CN107126915A - One kind prepares mandelic acid reactor - Google Patents
One kind prepares mandelic acid reactor Download PDFInfo
- Publication number
- CN107126915A CN107126915A CN201710321440.0A CN201710321440A CN107126915A CN 107126915 A CN107126915 A CN 107126915A CN 201710321440 A CN201710321440 A CN 201710321440A CN 107126915 A CN107126915 A CN 107126915A
- Authority
- CN
- China
- Prior art keywords
- tank body
- reative cell
- storage room
- mandelic acid
- prepares
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C59/00—Compounds having carboxyl groups bound to acyclic carbon atoms and containing any of the groups OH, O—metal, —CHO, keto, ether, groups, groups, or groups
- C07C59/40—Unsaturated compounds
- C07C59/42—Unsaturated compounds containing hydroxy or O-metal groups
- C07C59/48—Unsaturated compounds containing hydroxy or O-metal groups containing six-membered aromatic rings
- C07C59/50—Mandelic acid
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The present invention relates to reactor technology field, especially one kind prepares mandelic acid reactor, the cover is arranged on tank body by multigroup retention mechanism, ring baffle is provided with the tank body, the reative cell is internally provided with multiple heaters, reative cell bottom side is communicated with water pipe, the reative cell in storage room with being provided with rabbling mechanism, rabbling mechanism one end in reative cell is arranged on bearing block, and bearing block is arranged on reative cell inner bottom part, rabbling mechanism in storage room runs through tank body, and rabbling mechanism is provided with sealed bearings with tank body contact site, the lower end of rabbling mechanism in storage room is provided with bearing block, limit base is additionally provided with the base, the side-lower of storage room one is communicated with drain pipe, and drain pipe on water pipe with being provided with valve.This can be stored to reaction solution, can accomplish detachable between cover and tank body, regularly its inside is cleaned, it is ensured that the life-span used.
Description
Technical field
Mandelic acid reactor is prepared the present invention relates to reactor technology field, more particularly to one kind.
Background technology
Mandelic acid not only can also be used to synthesis for the synthesis antispasmodic such as oxybutynin and de- ethyl oxybutynin
The anticholinergic agent such as Oxyphenonium Bromide and Oxyphencyclimine, compare their racemization structure, and optically active medicine more has efficient medicine
Reason is acted on.Therefore, the market prospects of single enantiomer amygdalic acid are very huge.Mandelic acid is in the middle of a kind of important organic synthesis
Body, is widely used for the synthesis such as agricultural chemicals and medicine.With the continuous extension in its market, the demand to mandelic acid is continuously increased, should
Also gradually widened with scope, when preparing mandelic acid, reactor becomes than indispensable instrument, and reactor can only enter now
The simple reaction of row, its function is not enough, it is proposed to this end that one kind prepares mandelic acid reactor.
The content of the invention
The invention aims to solve shortcoming present in prior art, and the one kind proposed prepares mandelic acid with instead
Answer device.
To achieve these goals, present invention employs following technical scheme：
Design one kind prepares mandelic acid reactor, including tank body and cover, and tank body is in cylinder, and tank body lower end is provided with
Base, and base is hollow setting, the cover is arranged on tank body by multigroup retention mechanism, is connected at the upper side of the cover
It is connected with the charging aperture for there are many mouthfuls, the tank body and is provided with ring baffle, and dividing plate is placed with the upside of ring baffle, and passes through
Bolt is spacing, and tank body is divided into reative cell and storage room by dividing plate, and reative cell is located on the upside of storage room, is set inside the reative cell
Multiple heaters are equipped with, reative cell bottom side is communicated with water pipe, the reative cell and storage room and is provided with rabbling mechanism,
Rabbling mechanism one end in reative cell is arranged on bearing block, and bearing block is arranged on reative cell inner bottom part, and the other end is passed through
Wear cover and stirring handle is connected with by snap fastener, the rabbling mechanism in storage room runs through tank body, and passes through gear
Group is connected with connecting rod, and rabbling mechanism is provided with sealed bearings with tank body contact site, the rabbling mechanism in storage room
Lower end is provided with bearing block, and bearing block is arranged in base, and limit base is additionally provided with the base, and connecting rod is through limit
Position seat, and extend base, the side-lower of storage room one is communicated with drain pipe, and drain pipe on water pipe with being provided with valve
Door, rabbling mechanism includes rotating shaft, and rotating shaft is separately positioned on reative cell with storage room, multiple stir is provided with the outside of the rotating shaft
Mix leaf.
It is preferred that, it is provided with sealing ring at the top of the tank body.
