CN107184439A - A kind of skin care compositions with crease-resistant effect and preparation method and application - Google Patents

A kind of skin care compositions with crease-resistant effect and preparation method and application Download PDF

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Publication number
CN107184439A
CN107184439A CN201710449778.4A CN201710449778A CN107184439A CN 107184439 A CN107184439 A CN 107184439A CN 201710449778 A CN201710449778 A CN 201710449778A CN 107184439 A CN107184439 A CN 107184439A
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Prior art keywords
parts
oil
crease
resistant effect
care compositions
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CN201710449778.4A
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Inventor
林竹
陈萍
梁园园
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YUMEIJING GROUP CO Ltd TIANJIN
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YUMEIJING GROUP CO Ltd TIANJIN
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Priority to CN201710449778.4A priority Critical patent/CN107184439A/en
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00Cosmetics or similar toiletry preparations
    • A61K8/18Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/37Esters of carboxylic acids
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61QSPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00Preparations for care of the skin
    • A61Q19/08Anti-ageing preparations

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  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Public Health (AREA)
  • Animal Behavior & Ethology (AREA)
  • General Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Birds (AREA)
  • Epidemiology (AREA)
  • Dermatology (AREA)
  • Gerontology & Geriatric Medicine (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Emergency Medicine (AREA)
  • Cosmetics (AREA)

Abstract

The invention provides a kind of skin care compositions with crease-resistant effect and preparation method and application, the functional component of the skin care compositions is made up of apple seed oil, olive oil, apricot kernel oil and propylgallate, 36 parts of apple seed oil, 5 20 parts of olive oil, 3 15 parts of apricot kernel oil, 0.1 5 parts of propylgallate are calculated as by its parts by weight, obtained by hybrid mode, with significant crease-resistant effect.

