CN107100949B - A kind of combined type composite material brake disc and preparation method and application - Google Patents

A kind of combined type composite material brake disc and preparation method and application Download PDF

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Publication number
CN107100949B
CN107100949B CN201710249937.6A CN201710249937A CN107100949B CN 107100949 B CN107100949 B CN 107100949B CN 201710249937 A CN201710249937 A CN 201710249937A CN 107100949 B CN107100949 B CN 107100949B
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disk
carbon
composite material
aluminum matrix
silicon carbide
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CN107100949A (en
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李鹏涛
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Hunan Xin Xin New Material Co Ltd
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Hunan Xin Xin New Material Co Ltd
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D65/00Parts or details
    • F16D65/02Braking members; Mounting thereof
    • F16D65/12Discs; Drums for disc brakes
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C1/00Making non-ferrous alloys
    • C22C1/04Making non-ferrous alloys by powder metallurgy
    • C22C1/05Mixtures of metal powder with non-metallic powder
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/02Alloys based on aluminium with silicon as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C21/00Alloys based on aluminium
    • C22C21/10Alloys based on aluminium with zinc as the next major constituent
    • CCHEMISTRY; METALLURGY
    • C22METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22CALLOYS
    • C22C32/00Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ
    • C22C32/0047Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with carbides, nitrides, borides or silicides as the main non-metallic constituents
    • C22C32/0052Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with carbides, nitrides, borides or silicides as the main non-metallic constituents only carbides
    • C22C32/0063Non-ferrous alloys containing at least 5% by weight but less than 50% by weight of oxides, carbides, borides, nitrides, silicides or other metal compounds, e.g. oxynitrides, sulfides, whether added as such or formed in situ with carbides, nitrides, borides or silicides as the main non-metallic constituents only carbides based on SiC
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D65/00Parts or details
    • F16D65/02Braking members; Mounting thereof
    • F16D65/12Discs; Drums for disc brakes
    • F16D65/125Discs; Drums for disc brakes characterised by the material used for the disc body
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D65/00Parts or details
    • F16D65/02Braking members; Mounting thereof
    • F16D2065/13Parts or details of discs or drums
    • F16D2065/1304Structure
    • F16D2065/132Structure layered
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D65/00Parts or details
    • F16D65/02Braking members; Mounting thereof
    • F16D2065/13Parts or details of discs or drums
    • F16D2065/134Connection
    • F16D2065/1344Connection permanent, e.g. by casting
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D2200/00Materials; Production methods therefor
    • F16D2200/0004Materials; Production methods therefor metallic
    • F16D2200/0026Non-ferro
    • F16D2200/003Light metals, e.g. aluminium
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D2200/00Materials; Production methods therefor
    • F16D2200/0034Materials; Production methods therefor non-metallic
    • F16D2200/0039Ceramics
    • F16D2200/0047Ceramic composite, e.g. C/C composite infiltrated with Si or B, or ceramic matrix infiltrated with metal
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D2200/00Materials; Production methods therefor
    • F16D2200/0082Production methods therefor
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D2250/00Manufacturing; Assembly
    • F16D2250/0007Casting
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F16ENGINEERING ELEMENTS AND UNITS; GENERAL MEASURES FOR PRODUCING AND MAINTAINING EFFECTIVE FUNCTIONING OF MACHINES OR INSTALLATIONS; THERMAL INSULATION IN GENERAL
    • F16DCOUPLINGS FOR TRANSMITTING ROTATION; CLUTCHES; BRAKES
    • F16D2250/00Manufacturing; Assembly
    • F16D2250/0023Shaping by pressure

Abstract

The present invention relates to a kind of combined type composite material brake disc and preparation method and application;Belong to extraordinary brake disc development technique field.The combined type composite material brake disc includes frictional disk (1) and connection support plate (2);The material of the frictional disk (1) is carbon ceramic composite material, and the material of connection support plate (2) is the Gradient Aluminum Matrix compound by hot pressing.The combined type composite material brake disc includes that carbon ceramic composite material frictional disk (1) connects support plate (2) with Gradient Aluminum Matrix;Carbon ceramic composite material frictional disk (1) support plate (2) is connected with Gradient Aluminum Matrix by riveting to link into an integrated entity.When brake disc designed by the present invention is applied to high-speed rail, service life is apparently higher than existing product.

Description

A kind of combined type composite material brake disc and preparation method and application
Technical field
The present invention relates to a kind of combined type composite material brake disc and preparation method and application;Belong to extraordinary brake disc exploitation Technical field.
Background technique
Brake disc of high-speed train is one of component the most key in brake apparatus.Speed-raising and damped condition with train Lower service condition it is severe, huge braking thermic load and thermal shock can generate very big temperature gradient, lead to shape in brake disc At great thermal stress.It is therefore desirable to which disc material not only has stable, uniform frictional behaviour and higher wear-resisting property Except, it is necessary to there are higher thermal fatigue property and heating conduction, low elasticity modulus and thermal expansion coefficient, so that braking heat The rapid loss of energy, is formed by high thermal stress to reduce brake disc friction surface rapid heat cycle.Finally, to mitigate weight under vehicle spring Amount, disc material need to have lower density.
Currently, the brake disc that High Speed Train in China uses mainly uses cast iron and Forging Steel Brake Disc, such material is in room temperature With mechanical property, thermal deformation resistant ability and excellent heat stability under high temperature, wearability and processing performance are preferable, often with powder smelting Golden brake lining composition friction is secondary to be used.But it is heat-resisting consistent with wear-resisting property due to brake disc each section, make fatigue instead It is inconsistent with abrasion loss, it accelerates fire check and probability and expansion rate occurs, greatly reduce the service life of brake disc.And And such material heat dissipation effect is bad, high density limits the further promotion of train speed, and energy consumption in train journey is caused to increase Add.Therefore, development of new disc material is to improve brake disc performance, mitigate the weight of train, raising train speed as main Trend.
