CN107184517A - One kind shield hair composition and preparation method thereof - Google Patents
One kind shield hair composition and preparation method thereof Download PDFInfo
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- CN107184517A CN107184517A CN201710411994.XA CN201710411994A CN107184517A CN 107184517 A CN107184517 A CN 107184517A CN 201710411994 A CN201710411994 A CN 201710411994A CN 107184517 A CN107184517 A CN 107184517A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q5/00—Preparations for care of the hair
- A61Q5/12—Preparations containing hair conditioners
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/59—Mixtures
- A61K2800/592—Mixtures of compounds complementing their respective functions
- A61K2800/5922—At least two compounds being classified in the same subclass of A61K8/18
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Abstract
The invention provides one kind shield hair composition and preparation method thereof, the functional component of the shield hair composition is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, 2 10 parts of 15 parts of the Semen sesami nigrum dregs of rice, 13 parts of rye, 13 parts of black rice, 3 10 parts of the black soya bean dregs of rice and the fleece-flower root based on its parts by weight, prepared by hybrid mode；The shield hair composition, each component synergy has effect of hair nourishing, submissive hair, lifting hair gloss and elasticity concurrently；Its preparation method is simple, the need for being adapted to scale industrial production.
Description
Technical field
The present invention relates to a kind of hair products and preparation method thereof, especially a kind of shield hair composition and its preparation side
Method.
Background technology
Hair nursing technology is a kind of wide variety of technology in China's cosmetic field.In recent years, with cosmetics circle
Natural plant product is advocated, the correlative study using plant essence nursing hair, conditioning skin is also more and more.
Hair is the accessory organ of skin, stretches the hair outside skin and claims hair shaft, the long title hair root in skin.Hair root bag
In the hair follicle being made up of skin and connective tissue.All cell proliferations of hair and development and differentiation occur under skin surface
In hair follicle, once growing skin surface, most of metabolic activity has stopped, and is completely exposed to the external world, so as to keep physics complete
It is whole.Hair shaft is interior or endogenic repair process seldom occurs for surface.By taking hair as an example, though hair does not have to individual survival to pass
Important evolution effect, but when being grown in hair from the beginning skin, it more or less can produce influence to individual itself.Hair can
Pre- uv blocking, and in many species, hair (or fur) can provide heat-blocking action.In addition, although the hair style of people can occur
Change, but some social class crowds seem length hair in always thirsting for, and it is desirable that hair can flexible and gloss.So
And, hair can undergo the extensive infringement of environment, mainly UV irradiation, daily cleaning and with hair-dryer dry up caused by low humidity damage
Wound, various hairdressings and " anti-aging " treatment damage as caused by decolourizing, dye, persistently perm, stretch etc..Because hair can not be very
Protect oneself well, can not self-regeneration, be highly desirable to provide these nursing roles with product used in everyday.
Therefore, exploitation has the plant extraction elite of total care function to hair and skin, for cosmetics new product
Research and development are significant.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of shield hair composition.
Another technical problem to be solved by this invention is the preparation method for providing above-mentioned shield hair composition.
In order to solve the above technical problems, the technical scheme is that：
One kind shield hair composition, functional component is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, by it
2-10 parts of 1-5 parts of the parts by weight meter Semen sesami nigrum dregs of rice, 1-3 parts of rye, 1-3 parts of black rice, 3-10 parts of the black soya bean dregs of rice and the fleece-flower root.
It is preferred that, above-mentioned shield hair composition is prepared by following methods：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then with 10%
Salt acid for adjusting pH value adds 0.2-1kg composite plant hydrolases and dissolved to 3-5, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its quality percentage in the solution
Concentration is 0.3-0.5%, and in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation is by alkali protease, neutral protein
Enzyme and papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-
5：1-3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Detection water-soluble protein content >=60% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
It is preferred that, above-mentioned shield hair composition, 4 parts of the Semen sesami nigrum dregs of rice, 1 part of rye, 2 parts of black rice, black based on its parts by weight
4 parts of 6 parts of dregs of beans and the fleece-flower root.
The preparation method of above-mentioned shield hair composition, specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then with 10%
Salt acid for adjusting pH value adds 0.2-1kg composite plant hydrolases and dissolved to 3-5, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its quality percentage in the solution
Concentration is 0.3-0.5%, and in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation is by alkali protease, neutral protein
Enzyme and papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-
5：1-3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
It is preferred that, the preparation method of above-mentioned shield hair composition, step (3) the neutral and alkali protease, neutral proteinase
Weight ratio with papain is 4：3：1.
Above-mentioned shield hair composition is used in mixed way with commercial shampoos.
