CN107156563B - 一种鲜罗汉果脱色浓缩汁的制备工艺 - Google Patents
一种鲜罗汉果脱色浓缩汁的制备工艺 Download PDFInfo
- Publication number
- CN107156563B CN107156563B CN201710277285.7A CN201710277285A CN107156563B CN 107156563 B CN107156563 B CN 107156563B CN 201710277285 A CN201710277285 A CN 201710277285A CN 107156563 B CN107156563 B CN 107156563B
- Authority
- CN
- China
- Prior art keywords
- resin
- liquid
- fresh
- membrane
- ceramic membrane
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- 241001409321 Siraitia grosvenorii Species 0.000 title claims abstract description 69
- 235000011171 Thladiantha grosvenorii Nutrition 0.000 title claims abstract description 69
- 235000011389 fruit/vegetable juice Nutrition 0.000 title claims abstract description 58
- 238000002360 preparation method Methods 0.000 title claims abstract description 8
- 239000012528 membrane Substances 0.000 claims abstract description 111
- 239000000919 ceramic Substances 0.000 claims abstract description 59
- 239000011347 resin Substances 0.000 claims abstract description 55
- 229920005989 resin Polymers 0.000 claims abstract description 55
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 48
- 238000005406 washing Methods 0.000 claims abstract description 32
- 238000000108 ultra-filtration Methods 0.000 claims abstract description 31
- 229920006122 polyamide resin Polymers 0.000 claims abstract description 30
- 238000000605 extraction Methods 0.000 claims abstract description 23
- 238000000034 method Methods 0.000 claims abstract description 19
- 230000001954 sterilising effect Effects 0.000 claims abstract description 18
- 235000013399 edible fruits Nutrition 0.000 claims abstract description 17
- 238000005352 clarification Methods 0.000 claims abstract description 15
- 238000001223 reverse osmosis Methods 0.000 claims abstract description 15
- 238000000926 separation method Methods 0.000 claims abstract description 15
- 238000001471 micro-filtration Methods 0.000 claims abstract description 14
- 238000009461 vacuum packaging Methods 0.000 claims abstract description 14
- 125000002091 cationic group Chemical group 0.000 claims abstract description 12
- 238000005325 percolation Methods 0.000 claims abstract description 11
- 238000004659 sterilization and disinfection Methods 0.000 claims abstract description 7
- 239000007788 liquid Substances 0.000 claims description 69
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 45
- 238000005086 pumping Methods 0.000 claims description 32
- 239000008213 purified water Substances 0.000 claims description 22
- 239000012535 impurity Substances 0.000 claims description 18
- 239000000126 substance Substances 0.000 claims description 16
- 238000011144 upstream manufacturing Methods 0.000 claims description 16
- 238000007599 discharging Methods 0.000 claims description 14
- 239000000047 product Substances 0.000 claims description 14
- 150000001450 anions Chemical class 0.000 claims description 8
- 229910001385 heavy metal Inorganic materials 0.000 claims description 8
- 239000000463 material Substances 0.000 claims description 8
- 239000000447 pesticide residue Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 229930189775 mogroside Natural products 0.000 claims description 6
- 239000002244 precipitate Substances 0.000 claims description 6
- 239000000428 dust Substances 0.000 claims description 5
