CN107141949A - A kind of gardens wooden bridge insect prevention, water-repellent paint and preparation method - Google Patents
A kind of gardens wooden bridge insect prevention, water-repellent paint and preparation method Download PDFInfo
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- CN107141949A CN107141949A CN201710479531.7A CN201710479531A CN107141949A CN 107141949 A CN107141949 A CN 107141949A CN 201710479531 A CN201710479531 A CN 201710479531A CN 107141949 A CN107141949 A CN 107141949A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
- C09D133/24—Homopolymers or copolymers of amides or imides
- C09D133/26—Homopolymers or copolymers of acrylamide or methacrylamide
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D175/00—Coating compositions based on polyureas or polyurethanes; Coating compositions based on derivatives of such polymers
- C09D175/04—Polyurethanes
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/14—Paints containing biocides, e.g. fungicides, insecticides or pesticides
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/011—Nanostructured additives
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Plant Pathology (AREA)
- Paints Or Removers (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention discloses a kind of gardens wooden bridge insect prevention, water-repellent paint and preparation method, the coating includes following component：Polyacrylamide, polyurethane, graphene, superfine talcum powder, nano silicon, nano aluminium oxide, white carbon, high viscous Concave-convex clay rod, Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, anistree time, garden burnet.Preparation method includes：Each traditional Chinese medicine ingredients are extracted, extract solution is obtained, freeze-dried powder is made；Polyacrylamide, aqueous polyurethane are added in reactor, graphene aqueous solution, 0.5 ~ 1.5h of stirring reaction is added；Superfine talcum powder, nano silicon, nano aluminium oxide, white carbon and high viscous Concave-convex clay rod are added, freeze-dried powder is added after being well mixed, is well mixed, produces the coating.The coating is decorated applied to gardens wooden bridge, not only causes wooden bridge to have preferable waterproof, antiseptic effect, also with excellent insect prevention, fungicidal properties, with preferable application value.
Description
Technical field
The present invention relates to gardens auxiliary facility technical field, and in particular to a kind of gardens wooden bridge insect prevention, water-repellent paint and
Preparation method.
Background technology
With the quickening of process of modernization, ratio of the reinforced concrete structure in our cities is increasing, city
City's " tropical island effect " is increasingly severe, in order that obtaining city can develop in a healthy way, urban landscaping is increasingly closed by people
Note.
In afforestation in addition to planting green plant, river, pond and supporting foot bridge, some foot bridges are additionally provided with
It is wooden, and wooden foot bridge is due to environment moist around, during long-term use.The feelings of decay of wood usually occur
Condition, one of the most obvious speciality of decay of wood is exactly that wood chip can loosely drop, in addition, because environment mesoclimate and biological factor
Many chemical changes and physical change can occur for influence, wood surface, such as because of the drying shrinkage of climate change generation, bulking, cracking, torsion
Song, going mouldy for producing under the high temperature conditions is rotten, produce rotten etc. is lost by worm, bacterium moth, so as to cause foot bridge to realize original
Some performances.
And being gradually proposed some in the prior art has the coating of water resistance, but existing water-repellent paint has work(
The characteristics of energyization is single, it is impossible to realize the performance requirement of wooden bridge in gardens comprehensively, therefore, research and development are a kind of both to have been had preferably
Water-tight corrosion-proof effect, there is the wooden bridge of excellent insect prevention, fungicidal properties to turn into the emphasis studied at present with coating again where, is also accorded with
The need for closing afforestation, with preferable application value.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of gardens wooden bridge insect prevention, water-repellent paint and
Preparation method, the coating is decorated applied to gardens wooden bridge, not only causes wooden bridge to have preferable waterproof, antiseptic effect, also has
There are excellent insect prevention, fungicidal properties, the phenomenon that wooden bridge is damaged caused by wooden bridge rots, the wooden bridge greatly prolonged can be prevented effectively from
Service life, with preferable application value.