In recent years, domestic and international researcher develop in succession carbon/carbon compound material, aluminum matrix composite, carbon ceramic composite material, The brake discs new material such as bimetallic material, but all there is the advantage and deficiency of performance in use in various types of materials.Aluminium base is multiple The thermal conductivity of condensation material is good, is able to achieve disk body rapid cooling, ceramic particle is added, and forming ceramic reinforced aluminum matrix composites can Loss of weight, but it is low using temperature, and maximum operation (service) temperature is not higher than 400 DEG C, sharp wear will occurs more than this temperature surface, grinds Damage amount is higher than steel disk abrasion loss.
Summary of the invention
The present invention is used as brake disc after having attempted Gradient Aluminum Matrix and carbon ceramic composite material interworking for the first time.
A kind of combined type composite material brake disc of the present invention, the combined type composite material brake disc includes frictional disk (1) With connection support plate (2);The material of the frictional disk (1) is carbon ceramic composite material, and the material of connection support plate (2) is ladder Spend aluminum matrix composite;Contain SiC in the Gradient Aluminum Matrix, according to SiC content, by Gradient Aluminum Matrix point At the region E and the region F, the SiC content at any one position is greater than the content of any one position SiC in the region F in the region E; After frictional disk (1) and connection support plate (2) assembling, combined type composite material brake disc is obtained;Along combined type composite material system The direction of Moving plate thickness, the minimum range in the region E to frictional disk (1) are less than the region F to the minimum range of frictional disk (1).
A kind of combined type composite material brake disc of the present invention, the connection support plate (2) is by high silicon carbide aluminum-base composite material Charging tray (2-1) and low-carbon sial based composites disk (2-2) are constituted;The high silicon carbide aluminum matrix composite disk (2-1) with Mass percent meter includes following raw materials:
20~30wt% of SiC particulate;
Al-Mg-Si-Zr-Sc atomized powder 50-60wt%;
Surplus is Al powder and inevitable impurity;
The Al-Mg-Si-Zr-Sc atomized powder includes following components with mass percent:
Mg 1-7wt%;
Si 25-30wt%;
Zr 0.3-1.0wt%;
0.25~1.0wt% of Sc;
Surplus is Al;Above-mentioned raw materials are the raw material in the region E.
A kind of combined type composite material brake disc of the present invention, the low-carbon sial based composites disk (2-2) is with quality Percentages include following components:
5~10wt% of SiC particulate;
Zn 7.0-9.6wt%;Preferably 7.0-9.0wt%;
Mg 1.5-3.5wt%;
Cu 2.0-3.0wt%;
Zr 0.15-0.35wt%;
Sc 0.15-0.4wt%;
Surplus is Al powder and inevitable impurity.Said components are the component in the region F.
A kind of combined type composite material brake disc of the present invention, connection support plate (2) and frictional disk (1) pass through riveting and constitute one Body;After riveting;Along combined type composite material disc thickness direction, the low-carbon sial base connected on support plate (2) is multiple The minimum range of condensation material disk (2-2) to frictional disk (1) is greater than the high silicon carbide aluminum matrix composite disk in connection support plate (2) (2-1) arrives the minimum range of frictional disk (1).
A kind of combined type composite material brake disc of the present invention, the combined type composite material brake disc include carbon pottery composite wood Material frictional disk (1) connects support plate (2) with Gradient Aluminum Matrix;The carbon ceramic composite material frictional disk (1) include the face B and The face A, the face A are rubbing surface, and the face B is non-rubbing surface;The high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial Based composites disk (2-2) constitutes the connection support plate (2) by hot pressing;By frictional disk (1) and connection support plate (2) assembling Afterwards, along the direction of combined type composite material disc thickness, the high silicon carbide aluminum matrix composite disk (2-1) to the face B is most Small distance is less than its minimum range for arriving the face A.
A kind of combined type composite material brake disc of the present invention, the carbon ceramic composite material frictional disk (1) includes n frictional disk Counterbore (3);
The connection support plate (2) is equipped with n position counterbore (4) corresponding with frictional disk counterbore (3) and m Mesoporous (5);Counterbore (4) mesoporous (5) runs through high silicon carbide aluminum matrix composite disk (2-1) and low-carbon silicon aluminum-base composite Disk of material (2-2);
Support plate (2) and frictional disk (1) will be connected by frictional disk counterbore (3) and corresponding counterbore (4) with rivet Cold riveting is connected into an entirety;After cold riveting is connected into an entirety, rivet force is 0.7~1MPa;After cold riveting, obtain combined Material brake disc, the direction high silicon carbide aluminum matrix composite disk (2-1) along combined type composite material disc thickness arrive the face B Minimum range is -0.05mm~0.05mm.Preferably, riveting rivet used is copper or steel rivet.
A kind of preparation method of combined type composite material brake disc of the present invention: its scheme are as follows:
Connection support plate (2) is assembled with frictional disk (1);Obtain the combined type composite material brake disc;It is described The material of frictional disk (1) is carbon ceramic composite material;The connection support plate (2) is by high silicon carbide aluminum matrix composite disk (2-1) With low-carbon sial based composites disk (2-2) by being combined;
The high silicon carbide aluminum matrix composite disk (2-1) includes following raw materials by percentage to the quality:
20~30wt% of SiC particulate;
Al-Mg-Si-Zr-Sc atomized powder 50-60wt%;
Surplus is Al powder and inevitable impurity;
The Al-Mg-Si-Zr-Sc atomized powder includes following components with mass percent:
Mg 1-7wt%;
Si 25-30wt%;
Zr 0.3-1.0wt%;
0.25~1.0wt% of Sc;
Surplus is Al;
The low-carbon sial based composites disk (2-2) includes following components by percentage to the quality:
5~10wt% of SiC particulate;
Zn 7.0-9.6wt%, preferably 7.0-9.0wt%;
Mg 1.5-3.5wt%;
Cu 2.0-3.0wt%;
Zr 0.15-0.35wt%;
Sc 0.15-0.4wt%;
Surplus is Al powder and inevitable impurity.