Description

A kind of skin care compositions with crease-resistant effect and preparation method and application
Technical field
The present invention relates to skin care field, especially a kind of skin care compositions with crease-resistant effect and preparation method thereof with Using.
Background technology
In recent years, advocating with cosmetics bound pair natural plant product, utilizes the phase of plant extraction elite nursing skin Close research also more and more.
Skin is made up of epidermis, corium and hypodermis three parts.Epidermis is direct and extraneous contact part And be the part for having most deep relation with cosmetics.Epidermal thickness is only 0.2mm, is to be piled up to constitute by horn cell 's.On the inside of skin, epidermis can be divided into basalis, spinosity layer, stratum granulosum and cuticula again.The metabolism of skin is Constantly divided by the horn cell of basalis, about 28 day cycle was one bout.Cuticula, which has, keeps moisture Function and prevent skin internal moisture volatilize and the immersion of extraneous foreign matter barrier function, NMF in cuticula, A large amount of reductions of intercellular lipid, sodium hyaluronate, skin just occur it is dry, coarse, decortication a series of problems, such as.In addition, in base Bottom there are the melanocyte for producing Mai Laning, and it has by Mai Laning come the defensive enginery to ultraviolet.
The loads such as growth and ultraviolet, drying due to age, the load water dispenser of epidermis be able to will decline with barrier function, Spot and freckle can be produced from the melanocyte activated, the division of horn cell and the reduction of metabolic capability are all to cause skin The reason for there is wrinkle and causes aging in skin.
Exploitation has the plant extraction elite of total care function to skin, for keeping skin health, for cosmetics The research and development of new product are significant.
The content of the invention
The technical problems to be solved by the invention are to provide a kind of skin care compositions with crease-resistant effect.
Another technical problem to be solved by this invention is the system for providing the above-mentioned skin care compositions with crease-resistant effect Preparation Method.
Another technical problem to be solved by this invention is to provide answering for the above-mentioned skin care compositions with crease-resistant effect With.
In order to solve the above technical problems, the technical scheme is that:
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil and nutgall Propyl propionate is constituted, and 3-6 parts of apple seed oil, 5-20 parts of olive oil, 3-15 parts of apricot kernel oil, gallic acid third are calculated as by its parts by weight 0.1-5 parts of ester.
It is preferred that, the above-mentioned skin care compositions with crease-resistant effect, functional component is calculated as apple seed oil by its parts by weight 3-6 parts, 7-10 parts of olive oil, 10-12 parts of apricot kernel oil, 3-4 parts of propylgallate.
It is preferred that, the above-mentioned skin care compositions with crease-resistant effect, functional component is calculated as apple seed oil 5 by its parts by weight Part, 8 parts of olive oil, 11 parts of apricot kernel oil, 4 parts of propylgallate.
It is preferred that, the above-mentioned skin care compositions with crease-resistant effect, in addition to parts by weight are different for 10-60 parts of palmitic acid Monooctyl ester is used as oil-based solvent.
The preparation method of the above-mentioned skin care compositions with crease-resistant effect, specific preparation process is as follows:
(1) to weigh apple seed oil, olive oil, apricot kernel oil, propylgallate by prescription amount standby;
(2) apple seed oil, olive oil, apricot kernel oil and propylgallate are well mixed, produced.
It is preferred that, the preparation method of the above-mentioned skin care compositions with crease-resistant effect, by batch mixing from prescription amount to step (2) In simultaneously add isobutyl palmitate.
Application of the above-mentioned skin care compositions with crease-resistant effect in terms of the cosmetics with crease-resistant effect are prepared.
A kind of anti-wrinkle cosmetic is skin-care cosmetics or cleans class cosmetics, above-mentioned with anti-containing effective dose The skin care compositions of effect of wrinkling.
It is preferred that, above-mentioned anti-wrinkle cosmetic, the skin-care cosmetics are toner, emulsion or cream.
It is preferred that, above-mentioned anti-wrinkle cosmetic, the cleaning class cosmetics are mildy wash, cleansing cream, shampoo or shower cream.
Skin care compositions of the present invention with crease-resistant effect can mutually be added in cosmetics as addition, other groups The selection divided can be carried out according to the routine operation in this area, for example, may include some conventional oil phases and aqueous phase, Huo Zhejin One step includes other addition phases commonly used in art.In some emulsified make-ups, emulsifying agent, excipient are generally included (thickening) agent, can also add basic material and necessary additive that cosmetics are usually contained, such as emollient (such as plant Oil, white oil, animal fat and its derivative etc.), NMF (such as glycerine, propane diols, 1,3 butylene glycol), essence, go from Sub- water, antioxidant, preservative etc., can also add some nutritional ingredients, and the application of these specific compositions and consumption can be according to institutes State the specific species of cosmetics and selected, or added according to convention amount, this is for a person skilled in the art It is easy to what is grasped.