The present invention solves technical problem and adopted the following technical scheme that：
The present invention relates to a kind of gardens wooden bridge insect prevention, water-repellent paint, include each component of following parts by weight：Polyacrylamide 16
~ 30 parts, 12 ~ 35 parts of polyurethane, 0.5 ~ 3 part of graphene, 10 ~ 20 parts of superfine talcum powder, 8 ~ 15 parts of nano silicon, nano oxygen
5 ~ 10 parts of aluminium of change, 5 ~ 12 parts of white carbon, 10 ~ 20 parts of high viscous Concave-convex clay rod, 5 ~ 20 parts of Dalmatian chrysanthemum, 3 ~ 8 parts of the root of Dahurain angelica, cassia bark 5 ~
12 parts, 3 ~ 10 parts of the fruit of Rangoon creeper, 3 ~ 7 parts of the root of langdu, anistree return 2 ~ 5 parts, 1 ~ 6 part of garden burnet.
Preferably, 22 parts of the polyacrylamide, 30 parts of polyurethane, 1.8 parts of graphene, superfine talcum powder 16 part, nanometer
2 parts of silica 1,8 parts of nano aluminium oxide, 6 parts of white carbon, 18 parts of high viscous Concave-convex clay rod, 16 parts of Dalmatian chrysanthemum, 5 parts of the root of Dahurain angelica,
7 parts of cassia bark, 8 parts of the fruit of Rangoon creeper, 5 parts of the root of langdu, anistree time 3 parts, 4 parts of garden burnet.
Preferably, the high viscous attapulgite be that natural attapulgite clay is purified, the product after thermal activation.
The invention further relates to it is a kind of prepare gardens wooden bridge insect prevention, water-repellent paint method, comprise the following steps：
（1）According to proportioning weigh respectively Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, it is anistree return, garden burnet crush and cross 100 ~
150 mesh sieves, are well mixed, are subsequently placed in apparatus,Soxhlet's, under the conditions of 70 DEG C ~ 90 DEG C, in ethanol and the mixed solvent of water
3 ~ 4h of middle extraction, obtains extract solution；
（2）Extract solution is concentrated, freeze-dried powder is then made；
（3）Polyacrylamide, aqueous polyurethane are added in reactor, add while stirring the concentration that configure be 0.1 ~
0.3g/L graphene aqueous solution, in 70 ~ 80 DEG C of 0.5 ~ 1.5h of stirring reaction；
（4）According to proportioning to step（3）Superfine talcum powder, nano silicon, nano aluminium oxide, hard charcoal are added in middle mixture
Black and high viscous Concave-convex clay rod, be placed in after being mixed evenly rotating speed be 2000 ~ 3000 turns/min cutter in shearing 15 ~
Freeze-dried powder, is then added in mixture by 30min, and 20 ~ 30min of ultrasound in ultrasonic wave is placed in after being well mixed, and is produced described
Coating.
Preferably, the step（1）The addition of the mixed volume of middle ethanol and water for pulverulent mixture gross mass 10 ~
20 times, the wherein volume ratio of ethanol and water is 1:0.8~3.
Preferably, the step（2）Middle method for concentration is to remove partial solvent using Rotary Evaporators so that mixed liquor matter
0.1 ~ 0.3 times before measuring as concentration.
Preferably, the step（4）The preparation method of middle high viscous Concave-convex clay rod comprises the following steps：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add the water of 20 times of amounts of Concave-convex clay rod, stirring is formed
Mud in suspension, 10 ~ 20min of ultrasound under Ultrasonic Conditions, takes upper suspension in 2000 ~ 3000 turns/min centrifuge
5 ~ 10min of centrifugal treating, vacuum filtration obtains filter cake；
By filter cake in vacuum drying chamber dry, be subsequently placed in Muffle furnace, with 20 DEG C/min speed program be warming up to 800 DEG C ~
900 DEG C of 3 ~ 5h of roasting, is ground to particle diameter for 100 ~ 150 mesh after cooling, obtain high viscous Concave-convex clay rod.
Preferably, the step（4）Middle shear temperature is 70 ~ 80 DEG C, and ultrasonic temperature is 45 ~ 60 DEG C.