Preferably, a kind of preparation method of combined type composite material brake disc of the present invention, preparation connection support plate (2) include the following steps:
Step I
High silicon carbide aluminum matrix composite is prepared by the design component of high silicon carbide aluminum matrix composite disk (2-1);It is right Gained high silicon carbide aluminum matrix composite carries out roughing, obtains high silicon carbide aluminum matrix composite disk crude green body;
Low-carbon sial based composites are prepared by the design component of low-carbon sial based composites disk (2-2);It is right Gained low-carbon sial based composites carry out roughing, obtain low-carbon sial based composites disk crude green body;
Step II
By being beaten to joint face for high silicon carbide aluminum matrix composite disk crude green body and low-carbon sial based composites disk crude green body It is milled to 0.5~2.5 μm of surface roughness Ra, cleaning, drying;
Step III
The face paste to be connected of high silicon carbide aluminum matrix composite and low-carbon sial based composites after step II is handled Merge the pressure for applying 20~40MPa along the vertical direction of binding face, hot pressing, hot pressing temperature is 520~620 DEG C, soaking time It is 5~30 minutes, release later, natural cooling in air obtains Gradient Aluminum Matrix connector green body;
Step IV
The Gradient Aluminum Matrix connector green body of step II is machined to the shape and size of layout design, and Counterbore (4) and mesoporous (5);It obtains by high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial based composites disk The connection support plate (2) of (2-2) composition.
In industrial applications, in step II, by high silicon carbide aluminum matrix composite and low-carbon sial based composites Polished to joint face with sand paper, make 0.5~2.5 μm of surface roughness Ra, then with dehydrated alcohol clean surface.
In industrial applications, in step III, hot pressing can be carried out in air.
Preferably, a kind of preparation method of combined type composite material brake disc of the present invention, the high silicon carbide aluminium The preparation method of based composites disk crude green body includes the following steps:
Step 1
By by design component with taking SiC powder, Al-Mg-Si-Zr-Sc atomized powder, aluminium powder, wherein the granularity of SiC powder be 10~ 20 μm, the granularity of Al-Mg-Si-Zr-Sc atomized powder is 50~150 μm, and the granularity of aluminium powder is 50~150 μm;
Step 2
The raw material of step 1 are put into blender, mixing 2~4 hours;
Step 3
Mixture cold is molded, and 250~350MPa of pressing pressure, pressing speed is 5~8mm/min, pressure maintaining 40~50 Second, obtain high silicon carbide aluminum matrix composite green compact;
Step 4
High silicon carbide aluminum matrix composite green compact is sintered in a vacuum furnace, sintering temperature is 550~570 DEG C, soaking time is 1~2 hour, and control furnace pressure is less than or equal to 0.1Pa, then cools to 50 DEG C or less with the furnace and comes out of the stove, obtains To high silicon carbide aluminum matrix composite sintered blank;
Step 5
Hot pressing or warm and hot forging are carried out to silicon carbide aluminum matrix composite sintered blank obtained by step 4, control hot extrusion or hot forging Making temperature is 390~440 DEG C, and hot pressing ratio is 8~12:1, and it is 60-90% that warm and hot forging, which controls pass deformation, obtains deformable member;
Step 6
Deformable member is machined out to obtain high silicon carbide aluminum matrix composite disk crude green body by design size.
Preferably, a kind of preparation method of combined type composite material brake disc of the present invention, the low-carbon sial The preparation method of based composites disk crude green body includes the following steps:
Step is 1.
By design component with SiC particulate, the source Zn, the source Mg, the source Cu, the source Zr, the source Sc, Al is taken, Al is melted in smelting furnace, Then it will be placed in molten aluminum with the source Zr, the source Sc, the source Cu, Al, SiC particulate taken;It is stirred evenly at 780~900 DEG C;Then it drops Temperature is added with the source Mg and the source Zn taken to 650~760 DEG C, stirs evenly, refine, stand casting;Obtain slab;
Step is 2.
To step, 1. gained slab carries out Homogenization Treatments, the slab after obtaining Homogenization Treatments;The Homogenization Treatments Temperature be 460~465 DEG C, the time is 36-48 hours;
Step is 3.
Hot extrusion or warm and hot forging are carried out to the slab after step 2. gained Homogenization Treatments, control hot extrusion or warm and hot forging temperature Degree is 390~440 DEG C, and hot extrusion ratio is 8~12:1, and it is 60-90% that warm and hot forging, which controls pass deformation, obtains deformable member;
Step is 4.
Deformable member is subjected to solution treatment, solid solubility temperature is 480~510 DEG C, solution time 1~3 hour, water of coming out of the stove later It quenches or the temperature of oil quenching to part of quenching is 10~40 DEG C;
Step is 5.
After solution treatment, ageing treatment is carried out immediately, control aging temp is 120~130 DEG C, aging time is 20~24 Hour;After ageing treatment, roughing is carried out, low-carbon sial based composites disk crude green body is obtained.