The beneficial effects of the invention are as follows：
Above-mentioned shield hair composition, each component synergy, have concurrently hair nourishings, submissive hair, lifted hair gloss and
Effect of elasticity；Its preparation method is simple, the need for being adapted to scale industrial production.
Embodiment
Technical scheme of the present invention is further described with reference to specific embodiment.
Embodiment 1
One kind shield hair composition, functional component is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 4kg, rye 1kg, black rice 2kg, black soya bean dregs of rice 6kg and fleece-flower root 4kg.
Detection water-soluble protein content 67% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
The preparation method of above-mentioned shield hair composition, specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 45 DEG C of water of 80kg in a kettle., then adjusted with 10% hydrochloric acid
PH value adds 0.2-1kg composite plant hydrolases and dissolved to 4,4 hours reaction time；
(3) pH value is adjusted to 7 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.4%, hydrolyzed 6 hours in temperature 45 C；The complex enzyme formulation is by alkali protease, neutral proteinase and papain
Compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 4：3：1；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Embodiment 2
One kind shield hair composition, functional component is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 5kg, rye 1kg, black rice 1kg, black soya bean dregs of rice 3kg and fleece-flower root 10kg.
Detection water-soluble protein content 63% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
The preparation method of above-mentioned shield hair composition, specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 40 DEG C of water of 100kg in a kettle., then adjusted with 10% hydrochloric acid
PH value is saved to 5,1kg composite plant hydrolases is added and is dissolved, 3 hours reaction time；
(3) adjust pH value to 8.5 with sodium hydroxide solution, add complex enzyme formulation, make its in the solution quality percentage it is dense
Spend for 0.5%, hydrolyzed 5 hours in temperature 50 C；The complex enzyme formulation is by alkali protease, neutral proteinase and Papain
Enzyme compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1：1：1；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Embodiment 3
One kind shield hair composition, functional component is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 1kg, rye 3kg, black rice 3kg, black soya bean dregs of rice 10kg and fleece-flower root 2kg.
Detection water-soluble protein content 61% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
The preparation method of above-mentioned shield hair composition, specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 55 DEG C of water of 50kg in a kettle., then adjusted with 10% hydrochloric acid
PH value adds 0.2-1kg composite plant hydrolases and dissolved to 3,8 hours reaction time；
(3) pH value is adjusted to 7 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.3%, in temperature, 35 DEG C hydrolyze 12 hours；The complex enzyme formulation is by alkali protease, neutral proteinase and Papain
Enzyme compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 5：5：3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
Embodiment 4
One kind shield hair composition, functional component is made up of the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root, its
In, Semen sesami nigrum dregs of rice 4kg, rye 2kg, black rice 2kg, black soya bean dregs of rice 7kg and fleece-flower root 5kg.
Detection water-soluble protein content 65% (being performed by GB/T5511 appendix As) is carried out to above-mentioned resulting composition.
The preparation method of above-mentioned shield hair composition, specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicine
Material powder, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 45 DEG C of water of 80kg in a kettle., then adjusted with 10% hydrochloric acid
PH value adds 0.8kg composite plant hydrolases and dissolved to 4,6 hours reaction time；
(3) pH value is adjusted to 8 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.4%, in temperature, 40 DEG C hydrolyze 10 hours；The complex enzyme formulation is by alkali protease, neutral proteinase and Papain
Enzyme compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 4：3：2；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT is used after collecting supernatant, concentration, goes out wind-warm syndrome
95 DEG C of degree, homogenization pressure 30MPa is spray-dried, and is produced.
One of the embodiment 1-4 each components are commercially available prod, wherein, Novi of composite plant hydrolase purchase Denmark letter
(China) Investment Co., Ltd, enzyme activity is 100FGB/g；Alkali protease is purchased from lucky precious (Qingdao) bio tech ltd,
Its activity is 18000U/ml, and neutral proteinase is purchased from Beijing east prosperous and powerful Bioisystech Co., Ltd of China, its activity
20000U/ml；Papain is purchased from Zhengzhou De Xin chemical industry Industrial Co., Ltd., and its activity is 16000U/ml.Each component is used
Amount is increased or decreased according to same ratio, and the parts by weight relation of gained each component belongs to protection scope of the present invention.
Using effect is tested：
The gained of embodiment 1 shield hair composition and commercial shampoos are used in mixed way with (10% shield hair composition dilution water
Solution collocation 50ml commercial shampoos), carrying out using effect experiment, (the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice, the fleece-flower root are by weight
Amount compares 4:1:2:6:4 compoundings), wherein,
Contrast groups, using commercial shampoos.