, can be according to conventional production process, in addition addition phase, by of the present invention with crease-resistant in specific production The skin care compositions of effect is added to the change such as cream, emulsion, mildy wash, cleansing cream, shampoo, toner or firming lotion, bath agent In cosmetic, the structure of product will not be damaged, the stability to cosmetics will not bring detrimental effect, will not cause change The quality problems such as color, layering.Specifically, first make oil phase and the aqueous phase progress of cosmetic material primary emulsifying, adjust the emulsification The temperature of system adds the skin care compositions with crease-resistant effect when less than 50 DEG C, and system is agitated uniform, further After cooling operation is completed according to recipe requirements.
The beneficial effects of the invention are as follows:
The above-mentioned skin care compositions with crease-resistant effect, prescription analysis are as follows:
Apple seed extract, reduces for hormonal in ageing processes of skin, plays a part of substitute.
Olive oil contains abundant Cleupin, flavones isoreactivity composition, is effectively strengthened by improving collagen synthesis Skin collagen network structure;The unrighted acid and propylgallate enriched in olive elite provides anti-oxidant protect Shield, natural oil forms elastic moisture film.
Apricot kernel oil is effectively reduced moisture loss, promotes absorption of the skin to moisture, maintain skin tender with it is elastic, reach Skin care, effect of tender skin.
Propylgallate has antioxidation.
It can be seen that, the above-mentioned skin care compositions each component synergy with crease-resistant effect can be done directly on human body skin Surface, because the generation of skin aging and wrinkle is relevant with hormonal decline, hormone act on ECM molecules (collagen, Fibronectin) synthesis, these albumen constitute dermatoglyph, and composition of the present invention has effectively filled up skin He Er The reduction part of illiteracy, strengthens the prolonged water holding capacity of skin, helps balance skin water oil condition, reduces wrinkle, makes skin white Fair-skinned water is tender and high resilience;Its preparation method is simple, the need for being adapted to scale industrial production.
Embodiment
Technical scheme of the present invention is further described with reference to specific embodiment, it is used in following embodiments Component is commercially available prod, and each component consumption is increased or decreased according to same ratio, the parts by weight relation of gained each component Belong to protection scope of the present invention.
Embodiment 1
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil, nutgall Propyl propionate and isobutyl palmitate (oil-based solvent) composition, wherein, apple seed oil 5kg, olive oil 8kg, no apricot kernel oil 11kg, food Sub- propyl propionate 4kg, isobutyl palmitate 40kg.
The preparation method of the above-mentioned skin care compositions with crease-resistant effect, specific preparation process is as follows:
(1) to weigh apple seed oil, olive oil, apricot kernel oil, propylgallate, isobutyl palmitate by prescription amount standby;
(2) apple seed oil, olive oil, apricot kernel oil, propylgallate and isobutyl palmitate are well mixed, i.e., .
Embodiment 2
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil, nutgall Propyl propionate and isobutyl palmitate (oil-based solvent) composition, wherein, apple seed oil 6kg, olive oil 20kg, no apricot kernel oil 3kg, food Sub- propyl propionate 0.1kg, isobutyl palmitate 10kg.
Preparation method be the same as Example 1.
Embodiment 3
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil, nutgall Propyl propionate and isobutyl palmitate (oil-based solvent) composition, wherein, apple seed oil 3kg, olive oil 5kg, no apricot kernel oil 15kg, food Sub- propyl propionate 5kg, isobutyl palmitate 60kg.
Preparation method be the same as Example 1.
Embodiment 4
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil, nutgall Propyl propionate and isobutyl palmitate (oil-based solvent) composition, wherein, apple seed oil 4kg, olive oil 10kg, apricot kernel oil 10kg, do not have Propyl galate 3kg, isobutyl palmitate 30kg.
Preparation method be the same as Example 1.
Embodiment 5
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil, nutgall Propyl propionate and isobutyl palmitate (oil-based solvent) composition, wherein, apple seed oil 5kg, olive oil 7kg, no apricot kernel oil 12kg, food Sub- propyl propionate 4kg, isobutyl palmitate 40kg.
Preparation method be the same as Example 1.
Embodiment 6