Compared with prior art, the present invention has following beneficial effect：
（1）Wooden bridge insect prevention in gardens of the present invention, water-repellent paint, the coating are decorated applied to gardens wooden bridge, are not only made
Obtaining wooden bridge has preferable waterproof, antiseptic effect, also with excellent insect prevention, fungicidal properties, can be prevented effectively from wooden bridge and rot
The phenomenon that caused wooden bridge is damaged, the service life of the wooden bridge greatly prolonged, with preferable application value.
（2）Gardens wooden bridge of the present invention first passes through graphene to polyurethane and polyacrylamide with insect prevention, water-repellent paint
Amine is modified processing, due to unique laminar structured of graphene so that coating surface formation one layer of fine and close waterproof, anti-corrosion
Coating, considerably increases the water-tight corrosion-proof effect of coating, along with the mechanical property that graphene is excellent so that modified polymerization
Thing dope layer has the mechanical property such as preferable scratch-resistant, wear-resisting.
（3）Multiple traditional Chinese medicine ingredients are added with wooden bridge insect prevention in gardens of the present invention, water-repellent paint so that coating has
There are preferable expelling parasite, fungicidal properties, effectively prevent wooden bridge and grown by insect pest invasion and mould, extend the use longevity of wooden bridge
Life.
（4）High viscous Concave-convex clay rod is also added with wooden bridge insect prevention in gardens of the present invention, water-repellent paint, due to
Concave-convex clay rod unique chain layer structure and larger specific surface area so that each traditional Chinese medicinal components can uniform adsorption in bumps
The surface of rod stone clay, improves the dispersing uniformity of each component, along with the height of Concave-convex clay rod glues characteristic energy, increases
The antistripping property of strong coating, improves paint adhesion.
（5）Gardens wooden bridge of the present invention is simple and convenient to operate with the preparation method of insect prevention, water-repellent paint, preparation process
Thing pollutant is produced, safety and environmental protection, is adapted to popularization and application.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.The experimental method of unreceipted actual conditions in the following example, generally according to normal condition, for example
Sambrook equimoleculars are cloned：Laboratory manual（New York:Cold Spring Harbor Laboratory Press,
1989）Described in condition, or according to the condition proposed by manufacturer.
Embodiment 1：
A kind of gardens wooden bridge insect prevention, water-repellent paint and the preparation method of the preferred embodiment of the present invention；
The gardens wooden bridge insect prevention, water-repellent paint, are prepared from by each component of following weight：
22 parts of polyacrylamide, 30 parts of polyurethane, 1.8 parts of graphene, 16 parts of superfine talcum powder, 12 parts of nano silicon, receive
8 parts of aluminum oxide of rice, 6 parts of white carbon, 18 parts of high viscous Concave-convex clay rod, 16 parts of Dalmatian chrysanthemum, 5 parts of the root of Dahurain angelica, 7 parts of cassia bark, the fruit of Rangoon creeper 8
Part, 5 parts of the root of langdu, anistree time 3 parts, 4 parts of garden burnet.
The high viscous attapulgite is that natural attapulgite clay is purified, the product after thermal activation.
The present invention prepares gardens wooden bridge insect prevention, the method for water-repellent paint, comprises the following steps：
（1）According to proportioning weigh respectively Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, it is anistree return, garden burnet is crushed and crosses 150 mesh
Sieve, is well mixed, is subsequently placed in apparatus,Soxhlet's, under the conditions of 80 DEG C, extracts 4h in the in the mixed solvent of ethanol and water, obtains
Extract solution；
（2）Extract solution is concentrated, freeze-dried powder is then made；
（3）Polyacrylamide, aqueous polyurethane are added in reactor, the concentration configured is added while stirring is
0.2g/L graphene aqueous solution, in 80 DEG C of stirring reaction 1h；
（4）According to proportioning to step（3）Superfine talcum powder, nano silicon, nano aluminium oxide, hard charcoal are added in middle mixture
Black and high viscous Concave-convex clay rod, is placed in the cutter that rotating speed is 3000 turns/min after being mixed evenly and shears 20min, so
Freeze-dried powder is added in mixture afterwards, ultrasound 20min in ultrasonic wave is placed in after being well mixed, produces the coating.