- 239000002994 raw material Substances 0.000 claims description 5
- 239000004576 sand Substances 0.000 claims description 5
- 238000004042 decolorization Methods 0.000 claims description 4
- 231100000331 toxic Toxicity 0.000 claims description 4
- 230000002588 toxic effect Effects 0.000 claims description 4
- 238000009423 ventilation Methods 0.000 claims description 4
- 238000004440 column chromatography Methods 0.000 claims description 3
- 239000012141 concentrate Substances 0.000 claims description 2
- 239000011148 porous material Substances 0.000 claims 1
- 238000005516 engineering process Methods 0.000 abstract description 12
- 239000000796 flavoring agent Substances 0.000 abstract description 12
- 235000019634 flavors Nutrition 0.000 abstract description 12
- 238000004519 manufacturing process Methods 0.000 abstract description 10
- 235000019640 taste Nutrition 0.000 abstract description 9
- 235000021049 nutrient content Nutrition 0.000 abstract description 4
- 238000000247 postprecipitation Methods 0.000 abstract description 4
- 238000005119 centrifugation Methods 0.000 abstract description 3
- 239000003814 drug Substances 0.000 abstract description 3
- 235000013305 food Nutrition 0.000 abstract description 3
- 235000013361 beverage Nutrition 0.000 abstract description 2
- 238000005265 energy consumption Methods 0.000 abstract description 2
- 230000006837 decompression Effects 0.000 abstract 1
- 238000010979 pH adjustment Methods 0.000 abstract 1
- 230000001276 controlling effect Effects 0.000 description 13
- 239000000049 pigment Substances 0.000 description 8
- GHBNZZJYBXQAHG-KUVSNLSMSA-N (2r,3r,4s,5s,6r)-2-[[(2r,3s,4s,5r,6r)-6-[[(3s,8s,9r,10r,11r,13r,14s,17r)-17-[(2r,5r)-5-[(2s,3r,4s,5s,6r)-4,5-dihydroxy-3-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-6-[[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@H](CC[C@@H](C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]6[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O6)O)O5)O)CC4)(C)C)=CC[C@H]3[C@]2(C)CC1)C)C(C)(C)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O GHBNZZJYBXQAHG-KUVSNLSMSA-N 0.000 description 6
- TVJXHJAWHUMLLG-UHFFFAOYSA-N mogroside V Natural products CC(CCC(OC1OC(COC2OC(CO)C(O)C(O)C2OC3OC(CO)C(O)C(O)C3O)C(O)C(O)C1O)C(C)(C)O)C4CCC5(C)C6CC=C7C(CCC(OC8OC(COC9OC(CO)C(O)C(O)C9O)C(O)C(O)C8O)C7(C)C)C6(C)C(O)CC45C TVJXHJAWHUMLLG-UHFFFAOYSA-N 0.000 description 6
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 5
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 5
- 239000003729 cation exchange resin Substances 0.000 description 5
- 235000015097 nutrients Nutrition 0.000 description 5
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 4
- 229930006000 Sucrose Natural products 0.000 description 4
- CZMRCDWAGMRECN-UGDNZRGBSA-N Sucrose Chemical compound O[C@H]1[C@H](O)[C@@H](CO)O[C@@]1(CO)O[C@@H]1[C@H](O)[C@@H](O)[C@H](O)[C@@H](CO)O1 CZMRCDWAGMRECN-UGDNZRGBSA-N 0.000 description 4
- 238000001914 filtration Methods 0.000 description 4
- 238000001556 precipitation Methods 0.000 description 4
- 230000001105 regulatory effect Effects 0.000 description 4
- 229960004793 sucrose Drugs 0.000 description 4
- 241000196324 Embryophyta Species 0.000 description 3
- 229930091371 Fructose Natural products 0.000 description 3
- 239000005715 Fructose Substances 0.000 description 3