A kind of skin care compositions with crease-resistant effect, functional component is by apple seed oil, olive oil, apricot kernel oil and nutgall Propyl propionate is constituted, wherein, apple seed oil 4kg, olive oil 9kg, apricot kernel oil 10kg, propylgallate 4kg.
The preparation method of the above-mentioned skin care compositions with crease-resistant effect, specific preparation process is as follows:
(1) to weigh apple seed oil, olive oil, apricot kernel oil, propylgallate by prescription amount standby;
(2) apple seed oil, olive oil, apricot kernel oil and propylgallate are well mixed, produced.
Embodiment 7
A kind of creams with crease-resistant effect, formula is:
There is the skin care compositions of crease-resistant effect described in embodiment 1:5%
Laruyl alcohol sodium sulfovinate:0.8%
Ceteth -20:1%
Nexbase 2004:8%
Dimethyl silicone polymer:6%
Isopropyl palmitate:8%
Excipient thickener:6%
Preservative:IPBC- I (0.005%), is the 50% of convention amount
Bronopol (0.01%), is the 50% of convention amount
Deionized water:Surplus.
The method for preparing the cosmetics, the raw material composition of the cosmetics includes oil phase, aqueous phase and tool of the present invention There is the skin care compositions of crease-resistant effect, this method includes:
First make oil phase and the aqueous phase progress of cosmetic material primary emulsifying, adjust the temperature of the emulsification system, be cooled to 35 ~40 DEG C, the skin care compositions of the present invention with crease-resistant effect is added, system is agitated uniform, further basis after cooling Recipe requirements complete operation.
Embodiment 8
A kind of emulsion with crease-resistant effect, the raw material proportioning of the emulsion is as shown in table 1 below:
Table 1
The preparation method of the emulsion can be carried out according to the routine operation of this area, and it is generally comprised the steps:
(1) in oil phase pretreatment pot, by all raw material inputs of oil phase wherein, 90~95 DEG C are heated to, in heating Stirring, to being completely melt;
(2) aqueous phase pretreatment pot in, add deionized water after open stirring, then successively by the carbomer aqueous solution, glycerine, Propane diols, 1,3-BDO, Lubrajel oil input wherein, heat while stirring, are heated to more than 90 DEG C;
(3) before feeding intake, through filtering in oil phase all suction vacuum emulsification kettle, scraper plate stirring is started;Then again through filtering Suck aqueous phase, after the completion of change up successively speed stirring, homogenizer carry out vacuum emulsification, now emulsify temperature in the kettle be not lower than 80 ℃;Insulated and stirred 10~15 minutes, starts cooling;
(4) when emulsion temperature is down to less than 45 DEG C, sodium hydrate aqueous solution is added, is stirred;Maintain the temperature at Between 35~40 DEG C, after stirring, examine pH to qualified, then sequentially add aqueous preservative solution under stirring, Aqueous solution of sodium hyaluronate, composition and essence, are stirred;
(5) feeding carries out pH value detection and adjusted, and organoleptic indicator examines emulsion, qualified, filtering and discharging on request.
Experimental example 1
Test product:There are the creams of crease-resistant effect described in embodiment 7
Test object:100 healthy womens, 50-56 Sui
Method of testing:Sooner or later uniformly it is applied near the eyes
Testing time:28 days
Evaluation method:Silica gel replica, the statistical analysis of result is carried out using Quantirides softwares
The 3D analysis shows of silica gel replica thing, the creams with crease-resistant effect described in embodiment 7 effectively reduce wrinkle area 25%th, wrinkle length 23%, reduce wrinkle quantity 9%, and these results tool is statistically significant.
Experimental example 2
Test content see the table below 2.
Table 2
Comparative experimental example
Control group:It is shown in Table 3, preparation method be the same as Example 8, the reference composition is by rose, Rosa Damascana, olive Oil, apricot kernel oil and isobutyl palmitate (oil-based solvent) composition, wherein, rose 4kg, Rosa Damascana 5kg, olive oil 8kg, Apricot kernel oil 11kg, isobutyl palmitate 40kg, the preparation method ginseng be the same as Example 1 of the reference composition.
Experimental group:There is the emulsion of crease-resistant effect described in embodiment 8.
Method of testing is with experimental example 2.
Table 3
Result of the test shows that emulsion described in embodiment 8 has conspicuousness to change the wrinkle of subject than the control group emulsion of table 3 It is kind.After test 28 days, wrinkle area reduces 202% (p=0.0093), and wrinkle number reduces 180% (p=0.023), wrinkle Less 131% (p=0.027) of line total length, total wrinkle depth and mean depth reduce 324% and 160% (p respectively =0.0098 and p=0.030).
It is above-mentioned that a kind of skin care compositions with crease-resistant effect and preparation method and application is carried out with reference to embodiment Detailed description, be illustrative rather than limited, can include several embodiments according to limited scope, thus Changing and modifications under present general inventive concept is not departed from, should be belonged within protection scope of the present invention.