Step（1）The addition of the mixed volume of middle ethanol and water is 15 times of pulverulent mixture gross mass, wherein ethanol
Volume ratio with water is 1:1.5.
Step（2）Middle method for concentration is to remove partial solvent using Rotary Evaporators so that before mixed liquor quality is concentration
0.2 times.
Step（4）The preparation method of middle high viscous Concave-convex clay rod comprises the following steps：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add the water of 20 times of amounts of Concave-convex clay rod, stirring is formed
Mud in suspension, the ultrasound 15min under Ultrasonic Conditions takes upper suspension centrifugal treating in 3000 turns/min centrifuge
10min, vacuum filtration obtains filter cake；
Filter cake is dried in vacuum drying chamber, is subsequently placed in Muffle furnace, 800 DEG C is warming up to 20 DEG C/min speed program
4h is calcined, particle diameter is ground to after cooling for 150 mesh, high viscous Concave-convex clay rod is obtained.
Step（4）Middle shear temperature is 80 DEG C, and ultrasonic temperature is 50 DEG C.
Embodiment 2：
A kind of gardens wooden bridge insect prevention, water-repellent paint and the preparation method of the preferred embodiment of the present invention；
The gardens wooden bridge insect prevention, water-repellent paint, are prepared from by each component of following weight：
16 parts of polyacrylamide, 12 parts of polyurethane, 0.5 part of graphene, 10 parts of superfine talcum powder, nano silicon 8 part, nanometer
5 parts of aluminum oxide, 5 parts of white carbon, 10 parts of high viscous Concave-convex clay rod, 5 parts of Dalmatian chrysanthemum, 3 parts of the root of Dahurain angelica, 5 parts of cassia bark, 3 parts of the fruit of Rangoon creeper,
3 parts of the root of langdu, anistree time 2 parts, 1 part of garden burnet.
The high viscous attapulgite is that natural attapulgite clay is purified, the product after thermal activation.
The present invention prepares gardens wooden bridge insect prevention, the method for water-repellent paint, comprises the following steps：
（1）According to proportioning weigh respectively Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, it is anistree return, garden burnet is crushed and crosses 100 mesh
Sieve, is well mixed, is subsequently placed in apparatus,Soxhlet's, under the conditions of 70 DEG C, extracts 4h in the in the mixed solvent of ethanol and water, obtains
Extract solution；
（2）Extract solution is concentrated, freeze-dried powder is then made；
（3）Polyacrylamide, aqueous polyurethane are added in reactor, the concentration configured is added while stirring is
0.1g/L graphene aqueous solution, in 70 DEG C of stirring reaction 1.5h；
（4）According to proportioning to step（3）Superfine talcum powder, nano silicon, nano aluminium oxide, hard charcoal are added in middle mixture
Black and high viscous Concave-convex clay rod, is placed in the cutter that rotating speed is 2000 turns/min after being mixed evenly and shears 30min, so
Freeze-dried powder is added in mixture afterwards, ultrasound 20min in ultrasonic wave is placed in after being well mixed, produces the coating.
Step（1）The addition of the mixed volume of middle ethanol and water is 10 times of pulverulent mixture gross mass, wherein ethanol
Volume ratio with water is 1:0.8.
Step（2）Middle method for concentration is to remove partial solvent using Rotary Evaporators so that before mixed liquor quality is concentration
0.1 times.
Step（4）The preparation method of middle high viscous Concave-convex clay rod comprises the following steps：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add the water of 20 times of amounts of Concave-convex clay rod, stirring is formed
Mud in suspension, the ultrasound 10min under Ultrasonic Conditions takes upper suspension centrifugal treating in 2000 turns/min centrifuge
10min, vacuum filtration obtains filter cake；
Filter cake is dried in vacuum drying chamber, is subsequently placed in Muffle furnace, 800 DEG C is warming up to 20 DEG C/min speed program
5h is calcined, particle diameter is ground to after cooling for 100 mesh, high viscous Concave-convex clay rod is obtained.