- RFSUNEUAIZKAJO-ARQDHWQXSA-N Fructose Chemical compound OC[C@H]1O[C@](O)(CO)[C@@H](O)[C@@H]1O RFSUNEUAIZKAJO-ARQDHWQXSA-N 0.000 description 3
- 150000001768 cations Chemical class 0.000 description 3
- 235000009508 confectionery Nutrition 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- -1 etc. Chemical compound 0.000 description 3
- 235000015203 fruit juice Nutrition 0.000 description 3
- 239000004615 ingredient Substances 0.000 description 3
- 235000016709 nutrition Nutrition 0.000 description 3
- 239000001814 pectin Substances 0.000 description 3
- 235000010987 pectin Nutrition 0.000 description 3
- 229920001277 pectin Polymers 0.000 description 3
- 210000003491 skin Anatomy 0.000 description 3
- 238000001179 sorption measurement Methods 0.000 description 3
- FBPFZTCFMRRESA-KVTDHHQDSA-N D-Mannitol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO FBPFZTCFMRRESA-KVTDHHQDSA-N 0.000 description 2
- ZZZCUOFIHGPKAK-UHFFFAOYSA-N D-erythro-ascorbic acid Natural products OCC1OC(=O)C(O)=C1O ZZZCUOFIHGPKAK-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- 108010059820 Polygalacturonase Proteins 0.000 description 2
- 229930003268 Vitamin C Natural products 0.000 description 2
- 238000010411 cooking Methods 0.000 description 2
- 238000009295 crossflow filtration Methods 0.000 description 2
- 230000007547 defect Effects 0.000 description 2
- 239000008367 deionised water Substances 0.000 description 2
- 229910021641 deionized water Inorganic materials 0.000 description 2
- 108010093305 exopolygalacturonase Proteins 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 230000020477 pH reduction Effects 0.000 description 2
- 238000004806 packaging method and process Methods 0.000 description 2
- 150000007965 phenolic acids Chemical class 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 235000019154 vitamin C Nutrition 0.000 description 2
- 239000011718 vitamin C Substances 0.000 description 2
- LTDANPHZAHSOBN-IPIJHGFVSA-N (2R,3R,4S,5S,6R)-2-[[(2R,3S,4S,5R,6R)-6-[[(3S,8R,9R,10S,11R,13R,14S,17R)-17-[(2R,5R)-5-[(2S,3R,4S,5S,6R)-4,5-dihydroxy-3-[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-6-[[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxymethyl]oxan-2-yl]oxy-6-hydroxy-6-methylheptan-2-yl]-11-hydroxy-4,4,9,13,14-pentamethyl-2,3,7,8,10,11,12,15,16,17-decahydro-1H-cyclopenta[a]phenanthren-3-yl]oxy]-3,4-dihydroxy-5-[(2S,3R,4S,5S,6R)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]methoxy]-6-(hydroxymethyl)oxane-3,4,5-triol Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O[C@H]1[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O1)O)O[C@H](CC[C@@H](C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]6[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O6)O)O5)O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O5)O)CC4)(C)C)=CC[C@@H]3[C@]2(C)CC1)C)C(C)(C)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O LTDANPHZAHSOBN-IPIJHGFVSA-N 0.000 description 1
- XDIYNQZUNSSENW-UUBOPVPUSA-N (2R,3S,4R,5R)-2,3,4,5,6-pentahydroxyhexanal Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O.OC[C@@H](O)[C@@H](O)[C@H](O)[C@@H](O)C=O XDIYNQZUNSSENW-UUBOPVPUSA-N 0.000 description 1
- SWMBOMMGMHMOHE-KZXKDKCNSA-N (2r,3r,4r,5r)-hexane-1,2,3,4,5,6-hexol Chemical compound OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO.OC[C@@H](O)[C@@H](O)[C@H](O)[C@H](O)CO SWMBOMMGMHMOHE-KZXKDKCNSA-N 0.000 description 1
