CN107094880A - Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues - Google Patents
Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues Download PDFInfo
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- CN107094880A CN107094880A CN201710265109.1A CN201710265109A CN107094880A CN 107094880 A CN107094880 A CN 107094880A CN 201710265109 A CN201710265109 A CN 201710265109A CN 107094880 A CN107094880 A CN 107094880A
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/16—Preserving with chemicals
- A23B9/24—Preserving with chemicals in the form of liquids or solids
- A23B9/26—Organic compounds; Microorganisms; Enzymes
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- A—HUMAN NECESSITIES
- A23—FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
- A23B—PRESERVING, e.g. BY CANNING, MEAT, FISH, EGGS, FRUIT, VEGETABLES, EDIBLE SEEDS; CHEMICAL RIPENING OF FRUIT OR VEGETABLES; THE PRESERVED, RIPENED, OR CANNED PRODUCTS
- A23B9/00—Preservation of edible seeds, e.g. cereals
- A23B9/16—Preserving with chemicals
- A23B9/24—Preserving with chemicals in the form of liquids or solids
- A23B9/30—Inorganic compounds
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- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Wood Science & Technology (AREA)
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- Food Science & Technology (AREA)
- Polymers & Plastics (AREA)
- Inorganic Chemistry (AREA)
- Microbiology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Auxiliary agent is stored the invention discloses oilseed prepared by a kind of utilization Zanthoxylum essential oil process residues, is related to oilseed storage technology field, is made up of the raw material of following parts by weight：25 35 parts of Zanthoxylum essential oil process residues freeze-dried powder, 5 10 parts of modified coal ash, 35 parts of furfural dregs freeze-dried powder, 23 parts of soy sauce residues freeze-dried powder, the root bark of tree peony extract 12 parts of residue freeze-dried powder, 12 parts of PVPP, 0.5 1 parts of pre-gelatinized pueraria starch, 0.5 1 parts of wood powder of Mi leaves immersion, 0.5 1 parts of saleratus power, 0.2 0.3 parts of oxytetracycline calcium, 0.2 0.3 parts of calamine stone.Oilseed storage auxiliary agent of the present invention not only realizes effective utilization of agricultural byproducts leftover bits and pieces Zanthoxylum essential oil process residues, furfural dregs and soy sauce residues, and made storage auxiliary agent has excellent Vermins-proof mildew-proof effect, while effective component contained by storing auxiliary agent has slow release effect.
Description
Technical field：
The present invention relates to oilseed storage technology field, and in particular to oil prepared by a kind of utilization Zanthoxylum essential oil process residues
Expect seed storage auxiliary agent.
Background technology：
The fat content of oilseed is high, is mainly used in squeezing for vegetable oil.Oilseed is in storage period, its contained oil
Fat carries out two course of reaction-hydrolysis and oxidation simultaneously.When epidemic disaster is suitable, fat resolves into free-fat in hydrolysis
Acid, the aggravation of this decomposable process often leads to become sour；Oxidizing process produces more peroxide, oilseed is gone bad.
In order to ensure the storage quality of oilseed, extend the storage time of oilseed, it is necessary to strictly control it to store
Condition.General impurity content, water content and storage temperature by controlling oilseed, the ventilation and heat situation of storeroom,
To prevent oilseed from phenomenon of going mouldy and become sour occur.In addition, by placing insecticide in storeroom outside or inside
Mode, to prevent Pests Damage oilseed.For above-mentioned situation, our company is using self-produced Zanthoxylum essential oil process residues to be main former
Material, is made oilseed storage auxiliary agent, to play Vermins-proof mildew-proof effect, it is to avoid insect pest and mould destruction oilseed.
The content of the invention：
The technical problems to be solved by the invention are to provide the profit that a kind of Vermins-proof mildew-proof effect is notable and preparation cost is low
The oilseed prepared with Zanthoxylum essential oil process residues stores auxiliary agent.