It is preferred that, it is provided with one of charging aperture in capping, and capping and is provided with thermometer, thermometer is through envelope
Lid, and extend to reative cell bottom.
It is preferred that, also it is communicated with drug-feeding tube above the storage room side.
It is preferred that, the square groove that snap fastener includes being opened in reative cell in rotating shaft is connected on handle with being arranged on
Square fixture block, square fixture block is plugged in square groove, and cooperated between square groove and square fixture block.
It is preferred that, retention mechanism includes the first connecting plate being arranged on cover with installing the second connecting plate on tank body,
And first connecting plate and the second connecting plate outer sheath be provided with both sides above and below U-shaped frame, the U-shaped frame and be provided with bolt, it is entered
Row pretension.
It is preferred that, gear train includes the second bevel type gear being arranged in connecting rod and is mounted on rotating shaft in storage room
On the first bevel type gear, and between the first bevel type gear and the second bevel type gear be intermeshed.
It is preferred that, the base lower end is additionally provided with antiskid plate, and antiskid plate lower surface be provided with big sucker with it is multiple small
Sucker, multiple small suckers are arranged on the outside of big sucker.
One kind proposed by the present invention prepares mandelic acid reactor, and beneficial effect is：This prepares mandelic acid reactor
Reaction solution can be stored after completion of the reaction, it is to avoid specifically look for storage container, can accomplished between cover and tank body
It is detachable, regularly its inside is cleaned, it is ensured that the life-span used.
Brief description of the drawings
Fig. 1 is a kind of structural representation for preparing mandelic acid reactor proposed by the present invention；
Fig. 2 is a kind of retention mechanism structural representation for preparing mandelic acid reactor proposed by the present invention；
Fig. 3 is a kind of antiskid plate present invention looks up structural representation for preparing mandelic acid reactor proposed by the present invention；
Fig. 4 is a kind of pivot structure schematic diagram for preparing mandelic acid reactor proposed by the present invention.
In figure：1 tank body, 2 storage rooms, 3 ring baffles, 4 reative cells, 5 retention mechanisms, 51U types frame, 52 bolts, 6 covers, 7
Charging aperture, 8 thermometers, 9 connection handles, 10 rotating shafts, 101 square grooves, 11 paddles, 12 heaters, 13 drug-feeding tubes, 14 go out liquid
Pipe, 15 valves, 16 bases, 17 antiskid plates, 171 big suckers, 172 small suckers, 18 first bevel type gears, 19 second bevel type gears,
20 connecting rods, 21 limit bases, 22 water pipes, 23 sealing rings.
Embodiment
Below in conjunction with the accompanying drawing in the embodiment of the present invention, the technical scheme in the embodiment of the present invention is carried out clear, complete
Site preparation is described, it is clear that described embodiment is only a part of embodiment of the invention, rather than whole embodiments.
Reference picture 1-4, one kind prepares mandelic acid reactor, including tank body 1 and cover 6, and tank body 1 is in cylinder, tank body 1
Lower end is provided with base 16, and base 16 is set to be hollow, and cover 6 is arranged on tank body 1 by multigroup retention mechanism 5, cover 6
Upper side is communicated with the charging aperture 7 for having many mouthfuls, and a variety of reaction solutions can carry out reative cell together by same charging aperture 7
In 4, reacted, can accomplish detachable between cover 6 and tank body 1, regularly its inside be cleaned, it is ensured that use
Life-span.
Ring baffle 3 is provided with tank body 1, and the upside of ring baffle 3 is placed with dividing plate, and, dividing plate spacing by bolt
By tank body, 1 point is reative cell 4 and storage room 2, and reative cell 4 is located at the upside of storage room 2, and reative cell 4 is internally provided with multiple add
Hot device 12, multiple heaters 12 are connected with same switch by wire, and switch is arranged on the outside of tank body 1, and are connected with
External power supply, the bottom side of reative cell 4 is communicated with water pipe 22, and reative cell 4 is located at being provided with rabbling mechanism in storage room 2
Rabbling mechanism one end in reative cell 4 is arranged on bearing block, and bearing block is arranged on the inner bottom part of reative cell 4, and the other end runs through
Cover 6 is simultaneously connected with stirring handle 9 by snap fastener, has accomplished the mixing to the reaction solution in reative cell 4.
Rabbling mechanism in storage room 2 runs through tank body 1, and is connected with connecting rod 20, and mixer by gear train
Structure is provided with sealed bearings with the contact site of tank body 1, it is ensured that its sealing, the lower end of the rabbling mechanism in storage room 2
Bearing block is provided with, and bearing block is arranged in base 16, and limit base 21 is additionally provided with base 16, and connecting rod 20 is through limit
Position seat 21, and extend base 16, the storing liquid in storage room 2 can be stirred, to prevent it from precipitating.
