | B1 | 635 |
| Embodiment 3 | 0.029 | 2.1 | B1 | 641 |
| Comparative example | 0.078 | 3 | B2 | 525 |
A kind of fire-resistant waterproof insulation material of the present invention its there is relatively low water absorption rate and thermal conductivity factor, insulation, fire prevention, stability
It is good, there is a stronger mechanical strength, rub resistance, corrosion-resistant, service life is longer, additionally can persistently discharge anion and suction
The pollutant in air is received, the effect of purification air is reached；The raw material components of the present invention are safe and reliable simultaneously, environmental sound,
And raw material is easy to get, cost is relatively low, and technique is concise, with higher practical value and good application prospect.
It is obvious to a person skilled in the art that the invention is not restricted to the details of above-mentioned one exemplary embodiment, Er Qie
In the case of without departing substantially from spirit or essential attributes of the invention, the present invention can be realized in other specific forms.Therefore, no matter
From the point of view of which point, embodiment all should be regarded as exemplary, and be nonrestrictive, the scope of the present invention is by appended power
Profit is required rather than described above is limited, it is intended that all in the implication and scope of the equivalency of claim by falling
Change is included in the present invention.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical scheme, this narrating mode of specification is only that for clarity, those skilled in the art should
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It may be appreciated other embodiment.
Claims (10)
1. a kind of fire-resistant waterproof insulation material, it is characterised in that include the raw material of following parts by weight：
It is 15-25 parts of polyvinyl alcohol, 12-25 parts of lightweight sierozem power, 8-18 parts of hydroxymethyl cellulose, 3-7 parts of hydrophober, for building
Native 10-16 parts of the filler of 8-12 parts of negative ion powder, mineral, 8-14 parts of fire retardant, 6-12 parts of reinforcing fibre, inorganic binder 7-15
Part, 35-45 parts of water.
2. a kind of fire-resistant waterproof insulation material according to claim 1, it is characterised in that the fire-resistant waterproof insulation material
Include the raw material of following parts by weight：
20 parts of polyvinyl alcohol, 18 parts of lightweight sierozem power, 13 parts of hydroxymethyl cellulose, hydrophober 5,10 parts of negative ion powder for building,
13 parts of filler of mineral soil, 11 parts of fire retardant, 9 parts of reinforcing fibre, 11 parts of inorganic binder, 40 parts of water.
3. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the hydrophober is tristearin
Sour calcium, aluminum stearate or sodium methyl silicate, compare 2 according to weight:1:The mixture of 1 composition.
4. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the anion for building
Powder is tourmaline powder, neodymia, terbium peroxide compare 5 according to weight:1:The mixture of 1 composition.
5. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the native filler of the mineral is
Bentonite, kaolin, attapulgite are according to 2:1:The mixture of 1 composition, the bentonite, kaolin, attapulgite are in temperature
Spend to calcine 1 hour at 700-750 DEG C, be incubated 0.5 hour, discharged after natural cooling, finally by the bentonite after calcining, kaolinite
The powder that particle mean size is below 500nm is made in soil, attapulgite.
6. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the fire retardant be graphite,
Magnesium hydroxide, aluminium hydroxide and halogenated phosphate, compare 2 according to weight:1:2:The mixture of 1 composition.
7. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the reinforcing fibre is glass
Glass fiber, silicon nitride fiber and alumina silicate fibre are according to weight ratio 3:1:The mixture of 2 compositions.
8. a kind of fire-resistant waterproof insulation material according to claim 1 or 2, it is characterised in that the inorganic binder is
One kind in waterglass, aluminium hydroxide or zinc oxide.
9. a kind of method for preparing fire-resistant waterproof insulation material as claimed in claim 1 or 2, it is characterised in that including following
Step：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, 10-20 points of stirring
Clock, speed of agitator 200-300r/min, adds water, is warming up to 45-65 DEG C, continues to stir 15-25 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 300-
400 r/min, are stirred 15-25 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir
45-65 minutes, obtain mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed in the case where hydraulic press pressure is 40-60MPa, will
Dried in feedstock module feeding baking oven after shaping, drying temperature is 100-120 DEG C, and drying time is 1-3 hours, naturally cold
But, the fire-resistant waterproof insulation material invented.