Preferably, a kind of preparation method of combined type composite material brake disc of the present invention, the preparation of frictional disk (1) Method includes the following steps:
Step A
By charcoal cloth and charcoal felt mass ratio 7.5~9:3~1, by 0 ° without latitude charcoal cloth, Carbon fibe net tire, 90 ° without latitude charcoal cloth, charcoal For web tire successively after successively circulation superposition, the method using relay-type needle thorn is introducing Carbon fibe beam system perpendicular to laying direction It is 0.3~0.6g/cm at density32.5D Carbon fibe needle pierce whole felt;
Step B
Carbon fibe needle obtained by step A is pierced whole felt fixation to be placed in high temperature furnace, under an argon atmosphere, in 1500~ 2100 DEG C, 3~10 hours preceding high-temperature heat treatments are carried out, pressure is micro-positive pressure, the whole felt before obtaining after high-temperature heat treatment;
Step C
Whole felt after high-temperature heat treatment before step B gained is subjected to chemical vapor deposition pyrolytic carbon processing, is deposited Uniformly and density is 1.0~1.5g/cm3Low density carbon carbon composite, the carbon-source gas of chemical vapor deposition is methane, third At least one of alkene, natural gas, diluent gas are nitrogen and/or hydrogen, and the volume ratio of carbon-source gas and diluent gas is 1:1 ~3, depositing temperature is 900~1050 DEG C, and sedimentation time is 100~300 hours.
Step D
Under inert protective atmosphere, in 1800~2300 DEG C, the resulting low density carbon carbon composite of step C is carried out high Warm graphitization processing handles the time 2~5 hours, is machined out into desired shape and size, thickness direction to each face later The machining allowance with a thickness of 1mm is reserved, and processes the counterbore (3) for connecting support plate connection with aluminum matrix composite;
Step E
The carbon carbon composite green body that step D is obtained is placed in the graphite crucible for being paved with silicon powder, silicon particle size is 0.01~0.1 μm, purity is not less than 99%, and the quality of silicon powder is 1.2~2.0 times of the theoretical silicon powder needed, and carbon carbon is compound Body of material is lain on silicon powder, then in 1500~1900 DEG C of progress siliconisings in vacuum high temperature furnace, handling the time is 1~2 small When, interior furnace is negative pressure or the micro-positive pressure for being filled with inert gas, and obtaining density is 1.8~2.5g/cm3Carbon ceramic composite material;
Step F
Thickness face is processed into the thickness gauge of product requirement by carbon ceramic composite material preform made from step E on grinding machine It is very little, obtain carbon ceramic composite material frictional disk.
A kind of application of combined type composite material brake disc of the present invention, including the brake disc is applied to bullet train On.
Principle and advantage:
Compared with prior art, advantage with have the active effect that
(1) present invention is not only had using the carbon ceramic composite material of the method preparation of infiltration silicon in carbon carbon composite Higher mechanical property, and wear resistance and antioxygenic property greatly improve, and compared with steel brake disc, are made pottery with carbon compound Material can not only realize the significantly loss of weight of train as brake disc, and the thermal stability of carbon ceramic composite brake disc it is high, No thermal vibration, service life that is wear-resistant, can substantially extending brake disc.
(2) compared with steel brake disc, the present invention is connected using carbon ceramic composite material frictional disk and Gradient Aluminum Matrix The train brake disk for connecing support plate combination, not only realizes the further loss of weight of train, carbon ceramic composite material frictional disk and gradient Structure aluminum matrix composite connection support plate binding pattern make material distribution it is more reasonable, the impact strength of brake disc and Creep resistance significantly improves, and the distribution of entire brake disc body temperature field is improved, and reduces the thermal stress generated when braking about 20%~30%, the loss of brake disc is substantially reduced when braking, and the service life of brake disc substantially extends, and total quality is obtained compared to steel disk Significantly to reduce.
Aluminum matrix composite connection support plate of the invention uses gradient-structure, selects high-carbon close to carbon pottery frictional disk side SiClx, the aluminum matrix composite without Cu, high silicon play heat transfer and supporting role to carbon pottery frictional disk in brake.It is close The temperature that one end of frictional disk is born in brake is much higher than 300 DEG C, and at such a temperature, mechanical property is aobvious for conventional aluminum alloys Writing reduces, it is therefore desirable to redesign to the material close to one section of frictional disk.Designed high silicon carbide aluminium in the present invention Be added to a large amount of silicon carbide and silicon in based composites, be not added with copper, the synergistic effect through each component, mechanical property and Properties of High Temperature Creep is much higher than conventional aluminum alloys.Side selection low-carbon SiClx far from carbon pottery frictional disk contains high Zn, Mg, Cu Superhigh intensity aluminum matrix composite, effective supporting role is played to high silicon carbide aluminum matrix composite disk.Height is carbonized The superhigh intensity aluminum matrix composite of silicon, the aluminum matrix composite of high silicon and low-carbon SiClx is by hot pressing connects, since the two is Same type of material, therefore the shear strength of linkage interface is higher, in conjunction with densification.Compared with whole steel disk, such combined material Brake disc is expected while significant loss of weight and high thermal conductivity, and the high heat of bring will not cause the significant of material when frictional disk is braked Creep.
Detailed description of the invention
Attached drawing 1 is the schematic illustration of novel combination type composite brake disk of the present invention;
Attached drawing 2a is the structural schematic diagram of combined type composite material brake disc prepared by embodiment 1;
Attached drawing 2b is the longitudinal sectional view of attached drawing 2a;
Attached drawing 3 is the structural schematic diagram of carbon ceramic composite material friction consolidation disk (1) in Fig. 2 a;
Attached drawing 4a is the structural schematic diagram that aluminum matrix composite connects support plate (2) in Fig. 2 a
Attached drawing 4b is the longitudinal sectional view of Fig. 4 a.
In figure, 1 be frictional disk, 2 be connect support plate, 3 be frictional disk counterbore on frictional disk, 4 be in connection support plate Counterbore corresponding with 3,5 are mesoporous;2-1 is high silicon carbide aluminum matrix composite disk;2-2 is low-carbon sial based composites Disk;A is that rubbing surface, the B on frictional disk are non-rubbing surface on frictional disk.