The side-lower of storage room 2 one is communicated with drain pipe 14, and drain pipe 14 is stirred with being provided with valve 15 on water pipe 22
Mechanism includes rotating shaft 10, and rotating shaft 10 is separately positioned on reative cell 4 and in storage room 2, the outside of rotating shaft 10 is provided with multiple stirrings
Leaf 11.
The top of tank body 1 is provided with sealing ring 23.
It is provided with one of charging aperture 7 in capping, and capping and is provided with thermometer 8, thermometer 8 runs through capping, and
The bottom of reative cell 4 is extended to, the temperature variations in reative cell 4 can be checked in real time.
Drug-feeding tube 13 is also communicated with above the side of storage room 2, storage room 2 can be carried out being passed through catalyst when necessary,
So as to improve the quality of reaction solution.
The square groove 101 that snap fastener includes being opened in reative cell 4 in rotating shaft 10 is connected on handle 9 with being arranged on
Square fixture block, square fixture block is plugged in square groove 101, and cooperated between square groove 101 and square fixture block.
Retention mechanism includes the first connecting plate being arranged on cover 6 with installing the second connecting plate on tank body 1, and first
Connecting plate and the second connecting plate outer sheath are provided with U-shaped frame 51, and U-shaped frame is provided with bolt 52 in both sides about 51, it carried out pre-
Tightly.
Gear train includes the second bevel type gear 19 being arranged in connecting rod 20 with being mounted on rotating shaft 10 in storage room 2
On the first bevel type gear 18, and between the first bevel type gear 18 and the second bevel type gear 19 be intermeshed.
The lower end of base 16 is additionally provided with antiskid plate 17, and the lower surface of antiskid plate 17 is provided with big sucker 171 and multiple small suctions
Disk 172, multiple small suckers 172 are arranged on the outside of big sucker 171, it is ensured that the stability of device operationally.
More than, it is only the present invention preferably embodiment, but protection scope of the present invention is not limited thereto, and it is any
Those familiar with the art the invention discloses technical scope in, technique according to the invention scheme and its invention
Design is subject to equivalent substitution or change, should all be included within the scope of the present invention.
Claims (8)
1. one kind prepares mandelic acid reactor, including tank body (1) and cover (6), tank body (1) is in cylinder, it is characterised in that：
Tank body (1) lower end is provided with base (16), and base (16) is set to be hollow, and the cover (6) passes through multigroup retention mechanism (5)
On tank body (1), it is communicated with the charging aperture (7) for there are many mouthfuls, the tank body (1) and sets at the upper side of the cover (6)
It is equipped with the upside of ring baffle (3), and ring baffle (3) and is placed with dividing plate, and it is spacing by bolt, and tank body (1) is divided into by dividing plate
Reative cell (4) and storage room (2), and reative cell (4) is located at storage room (2) upside, the reative cell (4) is internally provided with multiple
Heater (12), reative cell (4) bottom side is communicated with water pipe (22), and the reative cell (4) in storage room (2) with being provided with
Rabbling mechanism, rabbling mechanism one end in reative cell (4) is arranged on bearing block, and bearing block is arranged on reative cell (4)
Inner bottom part, the other end through cover (6) and is connected with stirring handle (9), the stirring in storage room (2) by snap fastener
Mechanism runs through tank body (1), and is connected with connecting rod (20) by gear train, and rabbling mechanism is provided with tank body (1) contact site
Sealed bearings, the lower end of the rabbling mechanism in storage room (2) is provided with bearing block, and bearing block is arranged on base (16)
It is interior, limit base (21) is additionally provided with the base (16), and connecting rod (20) runs through limit base (21), and extend base
(16), the side-lower of storage room (2) one is communicated with drain pipe (14), and drain pipe (14) on water pipe (22) with being provided with valve
Door (15), rabbling mechanism includes rotating shaft (10), and rotating shaft (10) is separately positioned in reative cell (4) and storage room (2), described turn
Multiple paddles (11) are provided with the outside of axle (10).
2. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that set at the top of the tank body (1)
It is equipped with sealing ring (23).
3. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that one of charging aperture (7)
On be provided with capping, and thermometer (8) is provided with capping, thermometer (8) extends to reative cell (4) bottom through capping.
4. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that storage room (2) side
Top is also communicated with drug-feeding tube (13).
5. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that snap fastener includes being opened in
Square groove (101) in reative cell (4) interior rotating shaft (10) is with being arranged on the square fixture block being connected on handle (9), square card
Block is plugged in square groove (101), and is cooperated between square groove (101) and square fixture block.
6. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that retention mechanism includes being arranged on
The first connecting plate on cover (6) is with installing on the outside of the second connecting plate on tank body (1), and the first connecting plate and the second connecting plate
U-shaped frame (51) is arranged with, the U-shaped frame (51) is provided with bolt (52) in both sides up and down, pretension is carried out to it.
7. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that gear train includes the company of being arranged on
The second bevel type gear (19) on extension bar (20) and the first bevel type gear being mounted in storage room (2) interior rotating shaft (10)
(18), and between the first bevel type gear (18) and the second bevel type gear (19) it is intermeshed.
8. one kind according to claim 1 prepares mandelic acid reactor, it is characterised in that base (16) lower end is also
Antiskid plate (17) is provided with, and antiskid plate (17) lower surface is provided with big sucker (171) and multiple small suckers (172), Duo Ge little
Sucker (172) is arranged on the outside of big sucker (171).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710321440.0A CN107126915A (en) | 2017-05-09 | 2017-05-09 | One kind prepares mandelic acid reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710321440.0A CN107126915A (en) | 2017-05-09 | 2017-05-09 | One kind prepares mandelic acid reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107126915A true CN107126915A (en) | 2017-09-05 |
Family
ID=59732683
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710321440.0A Pending CN107126915A (en) | 2017-05-09 | 2017-05-09 | One kind prepares mandelic acid reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107126915A (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107541454A (en) * | 2017-10-19 | 2018-01-05 | 江苏中通生物科技有限公司 | A kind of biological fermentation tank be easy to repair and observed |
| CN107875992A (en) * | 2017-12-11 | 2018-04-06 | 无锡市飞天油脂有限公司 | A kind of lubricating oil processing reactor of step reaction |
| CN108554317A (en) * | 2018-01-25 | 2018-09-21 | 葛映东 | The various feed type stirred autoclave of single channel |
| CN114130242A (en) * | 2021-11-08 | 2022-03-04 | 赣州澳丽尔化妆品有限公司 | Homogeneity mixing system is used in biological fermentation preparation of cosmetics |
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| CN204816416U (en) * | 2015-06-17 | 2015-12-02 | 南通拜森化工有限公司 | Acryl resin preparation facilities with adjustable |
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| CN205995344U (en) * | 2016-08-30 | 2017-03-08 | 山东固耐特新材料有限公司 | A kind of sludge proof coating mixed stirring device |
| CN206103802U (en) * | 2016-10-17 | 2017-04-19 | 青岛冠军石油化学有限公司 | Lubricating oil agitator |
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- 2017-05-09 CN CN201710321440.0A patent/CN107126915A/en active Pending
Patent Citations (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN204234090U (en) * | 2014-11-23 | 2015-04-01 | 中州大学 | The chemical reaction equipment of high stability |
| CN204816416U (en) * | 2015-06-17 | 2015-12-02 | 南通拜森化工有限公司 | Acryl resin preparation facilities with adjustable |
| CN205988745U (en) * | 2016-08-06 | 2017-03-01 | 李德文 | A kind of chemical reaction device |
| CN205995344U (en) * | 2016-08-30 | 2017-03-08 | 山东固耐特新材料有限公司 | A kind of sludge proof coating mixed stirring device |
| CN206103802U (en) * | 2016-10-17 | 2017-04-19 | 青岛冠军石油化学有限公司 | Lubricating oil agitator |
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Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107541454A (en) * | 2017-10-19 | 2018-01-05 | 江苏中通生物科技有限公司 | A kind of biological fermentation tank be easy to repair and observed |
| CN107875992A (en) * | 2017-12-11 | 2018-04-06 | 无锡市飞天油脂有限公司 | A kind of lubricating oil processing reactor of step reaction |
| CN108554317A (en) * | 2018-01-25 | 2018-09-21 | 葛映东 | The various feed type stirred autoclave of single channel |
| CN114130242A (en) * | 2021-11-08 | 2022-03-04 | 赣州澳丽尔化妆品有限公司 | Homogeneity mixing system is used in biological fermentation preparation of cosmetics |
| CN114130242B (en) * | 2021-11-08 | 2023-09-12 | 赣州澳丽尔化妆品有限公司 | Homogenizing stirring system for preparing biological fermentation of cosmetics |
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| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170905 |
|
| RJ01 | Rejection of invention patent application after publication |