Step（4）Middle shear temperature is 70 DEG C, and ultrasonic temperature is 45 DEG C.
Embodiment 3：
A kind of gardens wooden bridge insect prevention, water-repellent paint and the preparation method of the preferred embodiment of the present invention；
The gardens wooden bridge insect prevention, water-repellent paint, are prepared from by each component of following weight：
30 parts of polyacrylamide, 35 parts of polyurethane, 3 parts of graphene, 20 parts of superfine talcum powder, nano silicon 15 part, nanometer
10 parts of aluminum oxide, 12 parts of white carbon, 20 parts of high viscous Concave-convex clay rod, 20 parts of Dalmatian chrysanthemum, 8 parts of the root of Dahurain angelica, 12 parts of cassia bark, the fruit of Rangoon creeper
10 parts, 7 parts of the root of langdu, anistree return 5 parts, 6 parts of garden burnet.
The high viscous attapulgite is that natural attapulgite clay is purified, the product after thermal activation.
The present invention prepares gardens wooden bridge insect prevention, the method for water-repellent paint, comprises the following steps：
（1）According to proportioning weigh respectively Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, it is anistree return, garden burnet is crushed and crosses 150 mesh
Sieve, is well mixed, is subsequently placed in apparatus,Soxhlet's, under the conditions of 90 DEG C, extracts 3h in the in the mixed solvent of ethanol and water, obtains
Extract solution；
（2）Extract solution is concentrated, freeze-dried powder is then made；
（3）Polyacrylamide, aqueous polyurethane are added in reactor, the concentration configured is added while stirring is
0.3g/L graphene aqueous solution, in 80 DEG C of stirring reaction 0.5h；
（4）According to proportioning to step（3）Superfine talcum powder, nano silicon, nano aluminium oxide, hard charcoal are added in middle mixture
Black and high viscous Concave-convex clay rod, is placed in the cutter that rotating speed is 3000 turns/min after being mixed evenly and shears 15min, so
Freeze-dried powder is added in mixture afterwards, ultrasound 30min in ultrasonic wave is placed in after being well mixed, produces the coating.
Step（1）The addition of the mixed volume of middle ethanol and water is 20 times of pulverulent mixture gross mass, wherein ethanol
Volume ratio with water is 1: 3.
Step（2）Middle method for concentration is to remove partial solvent using Rotary Evaporators so that before mixed liquor quality is concentration
0.3 times.
Step（4）The preparation method of middle high viscous Concave-convex clay rod comprises the following steps：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add the water of 20 times of amounts of Concave-convex clay rod, stirring is formed
Mud in suspension, the ultrasound 20min under Ultrasonic Conditions takes upper suspension centrifugal treating in 3000 turns/min centrifuge
5min, vacuum filtration obtains filter cake；
Filter cake is dried in vacuum drying chamber, is subsequently placed in Muffle furnace, 900 DEG C is warming up to 20 DEG C/min speed program
3h is calcined, particle diameter is ground to after cooling for 150 mesh, high viscous Concave-convex clay rod is obtained.
Step（4）Middle shear temperature is 80 DEG C, and ultrasonic temperature is 60 DEG C.
In summary, wooden bridge insect prevention in gardens of the present invention, water-repellent paint, the coating are filled applied to gardens wooden bridge
Decorations, not only cause wooden bridge to have preferable waterproof, antiseptic effect, also with excellent insect prevention, fungicidal properties, can be prevented effectively from
The phenomenon that wooden bridge is damaged caused by wooden bridge rots, the service life of the wooden bridge greatly prolonged, with preferable application value.This hair
The preparation method of the bright coating is simple and convenient to operate, and preparation process thing pollutant is produced, safety and environmental protection, is adapted to popularization and application.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow
Ring the substantive content of the present invention.