Specific embodiment
Below with reference to attached drawing of the invention, technical solution of the present invention is clearly and completely described, it is clear that retouched The embodiment stated is only a part of the embodiment in technical solution recorded in the present invention, instead of all the embodiments.It is based on The embodiment of the present invention, every other reality obtained by those of ordinary skill in the art without making creative efforts Example is applied, protection scope of the present invention is belonged to.
Referring to shown in Fig. 2~4, this combined type composite material train brake disk, braking disk body includes that a carbon pottery is compound Material friction disk 1 connects support plate 2 with a Gradient Aluminum Matrix;Include on carbon ceramic composite material friction consolidation disk 1 Several keyholes 3;Gradient Aluminum Matrix connects support plate 2 by high silicon carbide aluminum matrix composite disk 2-1 and low-carbon SiClx Aluminum matrix composite disk 2-2;It further include several positions and carbon pottery composite wood in Gradient Aluminum Matrix connection support plate 2 Expect the corresponding counterbore 4 of counterbore 3 and mesoporous 5 of frictional disk 1;Successively carbon ceramic composite material is rubbed with copper or steel rivet Disk 1 connects the progress cold riveting of support plate 2 with Gradient Aluminum Matrix and links into an integrated entity, and rivet force is 0.7~1MPa, and carbon is made pottery The non-rubbing surface B of composite material frictional disk 1 is corresponding with the disk C of high silicon carbide aluminum matrix composite disk 2-1.In use, this hair The bright mesoporous 6 for connecting support plate 2 by aluminum matrix composite is connected with train wheel hub, and carbon ceramic composite material frictional disk 1 rubs Wiping face A is working face.Braking for a long time when the carbon ceramic composite material frictional disk 1 of brake disc through brake causes thickness to become smaller, When needing replacing by regulation, demounting bolt, replacement frictional disk be can be used continuously.
In the present embodiment, the preparation method of frictional disk (1) includes the following steps:
Step A
By charcoal cloth and charcoal felt mass ratio 4:1, by 0 ° without latitude charcoal cloth, Carbon fibe net tire, 90 ° without latitude charcoal cloth, Carbon fibe net tire Successively successively circulation superposition after, use relay-type needle pierce method perpendicular to laying direction introduce Carbon fibe beam be made density for 0.5g/cm32.5D Carbon fibe needle pierce whole felt;
Step B
Carbon fibe needle obtained by step A is pierced whole felt fixation to be placed in high temperature furnace, under an argon atmosphere, in 1800 DEG C, 10 hours preceding high-temperature heat treatments are carried out, pressure is micro-positive pressure, the whole felt before obtaining after high-temperature heat treatment;
Step C
Whole felt after high-temperature heat treatment before step B gained is subjected to chemical vapor deposition pyrolytic carbon processing, is deposited Uniformly and density is 1.2g/cm3Low density carbon carbon composite, the carbon-source gas of chemical vapor deposition is methane, propylene, day At least one of right gas, diluent gas are nitrogen and/or hydrogen, and the volume ratio of carbon-source gas and diluent gas is 1:2, deposition Temperature is 1050 DEG C, and sedimentation time is 200 hours.
Step D
Under inert protective atmosphere, in 2100 DEG C, pyrographite is carried out to the resulting low density carbon carbon composite of step C Change processing, handles the time 4 hours, is machined out into desired shape and size to each face later, thickness direction reserves thickness For the machining allowance of 1mm, and process the counterbore (3) that support plate connection is connect with aluminum matrix composite;
Step E
The carbon carbon composite green body that step D is obtained is placed in the graphite crucible for being paved with silicon powder, silicon particle size is 0.05 μm, purity is not less than 99%, and the quality of silicon powder is 2 times of the theoretical silicon powder needed, and carbon carbon composite green body is laid flat On silicon powder, then in 1800 DEG C of progress siliconisings in vacuum high temperature furnace, handling the time is 2 hours, is negative pressure in furnace or is filled with The micro-positive pressure of inert gas, obtaining density is 2.5g/cm3Carbon ceramic composite material;
Step F
Thickness face is processed into the thickness gauge of product requirement by carbon ceramic composite material preform made from step E on grinding machine It is very little, obtain carbon ceramic composite material frictional disk.
In the present embodiment, the preparation of high silicon carbide aluminum matrix composite needed for high silicon carbide aluminum matrix composite disk (2-1) Method are as follows:
Step is 1.
Ingredient, SiC particulate 30wt%, Al-Mg-Si-Zr-Sc atomized powder 60wt% are carried out as required;
Surplus is Al powder and inevitable impurity;
Wherein the granularity of SiC powder is 20 μm, and the granularity of Al-Mg-Si-Zr-Sc atomized powder is 50 μm, and the granularity of aluminium powder is 100μm;
Step 1. described in Al-Mg-Si-Zr-Sc atomized powder with mass percent include following components:
Mg 7wt%;
Si 30wt%;
Zr 1.0wt%;
Sc 1.0wt%;
Surplus is Al.
Step is 2.
The raw material of step 1. are put into blender, mixing 3 hours.
Step is 3.
Mixture cold is molded, and pressing pressure 300MPa, pressing speed 5mm/min pressure maintaining 40 seconds, obtain high carbonization Sial based composites green compact.
Step is 4.
High silicon carbide aluminum matrix composite green compact is sintered in a vacuum furnace, sintering temperature is 560 DEG C, heat preservation Time is 1.5 hours, and control furnace pressure is less than or equal to 0.1Pa, then cools to 50 DEG C or less with the furnace and comes out of the stove, obtains high carbonization Sial based composites sintered blank.
Step is 5.