Example 1, using formula with reference to embodiment 1, with rye, black rice, the fleece-flower root by weight 1：2：4 compoundings replace hair care
It is used in mixed way with composition and commercial shampoos (ratio be the same as Example 1), water-soluble protein content is 47% (by GB/T5511
Appendix A is performed).
Example 2, using formula with reference to embodiment 1, with the Semen sesami nigrum dregs of rice, the black soya bean dregs of rice, the fleece-flower root by weight 4：6：4 compounding generations
It is used in mixed way (ratio be the same as Example 1) for shield hair composition and commercial shampoos, water-soluble protein content (is pressed for 55%
GB/T5511 appendix As are performed).
Example 3, using formula with reference to embodiment 1, with the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice by weight 4：1：2：6
Compounding replaces shield hair composition and commercial shampoos to be used in mixed way (ratio be the same as Example 1), and water-soluble protein content is
65% (being performed by GB/T5511 appendix As).
About 100 subjects, have participated in 2 weeks use researchs by a definite date.When research starts, the hair for recording all subjects is equal
For drying, fragility, not submissive and " wanting help ".100 subjects are divided into 5 groups, and 20 people/group use above-mentioned compounding in every 4 days
Shampoo rinse hair, is during which had one's hair wash to subject and daily nursing is instructed, and laboratory is returned to after 12 days.Subject is sent out
Matter is estimated, and the results are shown in Table 1.
Table 1
The evaluation method of above-mentioned every detection parameter is as follows：
All parameters are evaluated according to 0 to 10 points, 10 points represent most probable situation.
1st, the aqueous weight testing method of hair
Use instrument：Sensitivity is 0.01mg electronic balances；Constant temperature and humidity incubator.
Topknot sample：5cm length, example weight 5g
Experimentation：Hair swatch is placed in room temperature, the constant temperature and humidity incubators of relative humidity ＜ 5% through combing rear overhang, is put
Put and taken out after 2 hours, weigh hair weight.The constant temperature and humidity culture between room temperature, relative humidity 40%-50% is suspended in again
In case, taken out after placing 2 hours, weigh hair weight.The difference divided by example weight of weight are hair water content twice.
2nd, hair intensity and elastomeric check method
Use instrument：Hair tensile strength detector
Topknot sample：20cm length
Experimentation：Using hair tensile strength detector, the fracture strength of hair is measured.Using linear variable power/away from
Hair elongation during increase strength is recorded from sensor.Hair extends, until fracture.The fracture strength of traction is typically smaller than
100 grams.Tractive force is with about 3 grams per second of speed increase.Coefficient of elasticity can be calculated according to these measurements.For comparing hair
Elasticity.With hair normal diameter, 70 μm all ultimate strength values are normalized.Detect individual's with standard microscopy
Hair diameter, calculates hairs break intensity level, for comparing hair intensity.
3rd, hair gloss is measured
Use instrument：Measurement of luster instrument
Topknot sample：Topknot length 20cm, weight 7.5g topknot
Experimentation：In the black box that hair is placed in measurement of luster instrument, Hair setting is allowed to comb equably to arrange
Into the straight line that width is 2.5cm.Using measurement of luster instrument, it is measured according to BNT gloss formula.
LBNT=gloss number
SinIntegrated in=reflectance curves in reflection peak
SoutPeak both wings are integrated in=reflectance curves
Integrated in D=diffusion curve maps
Wvisual=the average value by true picture along area-of-interest bandwidth
4th, hair drying comb rationality and wet hair comb rationality
Use instrument：Tensiometer；Constant temperature and humidity incubator
Topknot sample：Topknot length 50cm, weight 16g
Experimentation：
(1) hair drying comb rationality, topknot is placed in the constant temperature and humidity incubator of room temperature, relative humidity less than 5% 2 hours,
Take out and determine hair drying comb rationality.
(2) wet hair comb rationality, topknot is placed in the constant temperature and humidity incubator of room temperature, relative humidity more than 95% 2 hours,
Take out and determine wet hair comb rationality.
Tension tester is a kind of tester dedicated for Hair setting performance evaluation, passes through a standard comb mould
Apery combing hair is acted, and wisp of hair is combed and recorded by terminal.Sent out during test with 300mm/min speed tensile
Beam, displacement 200mm, the load value (unit that fetch bit is moved between 100-200mm：Gf) evaluated.
5th, compliance sensory evaluation standard
10 points, without tangling phenomenon, easily comb, no combing resistance hair soft such as silk, very smooth；
9 points, without obvious tangling phenomenon, easily comb, and slightly sense combs resistance hair soft, and smooth feeling is preferable；
7 separately begin slightly has tangling phenomenon when combing, and easily combs later, slightly combs resistance hair soft, there is certain smooth
Sense；
5 separately begin has tangling phenomenon when combing, and is easier to comb later, has certain resistance hair that combs relatively soft, smooth feeling
It is unobvious；
3 points have stronger tangling phenomenon when combing, and are difficult to comb later, have stronger combing resistance hair harder, not smooth；
There is very strong tangling phenomenon during 1 point of combing, hardly possible is combed, there is very strong combing resistance hair coarse, it is very hard and dry.