Claims (8)
1. a kind of gardens wooden bridge insect prevention, water-repellent paint, it is characterised in that：Include each component of following parts by weight：Polyacrylamide
16 ~ 30 parts of amine, 12 ~ 35 parts of polyurethane, 0.5 ~ 3 part of graphene, 10 ~ 20 parts of superfine talcum powder, 8 ~ 15 parts of nano silicon, receive
5 ~ 10 parts of aluminum oxide of rice, 5 ~ 12 parts of white carbon, 10 ~ 20 parts of high viscous Concave-convex clay rod, 5 ~ 20 parts of Dalmatian chrysanthemum, 3 ~ 8 parts of the root of Dahurain angelica, osmanthus
5 ~ 12 parts of skin, 3 ~ 10 parts of the fruit of Rangoon creeper, 3 ~ 7 parts of the root of langdu, anistree time 2 ~ 5 parts, 1 ~ 6 part of garden burnet.
2. wooden bridge insect prevention in gardens according to claim 1, water-repellent paint, it is characterised in that：The polyacrylamide 22
Part, 30 parts of polyurethane, 1.8 parts of graphene, 16 parts of superfine talcum powder, 12 parts of nano silicon, 8 parts of nano aluminium oxide, hard charcoal
Black 6 parts, it is 18 parts of high viscous Concave-convex clay rod, 16 parts of Dalmatian chrysanthemum, 5 parts of the root of Dahurain angelica, 7 parts of cassia bark, 8 parts of the fruit of Rangoon creeper, 5 parts of the root of langdu, anistree
Return 3 parts, 4 parts of garden burnet.
3. wooden bridge insect prevention in gardens according to claim 1, water-repellent paint, it is characterised in that：The high viscous attapulgite
Product for natural attapulgite clay is purified, after thermal activation.
4. one kind prepares gardens wooden bridge insect prevention as described in any one of claim 1 ~ 3, the method for water-repellent paint, its feature exists
In：Comprise the following steps：
（1）According to proportioning weigh respectively Dalmatian chrysanthemum, the root of Dahurain angelica, cassia bark, the fruit of Rangoon creeper, the root of langdu, it is anistree return, garden burnet crush and cross 100 ~
150 mesh sieves, are well mixed, are subsequently placed in apparatus,Soxhlet's, under the conditions of 70 DEG C ~ 90 DEG C, in ethanol and the mixed solvent of water
3 ~ 4h of middle extraction, obtains extract solution；
（2）Extract solution is concentrated, freeze-dried powder is then made；
（3）Polyacrylamide, aqueous polyurethane are added in reactor, add while stirring the concentration that configure be 0.1 ~
0.3g/L graphene aqueous solution, in 70 ~ 80 DEG C of 0.5 ~ 1.5h of stirring reaction；
（4）According to proportioning to step（3）Superfine talcum powder, nano silicon, nano aluminium oxide, hard charcoal are added in middle mixture
Black and high viscous Concave-convex clay rod, be placed in after being mixed evenly rotating speed be 2000 ~ 3000 turns/min cutter in shearing 15 ~
Freeze-dried powder, is then added in mixture by 30min, and 20 ~ 30min of ultrasound in ultrasonic wave is placed in after being well mixed, and is produced described
Coating.
5. wooden bridge insect prevention in gardens according to claim 4, the preparation method of water-repellent paint, it is characterised in that：The step
Suddenly（1）The addition of the mixed volume of middle ethanol and water is 10 ~ 20 times of pulverulent mixture gross mass, the wherein body of ethanol and water
Product is than being 1:0.8~3.
6. wooden bridge insect prevention in gardens according to claim 4, the preparation method of water-repellent paint, it is characterised in that：The step
Suddenly（2）Middle method for concentration is to remove partial solvent using Rotary Evaporators so that mixed liquor quality is 0.1 ~ 0.3 before concentration
Times.