10. a kind of preparation method of fire-resistant waterproof insulation material according to claim 9, it is characterised in that the step
For：
Step one, weigh on request and prepare each component raw material；
Step 2, lightweight sierozem power, negative ion powder for building, the native filler of mineral are mixed and added in mixer, stir 15 minutes,
Speed of agitator 250r/min, adds water, is warming up to 55 DEG C, continues to stir 20 minutes, obtains mixture A；
Step 3, polyvinyl alcohol, carboxymethyl cellulose, inorganic binder, hydrophober is added in mixer, rotating speed is 350r/
Min, is stirred 20 minutes, mixture A, fire retardant, reinforcing fibre made from step 2 are added, continues to stir 55 minutes, obtains
Mixture B；
Step 4, mixture B made from step is imported in mould, is press-formed, will be molded in the case where hydraulic press pressure is 50MPa
Dried in feedstock module feeding baking oven afterwards, drying temperature is 110 DEG C, and drying time is 2 hours, and natural cooling is invented
Fire-resistant waterproof insulation material.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710429336.3A CN107188469A (en) | 2017-06-08 | 2017-06-08 | A kind of fire-resistant waterproof insulation material and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710429336.3A CN107188469A (en) | 2017-06-08 | 2017-06-08 | A kind of fire-resistant waterproof insulation material and preparation method thereof |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107188469A true CN107188469A (en) | 2017-09-22 |
Family
ID=59876210
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710429336.3A Withdrawn CN107188469A (en) | 2017-06-08 | 2017-06-08 | A kind of fire-resistant waterproof insulation material and preparation method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107188469A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108249882A (en) * | 2018-03-29 | 2018-07-06 | 合肥聪亨新型建材科技有限公司 | A kind of new modified graphite external-wall heat-insulation material and preparation method thereof |
| CN108824070A (en) * | 2018-06-01 | 2018-11-16 | 合肥昂诺新材料有限公司 | A kind of cover paper and preparation method thereof with fire protection flame retarding function |
| CN111363426A (en) * | 2020-05-11 | 2020-07-03 | 江西清大高端技术服务有限公司 | Efficient and environment-friendly negative oxygen ion concentrated solution and preparation method thereof |
| CN112830718A (en) * | 2021-01-19 | 2021-05-25 | 浙江雅炻科技有限公司 | Fireproof flame-retardant plate and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104529293A (en) * | 2014-12-20 | 2015-04-22 | 魏超产 | Waterproof heat insulation environment-friendly mortar and preparation method thereof |
| CN105174897A (en) * | 2015-09-18 | 2015-12-23 | 广西路佳道桥勘察设计有限公司 | Flame-retardant external wall thermal insulation material and preparation method thereof |
| CN105384411A (en) * | 2015-12-11 | 2016-03-09 | 徐琪 | Preparation method of functional mortar capable of releasing negative ions |
-
2017
- 2017-06-08 CN CN201710429336.3A patent/CN107188469A/en not_active Withdrawn
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104529293A (en) * | 2014-12-20 | 2015-04-22 | 魏超产 | Waterproof heat insulation environment-friendly mortar and preparation method thereof |
| CN105174897A (en) * | 2015-09-18 | 2015-12-23 | 广西路佳道桥勘察设计有限公司 | Flame-retardant external wall thermal insulation material and preparation method thereof |
| CN105384411A (en) * | 2015-12-11 | 2016-03-09 | 徐琪 | Preparation method of functional mortar capable of releasing negative ions |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108249882A (en) * | 2018-03-29 | 2018-07-06 | 合肥聪亨新型建材科技有限公司 | A kind of new modified graphite external-wall heat-insulation material and preparation method thereof |
| CN108824070A (en) * | 2018-06-01 | 2018-11-16 | 合肥昂诺新材料有限公司 | A kind of cover paper and preparation method thereof with fire protection flame retarding function |
| CN111363426A (en) * | 2020-05-11 | 2020-07-03 | 江西清大高端技术服务有限公司 | Efficient and environment-friendly negative oxygen ion concentrated solution and preparation method thereof |
| CN111363426B (en) * | 2020-05-11 | 2022-03-04 | 江西清大高端技术服务有限公司 | Environment-friendly negative oxygen ion concentrated solution and preparation method thereof |
| CN112830718A (en) * | 2021-01-19 | 2021-05-25 | 浙江雅炻科技有限公司 | Fireproof flame-retardant plate and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103723993B (en) | A kind of body of wall thermal insulation fire-proof insulation material | |
| CN107162519A (en) | A kind of wall fire-retardant heat-insulation material and preparation method thereof | |
| CN102795826B (en) | Aerogel/inorganic lightweight aggregate composite thermal insulation material and preparation method thereof | |
| CN106518155B (en) | Geopolymer base thermal insulation mortar with waterproof fireproofing function | |
| CN107188469A (en) | A kind of fire-resistant waterproof insulation material and preparation method thereof | |
| CN102219415B (en) | Light sand without burning and preparation method thereof | |
| CN103588458A (en) | Low-density waterproof impervious autoclaved aerated concrete heat-insulation plate | |
| CN106565274A (en) | Fiber enhanced ceramsite foamed concrete and preparation method thereof | |
| CN103317789B (en) | Thick-plaster fireproof mortar phenolic resin plate and phenolic aldehyde special-purpose fireproof mortar | |
| CN107032716A (en) | A kind of light flame-retardant heat preservation energy-saving construction material and preparation method thereof | |
| CN105541313A (en) | Nano heat-insulating material and preparation method of nano heat-insulating board | |
| CN101172832A (en) | Light high-strength unburned brick | |
| CN103524106B (en) | A kind of fireproof heat insulation plate of outer wall and its production method | |
| CN107915953A (en) | A kind of flat plate collector compound insulating material and preparation method thereof | |
| CN107056226A (en) | A kind of preparation method of heat insulating material | |
| CN107337429B (en) | Preparation method of ceramic curtain wall and foamed ceramic composite material | |
| CN108275921A (en) | A kind of adiabatic heat-insulation wall material and preparation method thereof | |
| CN105924120B (en) | A kind of water proof anti-seepage phase-change energy-storage gypsum building block and preparation method thereof | |
| CN101538142A (en) | Phosphate heat preservation mortar for outer wall of buildings | |
| CN102731024B (en) | A thermal-insulation fireproof insulation board | |
| CN108585712A (en) | The preparation method of large dosage solid waste wet-milled slurry composite scrap EPS granule insulating materials | |
| KR100957674B1 (en) | Lightweight composite material for construction | |
| CN108947451A (en) | A kind of Novel wall body heat insulation material and preparation method thereof | |
| CN108341682A (en) | A kind of heat-insulating heat-preserving material and preparation method thereof | |
| CN104446331B (en) | The preparation method of aluminum phosphate-expanded graphite-alumina-silicate ceramic fibre heat-insulating and fire-proof matrix material |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170922 |
|
| WW01 | Invention patent application withdrawn after publication |