Subject uses shield hair composition of the present invention it can be seen from upper table 1, to hair water content, poppet
Luminous pool, elastic hair, wet hair comb rationality, hair drying comb rationality, hair compliance have clear improvement.
The above-mentioned detailed description carried out with reference to embodiment to a kind of shield hair composition and preparation method thereof, is illustrative
Rather than it is limited, several embodiments can be included according to limited scope, therefore do not departing from overall structure of the invention
Changing and modifications under thinking, should belong within protection scope of the present invention.
Claims (5)
1. one kind shield hair composition, it is characterised in that：Functional component is by the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root
Composition, 1-5 parts of the Semen sesami nigrum dregs of rice, 1-3 parts of rye, 1-3 parts of black rice, 3-10 parts of the black soya bean dregs of rice and fleece-flower root 2-10 based on its parts by weight
Part.
2. shield hair composition according to claim 1, it is characterised in that：Prepared by following methods：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicinal material powder
End, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then use 10% hydrochloric acid
PH value is adjusted to 3-5,0.2-1kg composite plant hydrolases is added and is dissolved, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.3-0.5%, in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation by alkali protease, neutral proteinase and
Papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-5：1-
3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT, leaving air temp 95 are used after collecting supernatant, concentration
DEG C, homogenization pressure 30MPa is spray-dried, and is produced.
3. shield hair composition according to claim 1, it is characterised in that：4 parts of the Semen sesami nigrum dregs of rice, black based on its parts by weight
4 parts of 1 part of wheat, 2 parts of black rice, 6 parts of the black soya bean dregs of rice and the fleece-flower root.
4. the preparation method of hair composition is protected described in claim 1, it is characterised in that：Specific preparation process is as follows：
(1) take the Semen sesami nigrum dregs of rice, rye, black rice, the black soya bean dregs of rice and the fleece-flower root to be crushed respectively for raw material and cross 200 mesh sieves and obtain medicinal material powder
End, is weighed by prescription amount and is well mixed each medicinal powder；
(2) press and mixed per 10kg mixing medicinal powder with 50-100kg 40-55 DEG C water in a kettle., then use 10% hydrochloric acid
PH value is adjusted to 3-5,0.2-1kg composite plant hydrolases is added and is dissolved, reaction time 3-8 hour；
(3) pH value is adjusted to 7-8.5 with sodium hydroxide solution, add complex enzyme formulation, make its mass percentage concentration in the solution
For 0.3-0.5%, in temperature, 35-50 DEG C hydrolyzes 5-12 hours；The complex enzyme formulation by alkali protease, neutral proteinase and
Papain compounding composition, the weight ratio of the alkali protease, neutral proteinase and papain is 1-5：1-5：1-
3；
(4) enzyme-deactivating, filtering, centrifugal treating are carried out, 175 DEG C of EAT, leaving air temp 95 are used after collecting supernatant, concentration
DEG C, homogenization pressure 30MPa is spray-dried, and is produced.
5. the preparation method of hair composition is protected according to claim 4, it is characterised in that：Step (3) the neutral and alkali egg
The weight ratio of white enzyme, neutral proteinase and papain is 4：3：1.
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| CN102424625A (en) * | 2011-08-30 | 2012-04-25 | 大连百祥聚生物科技有限公司 | Edible and medical fungi blackening agent, its preparation method and application |
| WO2016171464A1 (en) * | 2015-04-20 | 2016-10-27 | (주)이지희컴퍼니 | Composition for scalp and hair, containing green tea water |
| CN106616306A (en) * | 2017-02-10 | 2017-05-10 | 江西谷物源食品有限公司 | Instant hair blackening cereal staple food material and making method thereof |
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101019816A (en) * | 2006-02-16 | 2007-08-22 | 茹国军 | Prepn process of hair blackening shampoo |
| CN101721634A (en) * | 2009-12-15 | 2010-06-09 | 王洪亮 | Black corn extraction liquid |
| CN102424625A (en) * | 2011-08-30 | 2012-04-25 | 大连百祥聚生物科技有限公司 | Edible and medical fungi blackening agent, its preparation method and application |
| WO2016171464A1 (en) * | 2015-04-20 | 2016-10-27 | (주)이지희컴퍼니 | Composition for scalp and hair, containing green tea water |
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