To step, 4. gained silicon carbide aluminum matrix composite sintered blank carries out hot pressing, controls hot extrusion or warm and hot forging temperature is 440 DEG C, hot pressing ratio is 10:1, obtains deformable member;
Step is 6.
To gained high silicon carbide aluminum matrix composite deformable member by carry out roughing is sized, spare high silicon carbide is obtained Aluminum matrix composite.
In the present embodiment, the material of low-carbon sial based composites disk (2-2) is low-carbon sial based composites;Institute The preparation method for stating low-carbon sial based composites includes the following steps:
Step 1
Match by design component and takes SiC particulate (granularity is 10 μm), the source Zn, the source Mg, the source Cu, the source Zr, the source Sc, Al, then will It is placed in smelting furnace with the source Zr, the source Sc, the source Cu, Al, SiC particulate taken;It is stirred evenly at 860 DEG C;Then 720 DEG C are cooled to, It is added with the source Mg and the source Zn taken, stirs evenly, refine, stand casting;Obtain slab;
Step 2
Homogenization Treatments are carried out to slab obtained by step 1, the slab after obtaining Homogenization Treatments;The Homogenization Treatments Temperature be 460~465 DEG C;Time is 4 hours;
Step 3
Hot extrusion is carried out to the slab after Homogenization Treatments obtained by step 2, the temperature for controlling hot extrusion is 420 DEG C, hot extrusion Pressure ratio is 9:1, obtains deformable member;
Step 4
Deformable member is subjected to solution treatment, solid solubility temperature is 500 DEG C, solution time 1.5 hours, come out of the stove later water quenching or oil Quenching to the temperature for part of quenching is 25 DEG C;
Step 5
After solution treatment, ageing treatment is carried out immediately, and control aging temp is 120 DEG C, aging time is 20 hours, is obtained The low-carbon sial based composites.
Gained low-carbon sial based composites include following components by percentage to the quality:
SiC 8.0wt%;
Zn 9.0wt%;
Mg 2.5wt%;
Cu 2.5wt%;
Zr 0.25wt%;
Sc 0.30wt%;
Surplus is Al and inevitable impurity.
The source Zr used is Al-Zr intermediate alloy;The source Sc is Al-Sc intermediate alloy;The source Cu Al-Cu intermediate alloy.The Zn Source is pure Zn ingot, and the source Mg is pure Mg ingot.
Step 5 and step 4. products obtained therefrom are obtained into connection support plate (2) by following step:
Step I
By being polished to joint face with sand paper for high silicon carbide aluminum matrix composite and low-carbon sial based composites, make table 1.0 μm of surface roughness Ra, surface then is cleaned with dehydrated alcohol;
Step II
By the high silicon carbide aluminum matrix composite of step I and low-carbon sial based composites to joint face fitting and edge The vertical direction of binding face applies the pressure of 40MPa, carries out hot pressing in air, and hot pressing temperature is 580 DEG C, soaking time 5 Minute, release later, natural cooling obtains Gradient Aluminum Matrix connector green body;
Step III
The Gradient Aluminum Matrix connector green body of step II is machined to the shape and size of layout design, and is added Work mesoporous, and the counterbore connecting with carbon ceramic composite material frictional disk, polish each face on grinding machine, obtain being carbonized by height The connection support plate (2) of sial based composites disk (2-1) and low-carbon sial based composites disk (2-2) composition.
Connection support plate (2) obtained by step III and carbon ceramic composite material frictional disk are passed through into steel rivet;It is made Moving plate;The performance detection of described brake disc each section is as shown in table 1.Under different braking speed, the friction of brake disc of the present invention Polishing machine is shown in Table 2.Experiment condition are as follows: dry friction: brake pressure 1MPa, sliding speed are respectively 8ms-1、16m·s-1、 24m·s-1, 2000 turns of coasting distance, mating plate is 30CrMoSiVA steel alloy.
The performance detection value of combined type composite material brake disc each section that 1 embodiment 1 of table is developed
Friction and wear behavior of the combined type composite material brake disc of 2 embodiment 1 of table exploitation under different braking
After each component combination is at brake disc, tested through experiment, with traditional steel brake disc, carbon ceramic Moving plate, aluminium base system It is multiple that Moving plate, carbon ceramic composite material frictional disk and single high silicon carbide aluminum matrix composite connect support plate combination brake disc, carbon pottery Condensation material frictional disk is compared with single low-carbon sial based composites connection support plate combination brake disc, and carbon ceramic composite material rubs It wipes disk and connects support plate combination brake disc with Gradient Aluminum Matrix under high-frequency damped condition, wear-resisting property and mechanics Performance significantly improves, and thermal stress is greatly reduced.Pure carbon ceramic composite brake disc brake when temperature up to 400~500 DEG C, by The high heating conduction of aluminum matrix composite, the temperature of combined type composite material brake disc of the invention only have 180 DEG C~300 DEG C. It is adapted to the design requirement of next-generation high-speed rail completely.

Claims (10)

1. a kind of combined type composite material brake disc, the combined type composite material brake disc includes frictional disk (1) and connection branch Support plate (2);It is characterized by: the material of the frictional disk (1) is carbon ceramic composite material, the material of connection support plate (2) For Gradient Aluminum Matrix;Contain SiC in the Gradient Aluminum Matrix, according to SiC content, by gradient aluminum-base composite material Material is divided into the region E and the region F, and the SiC content at any one position is greater than any one position SiC in the region F and contains in the region E Amount;After frictional disk (1) and connection support plate (2) assembling, combined type composite material brake disc is obtained;Along combined type composite material The direction of disc thickness, the minimum range in the region E to frictional disk (1) are less than the region F to the most narrow spacing of frictional disk (1) From.