- WRPAFPPCKSYACJ-ZBYJYCAASA-N (2r,3r,4s,5s,6r)-2-[[(2r,3s,4s,5r,6r)-6-[[(3s,8r,9r,10s,11r,13r,14s,17r)-17-[(5r)-5-[(2s,3r,4s,5s,6r)-4,5-dihydroxy-6-(hydroxymethyl)-3-[(2r,3s,4r,5r,6s)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxyoxan-2-yl]oxy-6-hydroxy-6-methylheptan-2-yl]-11-hydrox Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@@H](CO)O[C@H]1O[C@H](CCC(C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO[C@H]6[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O6)O)O5)O)CC4)(C)C)=CC[C@@H]3[C@]2(C)CC1)C)C(C)(C)O)[C@H]1O[C@@H](CO)[C@H](O)[C@@H](O)[C@@H]1O WRPAFPPCKSYACJ-ZBYJYCAASA-N 0.000 description 1
- KYVIPFHNYCKOMQ-YMRJDYICSA-N (2r,3s,4s,5r,6r)-2-(hydroxymethyl)-6-[[(2r,3s,4s,5r,6s)-3,4,5-trihydroxy-6-[(3r,6r)-2-hydroxy-6-[(3s,8s,9r,10r,11r,13r,14s,17r)-11-hydroxy-4,4,9,13,14-pentamethyl-3-[(2r,3r,4s,5s,6r)-3,4,5-trihydroxy-6-(hydroxymethyl)oxan-2-yl]oxy-2,3,7,8,10,11,12,15,16,1 Chemical compound C([C@H]1O[C@H]([C@@H]([C@@H](O)[C@@H]1O)O)O[C@H](CC[C@@H](C)[C@@H]1[C@]2(C[C@@H](O)[C@@]3(C)[C@H]4C(C([C@@H](O[C@H]5[C@@H]([C@@H](O)[C@H](O)[C@@H](CO)O5)O)CC4)(C)C)=CC[C@H]3[C@]2(C)CC1)C)C(C)(C)O)O[C@@H]1O[C@H](CO)[C@@H](O)[C@H](O)[C@H]1O KYVIPFHNYCKOMQ-YMRJDYICSA-N 0.000 description 1
- 108090000790 Enzymes Proteins 0.000 description 1
- 102000004190 Enzymes Human genes 0.000 description 1
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 description 1
- KYVIPFHNYCKOMQ-UHFFFAOYSA-N Mogroside III Natural products C1CC2(C)C3CC=C(C(C(OC4C(C(O)C(O)C(CO)O4)O)CC4)(C)C)C4C3(C)C(O)CC2(C)C1C(C)CCC(C(C)(C)O)OC(C(C(O)C1O)O)OC1COC1OC(CO)C(O)C(O)C1O KYVIPFHNYCKOMQ-UHFFFAOYSA-N 0.000 description 1
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- GAMYVSCDDLXAQW-AOIWZFSPSA-N Thermopsosid Natural products O(C)c1c(O)ccc(C=2Oc3c(c(O)cc(O[C@H]4[C@H](O)[C@@H](O)[C@H](O)[C@H](CO)O4)c3)C(=O)C=2)c1 GAMYVSCDDLXAQW-AOIWZFSPSA-N 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 150000001413 amino acids Chemical class 0.000 description 1
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 description 1
- 235000019658 bitter taste Nutrition 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 210000002421 cell wall Anatomy 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000011968 cross flow microfiltration Methods 0.000 description 1
- 238000004332 deodorization Methods 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 210000002615 epidermis Anatomy 0.000 description 1
- 239000000835 fiber Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002212 flavone derivatives Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- 229930003935 flavonoid Natural products 0.000 description 1
- 235000017173 flavonoids Nutrition 0.000 description 1
- 239000008103 glucose Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- PNDPGZBMCMUPRI-UHFFFAOYSA-N iodine Chemical compound II PNDPGZBMCMUPRI-UHFFFAOYSA-N 0.000 description 1
- 238000005342 ion exchange Methods 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000011499 joint compound Substances 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 235000010355 mannitol Nutrition 0.000 description 1
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 1
- 239000012982 microporous membrane Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 229930191869 mogroside IV Natural products 0.000 description 1
