CN107106961B - 用于连续生产二硝基甲苯的方法中的废气净化 - Google Patents

用于连续生产二硝基甲苯的方法中的废气净化 Download PDF

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Publication number
CN107106961B
CN107106961B CN201580053881.6A CN201580053881A CN107106961B CN 107106961 B CN107106961 B CN 107106961B CN 201580053881 A CN201580053881 A CN 201580053881A CN 107106961 B CN107106961 B CN 107106961B
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CN
China
Prior art keywords
toluene
offgas
condenser
dinitrotoluene
stream
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
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CN201580053881.6A
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English (en)
Chinese (zh)
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CN107106961A (zh
Inventor
T.克瑙夫
J.明尼希
W.洛伦茨
B.佩内曼
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Covestro Deutschland AG
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Covestro Deutschland AG
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/002—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by condensation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/16—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C205/00—Compounds containing nitro groups bound to a carbon skeleton
    • C07C205/06—Compounds containing nitro groups bound to a carbon skeleton having nitro groups bound to carbon atoms of six-membered aromatic rings
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D2257/00—Components to be removed
    • B01D2257/70—Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • B01D2257/702—Hydrocarbons
    • B01D2257/7027—Aromatic hydrocarbons

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Analytical Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Treating Waste Gases (AREA)
CN201580053881.6A 2014-10-02 2015-09-29 用于连续生产二硝基甲苯的方法中的废气净化 Expired - Fee Related CN107106961B (zh)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP14187532 2014-10-02
EP14187532.8 2014-10-02
PCT/EP2015/072397 WO2016050759A1 (de) 2014-10-02 2015-09-29 Abgasreinigung in einem verfahren zur kontinuierlichen herstellung von dinitrotoluol

Publications (2)

Publication Number Publication Date
CN107106961A CN107106961A (zh) 2017-08-29
CN107106961B true CN107106961B (zh) 2020-08-07

Family

ID=51663034

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201580053881.6A Expired - Fee Related CN107106961B (zh) 2014-10-02 2015-09-29 用于连续生产二硝基甲苯的方法中的废气净化

Country Status (7)

Country Link
US (1) US9896407B2 (enExample)
EP (1) EP3201169B1 (enExample)
JP (1) JP6736547B2 (enExample)
KR (1) KR20170063644A (enExample)
CN (1) CN107106961B (enExample)
HU (1) HUE050513T2 (enExample)
WO (1) WO2016050759A1 (enExample)

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107986249B (zh) * 2017-10-31 2020-08-04 湖北东方化工有限公司 硝基甲苯废酸脱硝后稀硝酸去除硝基甲苯的方法
CN109438246A (zh) * 2018-09-27 2019-03-08 青岛海湾精细化工有限公司 一种蒽醌的处理方法及处理系统
DE102018217955B4 (de) * 2018-10-19 2020-06-04 Plinke Gmbh Verfahren zur Aufarbeitung von Mischsäure und Abwasser aus der Nitrierung von Aromaten sowie Vorrichtung zur Durchführung des Verfahrens
CN110170185B (zh) * 2019-05-30 2023-07-25 湖北东方化工有限公司 一种废硫酸硝基化合物分离的装置及方法
CN111408248B (zh) * 2020-04-28 2022-06-21 山东济新环境工程有限公司 一种烷基烯酮二聚体生产中的废气处理工艺
CN111603869A (zh) * 2020-06-04 2020-09-01 湖北东方化工有限公司 一种多硝基甲苯粉尘收集新工艺
CN114425221A (zh) * 2022-01-13 2022-05-03 江苏淮河化工有限公司 一硝基甲苯生产过程中的VOCs处理方法
CN120548213A (zh) 2023-01-09 2025-08-26 巴斯夫欧洲公司 用于从气流中除去氮氧化物、一氧化二氮和一氧化碳的方法
WO2025125207A1 (en) 2023-12-11 2025-06-19 Basf Se Process for removing nitrogen monoxide, nitrogen dioxide and nitrous oxide from an exhaust gas stream

Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1576236A (zh) * 2003-06-30 2005-02-09 拜尔材料科学股份公司 二硝基甲苯制备过程的废水的处理方法
CN101108805A (zh) * 2006-07-21 2008-01-23 拜尔材料科学股份公司 生产二硝基甲苯的方法
WO2011082977A1 (de) * 2009-12-16 2011-07-14 Basf Se VERFAHREN ZUR AUFARBEITUNG VON NOx-HALTIGEN ABGASEN AUS ABWASSERSTRÖMEN VON NITRIERANLAGEN
CN102879375A (zh) * 2012-10-12 2013-01-16 陕西师范大学 硝基芳烃类爆炸物的识别检测方法

Family Cites Families (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US4331819A (en) * 1980-04-24 1982-05-25 E. I. Du Pont De Nemours And Company Water removal in nitration of aromatic hydrocarbons
DE3409719A1 (de) 1984-03-16 1985-09-19 Bayer Ag, 5090 Leverkusen Verfahren zur herstellung von dinitrotoluol
US5313009A (en) 1990-01-04 1994-05-17 Nrm International Technologies C.V. Nitration process
US5275701A (en) 1993-03-15 1994-01-04 Air Products And Chemicals, Inc. Process for purification and concentration of sulfuric acid
DE19636191B4 (de) 1996-08-02 2008-04-03 Bayer Materialscience Ag Verfahren zur Reinigung und Aufkonzentrierung von gebrauchten Schwefelsäuren
US5963878A (en) 1998-07-30 1999-10-05 Noram Engineering & Constructors Ltd. Nitration process
EP2877441B2 (de) * 2012-07-27 2021-06-16 Covestro Intellectual Property GmbH & Co. KG Verfahren zur herstellung von nitrobenzol durch adiabate nitrierung
US9227909B2 (en) 2012-10-10 2016-01-05 Covestro Deutschland Ag Method for the continuous production of nitrobenzene

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1576236A (zh) * 2003-06-30 2005-02-09 拜尔材料科学股份公司 二硝基甲苯制备过程的废水的处理方法
CN101108805A (zh) * 2006-07-21 2008-01-23 拜尔材料科学股份公司 生产二硝基甲苯的方法
WO2011082977A1 (de) * 2009-12-16 2011-07-14 Basf Se VERFAHREN ZUR AUFARBEITUNG VON NOx-HALTIGEN ABGASEN AUS ABWASSERSTRÖMEN VON NITRIERANLAGEN
CN102879375A (zh) * 2012-10-12 2013-01-16 陕西师范大学 硝基芳烃类爆炸物的识别检测方法

Also Published As

Publication number Publication date
JP2017531641A (ja) 2017-10-26
US9896407B2 (en) 2018-02-20
JP6736547B2 (ja) 2020-08-05
WO2016050759A1 (de) 2016-04-07
EP3201169B1 (de) 2020-06-03
EP3201169A1 (de) 2017-08-09
US20170291869A1 (en) 2017-10-12
HUE050513T2 (hu) 2020-12-28
KR20170063644A (ko) 2017-06-08
CN107106961A (zh) 2017-08-29

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