Claims (10)

1. a kind of skin care compositions with crease-resistant effect, it is characterised in that:Functional component is by apple seed oil, olive oil, almond Oil and propylgallate composition, by its parts by weight be calculated as 3-6 parts of apple seed oil, 5-20 parts of olive oil, 3-15 parts of apricot kernel oil, 0.1-5 parts of propylgallate.
2. the skin care compositions according to claim 1 with crease-resistant effect, it is characterised in that:Functional component presses its weight Number is calculated as 3-6 parts of apple seed oil, 7-10 parts of olive oil, 10-12 parts of apricot kernel oil, 3-4 parts of propylgallate.
3. the skin care compositions according to claim 1 with crease-resistant effect, it is characterised in that:Functional component presses its weight Number is calculated as 5 parts of apple seed oil, 8 parts of olive oil, 11 parts of apricot kernel oil, 4 parts of propylgallate.
4. the skin care compositions according to claim 1 with crease-resistant effect, it is characterised in that:Also it is including parts by weight 10-60 parts of isobutyl palmitate is used as oil-based solvent.
5. the preparation method of the skin care compositions with crease-resistant effect described in one of claim 1-3, it is characterised in that:Specific system Standby step is as follows:
(1) to weigh apple seed oil, olive oil, apricot kernel oil, propylgallate by prescription amount standby;
(2) apple seed oil, olive oil, apricot kernel oil and propylgallate are well mixed, produced.
6. the preparation method of the skin care compositions according to claim 5 with crease-resistant effect, it is characterised in that:By prescription Measure into the batch mixing of step (2) while adding isobutyl palmitate.
7. the skin care compositions with crease-resistant effect described in one of claim 1-4 is preparing the cosmetics side with crease-resistant effect The application in face.
8. a kind of anti-wrinkle cosmetic, it is characterised in that:It is skin-care cosmetics or cleaning class cosmetics, the power containing effective dose Profit requires the skin care compositions described in one of 1-4 with crease-resistant effect.
9. anti-wrinkle cosmetic according to claim 8, it is characterised in that:The skin-care cosmetics be toner, emulsion or Cream.
10. anti-wrinkle cosmetic according to claim 8, it is characterised in that:The cleaning class cosmetics are mildy wash, washed one's face Cream, shampoo or shower cream.
CN201710449778.4A 2017-06-15 2017-06-15 A kind of skin care compositions with crease-resistant effect and preparation method and application Pending CN107184439A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112716868A (en) * 2021-03-06 2021-04-30 广州相宜化妆品有限公司 Multifunctional microcrystalline soft film powder and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102125509A (en) * 2010-01-19 2011-07-20 上海华银日用品有限公司 Olive nourishing and tonic oil and preparation method thereof
CN103432034A (en) * 2013-08-23 2013-12-11 卡姆丹克太阳能(江苏)有限公司 Essential oil for regulating water and oil balance of skin
CN103891924A (en) * 2014-04-21 2014-07-02 山东三星玉米产业科技有限公司 Blending oil containing corn oil and preparation method of blending oil
CN105662919A (en) * 2016-04-12 2016-06-15 孟根森 Almond oil containing skin whitening and caring cream
CN106063770A (en) * 2016-05-31 2016-11-02 武汉兵兵药业有限公司 A kind of gel pad pasting containing growth factor and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102125509A (en) * 2010-01-19 2011-07-20 上海华银日用品有限公司 Olive nourishing and tonic oil and preparation method thereof
CN103432034A (en) * 2013-08-23 2013-12-11 卡姆丹克太阳能(江苏)有限公司 Essential oil for regulating water and oil balance of skin
CN103891924A (en) * 2014-04-21 2014-07-02 山东三星玉米产业科技有限公司 Blending oil containing corn oil and preparation method of blending oil
CN105662919A (en) * 2016-04-12 2016-06-15 孟根森 Almond oil containing skin whitening and caring cream
CN106063770A (en) * 2016-05-31 2016-11-02 武汉兵兵药业有限公司 A kind of gel pad pasting containing growth factor and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN112716868A (en) * 2021-03-06 2021-04-30 广州相宜化妆品有限公司 Multifunctional microcrystalline soft film powder and preparation method thereof
CN112716868B (en) * 2021-03-06 2023-02-28 广州相宜化妆品有限公司 Multifunctional microcrystalline soft film powder and preparation method thereof

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