- OKGRRPCHOJYNKX-UHFFFAOYSA-N mogroside IV A Natural products C1CC2(C)C3CC=C(C(C(OC4C(C(O)C(O)C(COC5C(C(O)C(O)C(CO)O5)O)O4)O)CC4)(C)C)C4C3(C)C(O)CC2(C)C1C(C)CCC(C(C)(C)O)OC(C(C(O)C1O)O)OC1COC1OC(CO)C(O)C(O)C1O OKGRRPCHOJYNKX-UHFFFAOYSA-N 0.000 description 1
- WRPAFPPCKSYACJ-UHFFFAOYSA-N mogroside IV E Natural products C1CC2(C)C3CC=C(C(C(OC4C(C(O)C(O)C(COC5C(C(O)C(O)C(CO)O5)O)O4)O)CC4)(C)C)C4C3(C)C(O)CC2(C)C1C(C)CCC(C(C)(C)O)OC1OC(CO)C(O)C(O)C1OC1OC(CO)C(O)C(O)C1O WRPAFPPCKSYACJ-UHFFFAOYSA-N 0.000 description 1
- 230000009149 molecular binding Effects 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- 239000011733 molybdenum Substances 0.000 description 1
- 238000001728 nano-filtration Methods 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000012466 permeate Substances 0.000 description 1
- 239000002243 precursor Substances 0.000 description 1
- 239000003755 preservative agent Substances 0.000 description 1
- 230000002335 preservative effect Effects 0.000 description 1
- 238000003825 pressing Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 229910052711 selenium Inorganic materials 0.000 description 1
- 239000011669 selenium Substances 0.000 description 1
- 238000002791 soaking Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000005720 sucrose Substances 0.000 description 1
- 229910052718 tin Inorganic materials 0.000 description 1
- 239000011135 tin Substances 0.000 description 1
- 150000008130 triterpenoid saponins Chemical class 0.000 description 1
- VHBFFQKBGNRLFZ-UHFFFAOYSA-N vitamin p Natural products O1C2=CC=CC=C2C(=O)C=C1C1=CC=CC=C1 VHBFFQKBGNRLFZ-UHFFFAOYSA-N 0.000 description 1
Images
Classifications
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/04—Extraction of juices
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/02—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation containing fruit or vegetable juices
- A23L2/08—Concentrating or drying of juices
- A23L2/082—Concentrating or drying of juices by membrane processes
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/72—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration
- A23L2/74—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by filtration using membranes, e.g. osmosis, ultrafiltration
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L2/00—Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
- A23L2/70—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter
- A23L2/80—Clarifying or fining of non-alcoholic beverages; Removing unwanted matter by adsorption
-
- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23L—FOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
- A23L33/00—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof
- A23L33/10—Modifying nutritive qualities of foods; Dietetic products; Preparation or treatment thereof using additives
- A23L33/105—Plant extracts, their artificial duplicates or their derivatives
Landscapes
- Engineering & Computer Science (AREA)
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- Nutrition Science (AREA)
- Chemical & Material Sciences (AREA)
- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Water Supply & Treatment (AREA)
- Botany (AREA)
- Mycology (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
Abstract
Description
Claims (6)