7. wooden bridge insect prevention in gardens according to claim 4, the preparation method of water-repellent paint, it is characterised in that：The step
Suddenly（4）The preparation method of middle high viscous Concave-convex clay rod comprises the following steps：
Take natural attapulgite clay to be crushed and cross 200 mesh sieves, add the water of 20 times of amounts of Concave-convex clay rod, stirring is formed
Mud in suspension, 10 ~ 20min of ultrasound under Ultrasonic Conditions, takes upper suspension in 2000 ~ 3000 turns/min centrifuge
5 ~ 10min of centrifugal treating, vacuum filtration obtains filter cake；
By filter cake in vacuum drying chamber dry, be subsequently placed in Muffle furnace, with 20 DEG C/min speed program be warming up to 800 DEG C ~
900 DEG C of 3 ~ 5h of roasting, is ground to particle diameter for 100 ~ 150 mesh after cooling, obtain high viscous Concave-convex clay rod.
8. wooden bridge insect prevention in gardens according to claim 4, the preparation method of water-repellent paint, it is characterised in that：The step
Suddenly（4）Middle shear temperature is 70 ~ 80 DEG C, and ultrasonic temperature is 45 ~ 60 DEG C.
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107868560A (en) * | 2017-11-30 | 2018-04-03 | 明光市泰丰新材料有限公司 | A kind of waterproof peel timber paint and preparation method |
| CN108456488A (en) * | 2018-01-23 | 2018-08-28 | 合肥华盖光伏科技有限公司 | A kind of photovoltaic coating and preparation method improving solar energy conversion |
| CN108727980A (en) * | 2018-07-09 | 2018-11-02 | 合肥择浚电气设备有限公司 | A kind of preparation method of coating used for building exterior wall |
| CN112931747A (en) * | 2021-02-05 | 2021-06-11 | 西南科技大学 | High-energy electron beam irradiation storage process for radix angelicae |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103600547A (en) * | 2013-10-16 | 2014-02-26 | 鲁奎 | Agricultural deinsectization film |
| CN105984005A (en) * | 2016-01-28 | 2016-10-05 | 阜南县天亿工艺品有限公司 | Compound type insert-resistant agent for wooden handicrafts and preparation method thereof |
| CN106142249A (en) * | 2016-07-29 | 2016-11-23 | 安徽昌发实业有限公司 | A kind of wood surface hydrophobic insect-prevention treatment method |
| CN106543792A (en) * | 2016-11-08 | 2017-03-29 | 佛山佳牧乐科技有限公司 | The preparation method of the botanical insect-proof bacteriostatic agent that corrosion-resistant reflecting coating includes |
-
2017
- 2017-06-22 CN CN201710479531.7A patent/CN107141949A/en not_active Withdrawn
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103600547A (en) * | 2013-10-16 | 2014-02-26 | 鲁奎 | Agricultural deinsectization film |
| CN105984005A (en) * | 2016-01-28 | 2016-10-05 | 阜南县天亿工艺品有限公司 | Compound type insert-resistant agent for wooden handicrafts and preparation method thereof |
| CN106142249A (en) * | 2016-07-29 | 2016-11-23 | 安徽昌发实业有限公司 | A kind of wood surface hydrophobic insect-prevention treatment method |
| CN106543792A (en) * | 2016-11-08 | 2017-03-29 | 佛山佳牧乐科技有限公司 | The preparation method of the botanical insect-proof bacteriostatic agent that corrosion-resistant reflecting coating includes |
Non-Patent Citations (1)
| Title |
|---|
| 莫梦婷等: "聚氨酯防腐涂料的改性及其性能研究进展", 《涂料工业》 * |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107868560A (en) * | 2017-11-30 | 2018-04-03 | 明光市泰丰新材料有限公司 | A kind of waterproof peel timber paint and preparation method |
| CN108456488A (en) * | 2018-01-23 | 2018-08-28 | 合肥华盖光伏科技有限公司 | A kind of photovoltaic coating and preparation method improving solar energy conversion |
| CN108727980A (en) * | 2018-07-09 | 2018-11-02 | 合肥择浚电气设备有限公司 | A kind of preparation method of coating used for building exterior wall |
| CN112931747A (en) * | 2021-02-05 | 2021-06-11 | 西南科技大学 | High-energy electron beam irradiation storage process for radix angelicae |
| CN112931747B (en) * | 2021-02-05 | 2022-11-11 | 西南科技大学 | High-energy electron beam irradiation storage process for radix angelicae |
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