The technical problems to be solved by the invention are realized using following technical scheme：
Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues, by the raw material system of following parts by weight
Into：
25-35 parts of Zanthoxylum essential oil process residues freeze-dried powder, 5-10 parts of modified coal ash, 3-5 parts of furfural dregs freeze-dried powder, soy sauce residues
2-3 parts of freeze-dried powder, the root bark of tree peony extract 1-2 parts of residue freeze-dried powder, 1-2 parts of PVPP, 0.5-1 parts of pre-gelatinized pueraria starch, Mi
0.5-1 parts of wood powder of leaf immersion, 0.5-1 parts of saleratus power, 0.2-0.3 parts of oxytetracycline calcium, 0.2-0.3 parts of calamine stone.
The Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract residue and freezed
The fineness of powder is 60-100 mesh.
Mi leaves immersion wood powder by Mi leaves add water defibrination after immersion wood powder be made, specific preparation method is：Xiang Shui
It is middle to add the Mi leaves for being ground into coarse powder, using defibrination three times repeatedly of power 1.5kW fiberizers, Mi leaves are filtered to remove, to institute
Obtain and wood powder is added in filtrate, stirring makes wood powder dispersed, wood powder is filtered after immersion 8-12h, and send into dry in freeze drier
It is dry, produce Mi leaves immersion wood powder.
The weight consumption ratio of the Mi leaves and wood powder is 3-5:1-2.
Made Mi leaves immersion wood powder is cooperateed with as auxiliary agent strengthens the Vermins-proof mildew-proof effect that made oilseed stores auxiliary agent,
And assign certain effect on moisture extraction.
The preparation method of the oilseed storage auxiliary agent comprises the following steps：
(1) furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder, the root bark of tree peony are added into Zanthoxylum essential oil process residues freeze-dried powder and extracts residue
Freeze-dried powder and Mi leaves immersion wood powder, stand 2-3h after being sufficiently mixed, produce powder I；
(2) PVPP, oxytetracycline calcium and calamine stone are added into modified coal ash, and is warming up to 80-90 DEG C of guarantor
Temperature mixing 5-10min, then naturally cools to room temperature, produces powder II；
(3) powder II, pre-gelatinized pueraria starch and saleratus power are added into powder I, gained is mixed after being sufficiently mixed
Thing is blocking through vacuum compression, is eventually fabricated granularity 1-2mm particle.
The modified coal ash is formed by flyash through microwave modification, and its method of modifying is：Turpentine is added into flyash
Oil and hydrogenated rosin pentaerythritol ester, are sufficiently mixed after microwave treatment 3-5min under microwave frequency 2450MHz, power 700W,
Cetyl trimethylammonium bromide and erucyl amide are added, continues microwave treatment 3-5min after being well mixed, it is then naturally cold
But to room temperature, gained mixture is cooled to -10 DEG C with 10 DEG C/min cooling rate, and powder is made in last size-reduced machine, produces
Modified coal ash.
The flyash, turpentine oil, hydrogenated rosin pentaerythritol ester, cetyl trimethylammonium bromide and erucyl amide
Quality amount ratio is 15-20:0.5-1:1-2:0.5-1:0.3-0.5.
Flyash assigned after above-mentioned modification, not only made storage auxiliary agent necessarily except moist, moreover it is possible to increase fine coal
The specific surface area and adsorptivity of ash, in favor of the uniform attachment of Vermins-proof mildew-proof effective component, and play the effect of drug effect sustained release.
The beneficial effects of the invention are as follows：The present invention is assisted with a variety of auxiliary using Zanthoxylum essential oil process residues freeze-dried powder as primary raw material
Oilseed storage auxiliary agent is made in material, not only realizes agricultural byproducts leftover bits and pieces Zanthoxylum essential oil process residues, furfural dregs and soy sauce residues
Effective utilization, reduction storage auxiliary agent preparation cost；And made storage auxiliary agent has excellent Vermins-proof mildew-proof effect, can show
Pest control and mould destruction oilseed are write, while effective component contained by storing auxiliary agent has slow release effect, to ensure whole
Certain Vermins-proof mildew-proof effect can be played during individual storage to oilseed.