Priority Applications (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710277285.7A CN107156563B (zh) | 2017-04-25 | 2017-04-25 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
PCT/CN2018/077304 WO2018196476A1 (zh) | 2017-04-25 | 2018-02-27 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201710277285.7A CN107156563B (zh) | 2017-04-25 | 2017-04-25 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN107156563A CN107156563A (zh) | 2017-09-15 |
CN107156563B true CN107156563B (zh) | 2020-08-28 |
Family
ID=59813434
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201710277285.7A Active CN107156563B (zh) | 2017-04-25 | 2017-04-25 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
Country Status (2)
Country | Link |
---|---|
CN (1) | CN107156563B (zh) |
WO (1) | WO2018196476A1 (zh) |
Families Citing this family (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107156563B (zh) * | 2017-04-25 | 2020-08-28 | 湖南华诚生物资源股份有限公司 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
CN108497248A (zh) * | 2018-04-11 | 2018-09-07 | 湖南华诚生物资源股份有限公司 | 一种罗汉果浓缩汁及罗汉果果粉的制备方法 |
CN109247561A (zh) * | 2018-09-06 | 2019-01-22 | 湖南绿蔓生物科技股份有限公司 | 一种从罗汉果中制备罗汉果甜味组合物的方法及其应用 |
CN109601791A (zh) * | 2018-12-29 | 2019-04-12 | 湖南华诚生物资源股份有限公司 | 一种无花果鲜果浓缩汁的制备方法 |
CN110521993A (zh) * | 2019-08-13 | 2019-12-03 | 湖南艾达伦科技有限公司 | 罗汉果苷甜味和风味组合物及其制备方法与应用 |
CN110521894A (zh) * | 2019-08-16 | 2019-12-03 | 湖南艾达伦科技有限公司 | 一种罗汉果甜香风味脱色浓缩汁及其制备方法 |
CN111296708A (zh) * | 2020-02-24 | 2020-06-19 | 湖南华诚生物资源股份有限公司 | 一种采用固定化酶技术生产罗汉果提取物的方法 |
CN111374247B (zh) * | 2020-04-17 | 2022-09-30 | 湖南华诚生物资源股份有限公司 | 一种接骨木莓浓缩汁及其制备方法 |
CN112617146A (zh) * | 2020-12-08 | 2021-04-09 | 江西海富生物工程有限公司 | 一种罗汉果风味浓缩汁及其制备方法 |
CN113634009B (zh) * | 2021-07-30 | 2022-09-23 | 桂林航天工业学院 | 一种罗汉果甜甙制备方法和加工装置 |
CN114271416B (zh) * | 2022-01-10 | 2023-08-29 | 江西海富生物工程有限公司 | 一种用无法自然成熟的罗汉果制备罗汉果浓缩汁的方法 |
Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1436786A (zh) * | 2003-03-07 | 2003-08-20 | 桂林莱茵生物制品有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN1683387A (zh) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN101283831A (zh) * | 2008-05-09 | 2008-10-15 | 桂林莱茵生物科技股份有限公司 | 一种脱色罗汉果果汁制备方法及由所述方法制备的果汁 |
CN101863946A (zh) * | 2010-07-12 | 2010-10-20 | 湖南希尔天然药业有限公司 | 一种从干罗汉果中提取高含量罗汉果甜甙v的方法 |
CN103767019A (zh) * | 2012-10-25 | 2014-05-07 | 汤首亮 | 一种低温水浸逆流法鲜罗汉果原液提取工艺 |
CN105218612A (zh) * | 2015-09-30 | 2016-01-06 | 大闽食品(漳州)有限公司 | 一种提高罗汉果甜苷中罗汉果甜甙v纯度的方法 |
Family Cites Families (8)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101050230A (zh) * | 2006-04-07 | 2007-10-10 | 广州泽力医药科技有限公司 | 一种罗汉果提取物的提取制备工艺 |
CN102716670B (zh) * | 2012-06-21 | 2015-11-18 | 范耀荣 | 一种采用膜分离技术制备鲜罗汉果浓缩液的工艺 |
CN104069151B (zh) * | 2014-06-03 | 2017-09-19 | 周治德 | 一种罗汉果甙ⅳ含量高的提取物制备方法 |
CN104069152A (zh) * | 2014-06-05 | 2014-10-01 | 桂林三宝生物科技有限公司 | 一种罗汉果甙ⅳ含量高的提取物制备方法 |
CN104086614B (zh) * | 2014-07-25 | 2016-01-20 | 湖南华诚生物资源股份有限公司 | 一种适用于工业生产的罗汉果提取物的制备方法 |
CN104431841B (zh) * | 2014-11-18 | 2017-09-19 | 桂林莱茵生物科技股份有限公司 | 一种降低罗汉果提取物中多菌灵的方法 |
CN104558088A (zh) * | 2015-01-23 | 2015-04-29 | 江西海富生物工程有限公司 | 一种从罗汉果中提取罗汉果苷v的方法 |
CN107156563B (zh) * | 2017-04-25 | 2020-08-28 | 湖南华诚生物资源股份有限公司 | 一种鲜罗汉果脱色浓缩汁的制备工艺 |
-
2017
- 2017-04-25 CN CN201710277285.7A patent/CN107156563B/zh active Active
-
2018
- 2018-02-27 WO PCT/CN2018/077304 patent/WO2018196476A1/zh active Application Filing