2. a kind of combined type composite material brake disc according to claim 1, it is characterised in that: the connection support plate (2) it is made of high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial based composites disk (2-2);The high carbonization Sial based composites disk (2-1) includes following raw materials by percentage to the quality:
20~30wt% of SiC particulate;
Al-Mg-Si-Zr-Sc atomized powder 50-60wt%;
Surplus is Al powder and inevitable impurity;
The Al-Mg-Si-Zr-Sc atomized powder includes following components with mass percent:
Mg 1-7wt%;
Si 25-30wt%;
Zr 0.3-1.0wt%;
0.25~1.0wt% of Sc;
Surplus is Al;
The low-carbon sial based composites disk (2-2) includes following components by percentage to the quality:
5~10wt% of SiC particulate;
Zn 7.0-9.6wt%;
Mg 1.5-3.5wt%;
Cu 2.0-3.0wt%;
Zr 0.15-0.35wt%;
Sc 0.15-0.4wt%;
Surplus is Al powder and inevitable impurity.
3. a kind of combined type composite material brake disc according to claim 1, it is characterised in that: connection support plate (2) with Frictional disk (1) is integrally formed by riveting;After riveting;Along combined type composite material disc thickness direction, connection support The minimum range of low-carbon sial based composites disk (2-2) to frictional disk (1) on disk (2) is greater than in connection support plate (2) High silicon carbide aluminum matrix composite disk (2-1) arrive frictional disk (1) minimum range.
4. a kind of combined type composite material brake disc according to claim 2, it is characterised in that:
The combined type composite material brake disc includes that carbon ceramic composite material frictional disk (1) connects branch with Gradient Aluminum Matrix Support plate (2);The carbon ceramic composite material frictional disk (1) includes the face B and the face A, and the face A is rubbing surface, and the face B is non-rubbing surface; The high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial based composites disk (2-2) pass through described in hot pressing composition It connects support plate (2);After frictional disk (1) and connection support plate (2) assembling, along the side of combined type composite material disc thickness To the minimum range of the high silicon carbide aluminum matrix composite disk (2-1) to the face B is less than its minimum range for arriving the face A.
5. a kind of combined type composite material brake disc according to claim 2, it is characterised in that:
The carbon ceramic composite material frictional disk (1) includes n frictional disk counterbore (3);
The connection support plate (2) is equipped with n position counterbore (4) corresponding with frictional disk counterbore (3) and m mesoporous (5);The counterbore (4) and mesoporous (5) run through high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial base composite wood Charging tray (2-2);
Support plate (2) and frictional disk (1) cold riveting will be connected by frictional disk counterbore (3) and corresponding counterbore (4) with rivet It is connected into an entirety;After cold riveting is connected into an entirety, rivet force is 0.7~1MPa;After cold riveting, combined type composite material is obtained Brake disc arrives the minimum in the face B along the direction high silicon carbide aluminum matrix composite disk (2-1) of combined type composite material disc thickness Distance is -0.05mm~0.05mm.
6. a kind of method for preparing the combined type composite material brake disc as described in claim 1-5 any one, feature exist In:
Connection support plate (2) is assembled with frictional disk (1);Obtain the combined type composite material brake disc;The friction The material of disk (1) is carbon ceramic composite material;The connection support plate (2) is by high silicon carbide aluminum matrix composite disk (2-1) and low Silicon carbide aluminum matrix composite disk (2-2) is by being combined;
The high silicon carbide aluminum matrix composite disk (2-1) includes following raw materials by percentage to the quality:
20~30wt% of SiC particulate;
Al-Mg-Si-Zr-Sc atomized powder 50-60wt%;
Surplus is Al powder and inevitable impurity;
The Al-Mg-Si-Zr-Sc atomized powder includes following components with mass percent:
Mg 1-7wt%;
Si 25-30wt%;
Zr 0.3-1.0wt%;
0.25~1.0wt% of Sc;
Surplus is Al;
The low-carbon sial based composites disk (2-2) includes following components by percentage to the quality:
5~10wt% of SiC particulate;
Zn 7.0-9.6wt%;
Mg 1.5-3.5wt%;
Cu 2.0-3.0wt%;
Zr 0.15-0.35wt%;
Sc 0.15-0.4wt%;
Surplus is Al powder and inevitable impurity.
7. a kind of preparation method of combined type composite material brake disc according to claim 6, it is characterised in that: preparation connects Support plate (2) is connect to include the following steps:
Step I
High silicon carbide aluminum matrix composite is prepared by the design component of high silicon carbide aluminum matrix composite disk (2-1);To gained High silicon carbide aluminum matrix composite carries out roughing, obtains high silicon carbide aluminum matrix composite disk crude green body;
Low-carbon sial based composites are prepared by the design component of low-carbon sial based composites disk (2-2);To gained Low-carbon sial based composites carry out roughing, obtain low-carbon sial based composites disk crude green body;
Step II
By being polishing to joint face for high silicon carbide aluminum matrix composite disk crude green body and low-carbon sial based composites disk crude green body 0.5~2.5 μm of surface roughness Ra, cleaning, drying;
Step III
After step II is handled high silicon carbide aluminum matrix composite and low-carbon sial based composites to joint face fitting simultaneously The pressure for applying 20~40MPa along the vertical direction of binding face, hot pressing along air, hot pressing temperature are 520~620 DEG C, when heat preservation Between be 5~30 minutes, release later, natural cooling in air obtains Gradient Aluminum Matrix connector green body;
Step IV
The Gradient Aluminum Matrix connector green body of step III is machined to the shape and size and counterbore of layout design (4) and mesoporous (5);It obtains by high silicon carbide aluminum matrix composite disk (2-1) and low-carbon sial based composites disk (2-2) The connection support plate (2) of composition.