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
(1) 3 parts of furfural dregs freeze-dried powders, 3 parts of soy sauce residues freeze-dried powders, 1 are added into 30 parts of Zanthoxylum essential oil process residues freeze-dried powders
Part root bark of tree peony extracts residue freeze-dried powder and 0.5 part of Mi leaves immersion wood powder, stands 2h after being sufficiently mixed, produces powder I；
(2) 2 parts of PVPPs, 0.3 part of oxytetracycline calcium and 0.2 part of calamine stone are added into 5 parts of modified coal ash, and
80-90 DEG C of insulation mixing 10min is warming up to, room temperature is then naturally cooled to, produces powder II；
(3) powder II, 0.5 part of pre-gelatinized pueraria starch and 0.5 part of saleratus power are added into powder I, after being sufficiently mixed
Gained mixture is blocking through vacuum compression, it is eventually fabricated granularity 1-2mm particle.
Wherein, Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract residue and freezed
The fineness of powder is 60-100 mesh.
Mi leaves soak the preparation of wood powder：Xiang Shuizhong adds 5 parts of Mi leaves for being ground into coarse powder, is ground using power 1.5kW
Pulp grinder defibrination three times repeatedly, are filtered to remove Mi leaves, and 1 part of wood powder is added into gained filtrate, and stirring makes wood powder dispersed, soaks
Wood powder is filtered after bubble 12h, and sends into drying in freeze drier, Mi leaves immersion wood powder is produced.
The preparation of modified coal ash：0.5 part of turpentine oil and 1 part of hydrogenated rosin pentaerythrite are added into 20 parts of flyash
Ester, is sufficiently mixed after microwave treatment 5min under microwave frequency 2450MHz, power 700W, adds 1 part of cetyl trimethyl
Ammonium bromide and 0.3 part of erucyl amide, microwave treatment 5min is continued after being well mixed, and then naturally cools to room temperature, gained mixing
Thing is cooled to -10 DEG C with 10 DEG C/min cooling rate, and powder is made in last size-reduced machine, produces modified coal ash.
Embodiment 2
(1) 5 parts of furfural dregs freeze-dried powders, 2 parts of soy sauce residues freeze-dried powders, 1 are added into 35 parts of Zanthoxylum essential oil process residues freeze-dried powders
Part root bark of tree peony extracts residue freeze-dried powder and 0.5 part of Mi leaves immersion wood powder, stands 2h after being sufficiently mixed, produces powder I；
(2) 1 part of PVPP, 0.3 part of oxytetracycline calcium and 0.2 part of calamine stone are added into 8 parts of modified coal ash, and
80-90 DEG C of insulation mixing 10min is warming up to, room temperature is then naturally cooled to, produces powder II；
(3) powder II, 1 part of pre-gelatinized pueraria starch and 0.5 part of saleratus power are added into powder I, will after being sufficiently mixed
Gained mixture is blocking through vacuum compression, is eventually fabricated granularity 1-2mm particle.
Wherein, Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract residue and freezed
The fineness of powder is 60-100 mesh.
Mi leaves soak the preparation of wood powder：Xiang Shuizhong adds 5 parts of Mi leaves for being ground into coarse powder, is ground using power 1.5kW
Pulp grinder defibrination three times repeatedly, are filtered to remove Mi leaves, and 1 part of wood powder is added into gained filtrate, and stirring makes wood powder dispersed, soaks
Wood powder is filtered after bubble 12h, and sends into drying in freeze drier, Mi leaves immersion wood powder is produced.
The preparation of modified coal ash：0.5 part of turpentine oil and 2 parts of hydrogenated rosin pentaerythrites are added into 20 parts of flyash
Ester, is sufficiently mixed after microwave treatment 5min under microwave frequency 2450MHz, power 700W, adds 0.5 part of cetyl front three
Base ammonium bromide and 0.5 part of erucyl amide, microwave treatment 5min is continued after being well mixed, and then naturally cools to room temperature, and gained is mixed
Compound is cooled to -10 DEG C with 10 DEG C/min cooling rate, and powder is made in last size-reduced machine, produces modified coal ash.