Patent Citations (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1436786A (zh) * | 2003-03-07 | 2003-08-20 | 桂林莱茵生物制品有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN1683387A (zh) * | 2005-03-16 | 2005-10-19 | 桂林莱茵生物科技股份有限公司 | 一种从罗汉果中提取罗汉果甜甙的方法 |
CN101283831A (zh) * | 2008-05-09 | 2008-10-15 | 桂林莱茵生物科技股份有限公司 | 一种脱色罗汉果果汁制备方法及由所述方法制备的果汁 |
CN101863946A (zh) * | 2010-07-12 | 2010-10-20 | 湖南希尔天然药业有限公司 | 一种从干罗汉果中提取高含量罗汉果甜甙v的方法 |
CN103767019A (zh) * | 2012-10-25 | 2014-05-07 | 汤首亮 | 一种低温水浸逆流法鲜罗汉果原液提取工艺 |
CN105218612A (zh) * | 2015-09-30 | 2016-01-06 | 大闽食品(漳州)有限公司 | 一种提高罗汉果甜苷中罗汉果甜甙v纯度的方法 |
Non-Patent Citations (1)
Title |
---|
微滤和反渗透膜组合工艺浓缩罗汉果汁的研究;苏小建等;《膜科学与技术》;20090225;第29卷(第01期);第66-68页 * |
Also Published As
Publication number | Publication date |
---|---|
WO2018196476A1 (zh) | 2018-11-01 |
CN107156563A (zh) | 2017-09-15 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN107156563B (zh) | 一种鲜罗汉果脱色浓缩汁的制备工艺 | |
CN106008645B (zh) | 一种从罗汉果中提取罗汉果苷v的方法 | |
CN101548783B (zh) | 拐枣澄清果汁及其制备方法 | |
CN101040693B (zh) | 一种青梅浓缩果汁的制备方法 | |
CN106333193B (zh) | 一种甘薯淀粉加工废水全资源化利用方法 | |
CN101671378B (zh) | 一种利用真空低温提取分离甜菊糖苷的方法 | |
CN102349632B (zh) | 一种高色值红薯浓缩清汁的制备方法 | |
CN101167539B (zh) | 一种罗汉果鲜果脱臭浓缩汁生产方法 | |
CN106923113B (zh) | 从罗汉果甜甙吸附树脂柱排出的废液中生产罗汉果浓缩汁的工艺 | |
CN104489827A (zh) | 一种甘蔗浓缩汁的加工工艺 | |
CN102406048B (zh) | 利用海参漂烫液制取海参糖蛋白的方法 | |
CN102429275B (zh) | 一种植物本草饮料及其制备方法 | |
CN105294467A (zh) | 一种从发酵液中提取饲料级缬氨酸的新工艺 | |
KR20170139848A (ko) | 신기술을 이용한 사탕수수로부터 고순도 원당의 제조방법 | |
CN102888332A (zh) | 一种红枣醋的制备方法 | |
CN107188911A (zh) | 利用大豆糖蜜提取大豆低聚糖和大豆异黄酮的方法 | |
CN109619264A (zh) | 大豆益生肽复合水溶性功能因子的清洁生产方法 | |
CN108823034A (zh) | 一种拐枣果酒的酿造方法 | |
CN105859916B (zh) | 一种南菊芋9号菊芋菊粉的制备方法 | |
CN101597635B (zh) | 高纯度水苏糖的制备方法 | |
CN1927946A (zh) | 天然植物水溶性红色素的提取方法 | |
CN106350615A (zh) | 一种制备高纯度水果果糖的方法 | |
CN109601791A (zh) | 一种无花果鲜果浓缩汁的制备方法 | |
CN105688501A (zh) | 一种芦荟原汁凝胶的膜法浓缩工艺 | |
CN106135615B (zh) | 一种葛根糖的生产方法 |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
PB01 | Publication | ||
PB01 | Publication | ||
SE01 | Entry into force of request for substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
TA01 | Transfer of patent application right | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20180824 Address after: 410205 Hunan Changsha high tech Development Zone, Donghong street, 8 Xing Kang Nan Road. Applicant after: HUNAN HUACHENG BIOTECH, Inc. Address before: 541805 No. 6 Huaihe Road, Suqiao Economic Development Zone, Yongfu County, Guilin, the Guangxi Zhuang Autonomous Region Applicant before: GUANGXI AGLYCONE PLANT PRODUCTS Co.,Ltd. |
|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation of decolorized concentrated juice of fresh Siraitia grosvenorii Effective date of registration: 20210422 Granted publication date: 20200828 Pledgee: CITIC Bank Changsha branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2021980002898 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20231127 Granted publication date: 20200828 Pledgee: CITIC Bank Changsha branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2021980002898 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Preparation of decolorized concentrated juice of fresh siraitia grosvenorii Granted publication date: 20200828 Pledgee: Agricultural Bank of China Limited Changsha Wangcheng District sub branch Pledgor: HUNAN HUACHENG BIOTECH, Inc. Registration number: Y2024980000707 |