8. a kind of preparation method of combined type composite material brake disc according to claim 7, it is characterised in that;
The preparation method of the high silicon carbide aluminum matrix composite disk crude green body includes the following steps:
Step 1
By design component with SiC powder, Al-Mg-Si-Zr-Sc atomized powder, aluminium powder is taken, wherein the granularity of SiC powder is 10~20 μm, The granularity of Al-Mg-Si-Zr-Sc atomized powder is 50~150 μm, and the granularity of aluminium powder is 50~150 μm;
Step 2
The raw material of step 1 are put into blender, mixing 2~4 hours;
Step 3
Mixture cold is molded, and 250~350MPa of pressing pressure, pressing speed is 5~8mm/min, pressure maintaining 40~50 seconds, is obtained To high silicon carbide aluminum matrix composite green compact;
Step 4
High silicon carbide aluminum matrix composite green compact is sintered in a vacuum furnace, sintering temperature is 550~570 DEG C, is protected The warm time is 1~2 hour, and control furnace pressure is less than or equal to 0.1Pa, then cools to 50 DEG C or less with the furnace and comes out of the stove, obtains height Silicon carbide aluminum matrix composite sintered blank;
Step 5
Hot pressing or warm and hot forging are carried out to high silicon carbide aluminum matrix composite sintered blank obtained by step 4, control hot extrusion or warm and hot forging Temperature is 390~440 DEG C, and hot pressing ratio is 8~12:1, and it is 60-90% that warm and hot forging, which controls pass deformation, obtains deformable member;
Step 6
Deformable member is machined out to obtain high silicon carbide aluminum matrix composite disk crude green body by design size;
The preparation method of the low-carbon sial based composites disk crude green body includes the following steps:
Step is 1.
By design component with SiC particulate, the source Zn, the source Mg, the source Cu, the source Zr, the source Sc, Al is taken, Al is melted in smelting furnace, then It will be placed in molten aluminum with the source Zr, the source Sc, the source Cu, Al, SiC particulate taken;It is stirred evenly at 780~900 DEG C;Then it is cooled to It 650~760 DEG C, is added with the source Mg and the source Zn taken, stirs evenly, refine, stand casting;Obtain slab;
Step is 2.
To step, 1. gained slab carries out Homogenization Treatments, the slab after obtaining Homogenization Treatments;The temperature of the Homogenization Treatments Degree is 460~465 DEG C, the time is 36-48 hours;
Step is 3.
Hot extrusion or warm and hot forging are carried out to the slab after step 2. gained Homogenization Treatments, hot extrusion is controlled or warm and hot forging temperature is 390~440 DEG C, hot extrusion ratio is 8~12:1, and it is 60-90% that warm and hot forging, which controls pass deformation, obtains deformable member;
Step is 4.
Deformable member is subjected to solution treatment, solid solubility temperature is 480~510 DEG C, solution time 1~3 hour, come out of the stove later water quenching or The temperature of oil quenching to part of quenching is 10~40 DEG C;
Step is 5.
After solution treatment, ageing treatment is carried out immediately, control aging temp is 120~130 DEG C, aging time is 20~24 small When;After ageing treatment, roughing is carried out, low-carbon sial based composites disk crude green body is obtained.
9. a kind of preparation method of combined type composite material brake disc according to claim 6, it is characterised in that;Frictional disk (1) preparation method includes the following steps:
Step A
By charcoal cloth and charcoal felt mass ratio 7.5~9:3~1, by 0 ° without latitude charcoal cloth, Carbon fibe net tire, 90 ° without latitude charcoal cloth, Carbon fibe Net tire successively successively circulation superposition after, using relay-type needle thorn method perpendicular to laying direction introduce Carbon fibe beam be made it is close Degree is 0.3~0.6g/cm32.5D Carbon fibe needle pierce whole felt;
Step B
Carbon fibe needle obtained by step A is pierced whole felt fixation to be placed in high temperature furnace, under an argon atmosphere, in 1500~2100 DEG C, 3~10 hours preceding high-temperature heat treatments are carried out, pressure is micro-positive pressure, the whole felt before obtaining after high-temperature heat treatment;
Step C
Whole felt after high-temperature heat treatment before step B gained is subjected to chemical vapor deposition pyrolytic carbon processing, obtains depositing homogeneous And density is 1.0~1.5g/cm3Low density carbon carbon composite, the carbon-source gas of chemical vapor deposition be methane, propylene, At least one of natural gas, diluent gas are nitrogen and/or hydrogen, the volume ratio of carbon-source gas and diluent gas be 1:1~ 3, depositing temperature is 900~1050 DEG C, and sedimentation time is 100~300 hours;
Step D
Under inert protective atmosphere, in 1800~2300 DEG C, high fire stons is carried out to the resulting low density carbon carbon composite of step C Blackization processing, handles the time 2~5 hours, is machined out into desired shape and size to each face later, thickness direction reserves With a thickness of the machining allowance of 1mm, and process the counterbore (3) that support plate connection is connect with aluminum matrix composite;
Step E
The carbon carbon composite green body that step D is obtained is placed in the graphite crucible for being paved with silicon powder, silicon particle size be 0.01~ 0.1 μm, purity is not less than 99%, and the quality of silicon powder is 1.2~2.0 times of the theoretical silicon powder needed, by carbon carbon composite base Body is lain on silicon powder, then in 1500~1900 DEG C of progress siliconisings in vacuum high temperature furnace, handling the time is 1~2 hour, in furnace It is negative pressure or the micro-positive pressure for being filled with inert gas, obtaining density is 1.8~2.5g/cm3Carbon ceramic composite material;
Step F
Thickness face is processed into the thickness of product requirement by carbon ceramic composite material preform made from step E on grinding machine, Obtain carbon ceramic composite material frictional disk.
10. a kind of application of the combined type composite material brake disc as described in claim 1-5 any one, including by the braking Disk is applied on bullet train.
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