Embodiment 3
(1) 5 parts of furfural dregs freeze-dried powders, 2 parts of soy sauce residues freeze-dried powders, 1 are added into 35 parts of Zanthoxylum essential oil process residues freeze-dried powders
Part root bark of tree peony extracts residue freeze-dried powder and 0.5 part of Mi leaves immersion wood powder, stands 2h after being sufficiently mixed, produces powder I；
(2) 1 part of PVPP, 0.3 part of oxytetracycline calcium and 0.2 part of calamine stone are added into 8 parts of flyash, and is heated up
To 80-90 DEG C of insulation mixing 10min, room temperature is then naturally cooled to, powder II is produced；
(3) powder II, 1 part of pre-gelatinized pueraria starch and 0.5 part of saleratus power are added into powder I, will after being sufficiently mixed
Gained mixture is blocking through vacuum compression, is eventually fabricated granularity 1-2mm particle.
Wherein, Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract residue and freezed
The fineness of powder is 60-100 mesh.
Mi leaves soak the preparation of wood powder：Xiang Shuizhong adds 5 parts of Mi leaves for being ground into coarse powder, is ground using power 1.5kW
Pulp grinder defibrination three times repeatedly, are filtered to remove Mi leaves, and 1 part of wood powder is added into gained filtrate, and stirring makes wood powder dispersed, soaks
Wood powder is filtered after bubble 12h, and sends into drying in freeze drier, Mi leaves immersion wood powder is produced.
Embodiment 4
(1) 5 parts of furfural dregs freeze-dried powders, 2 parts of soy sauce residues freeze-dried powders, 1 are added into 35 parts of Zanthoxylum essential oil process residues freeze-dried powders
Part root bark of tree peony extracts residue freeze-dried powder and 0.5 part of wood powder, stands 2h after being sufficiently mixed, produces powder I；
(2) 1 part of PVPP, 0.3 part of oxytetracycline calcium and 0.2 part of calamine stone are added into 8 parts of modified coal ash, and
80-90 DEG C of insulation mixing 10min is warming up to, room temperature is then naturally cooled to, produces powder II；
(3) powder II, 1 part of pre-gelatinized pueraria starch and 0.5 part of saleratus power are added into powder I, will after being sufficiently mixed
Gained mixture is blocking through vacuum compression, is eventually fabricated granularity 1-2mm particle.
Wherein, Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract residue and freezed
The fineness of powder is 60-100 mesh.
The preparation of modified coal ash：0.5 part of turpentine oil and 2 parts of hydrogenated rosin pentaerythrites are added into 20 parts of flyash
Ester, is sufficiently mixed after microwave treatment 5min under microwave frequency 2450MHz, power 700W, adds 0.5 part of cetyl front three
Base ammonium bromide and 0.5 part of erucyl amide, microwave treatment 5min is continued after being well mixed, and then naturally cools to room temperature, and gained is mixed
Compound is cooled to -10 DEG C with 10 DEG C/min cooling rate, and powder is made in last size-reduced machine, produces modified coal ash.
Reference examples 1
35 parts of Zanthoxylum essential oil process residues freeze-dried powders are blocking through vacuum compression, and granularity 1-2mm particle is made.Wherein,
The fineness of Zanthoxylum essential oil process residues freeze-dried powder is 60-100 mesh.
Embodiment 5
Embodiment 1, embodiment 2, embodiment 3 and the made oilseed of embodiment 4 storage auxiliary agent is utilized respectively to be made by double
Filling storage auxiliary agent 25g, is embedded in in batch rapeseed, is buried in 100kg rapeseed in the material bag of layer non-woven wraps, material bag
3 are put, remaining storage condition is identical, and compared with reference examples 1, the hoarding effect after determining 1 year, as a result as shown in table 1.
The oilseed of the present invention of table 1 stores the hoarding effect of auxiliary agent
| Project | Embodiment 1 | Embodiment 2 | Embodiment 3 | Embodiment 4 | Reference examples 1 |
| Can be extracted oil qualification rate/% | 99.85 | 99.91 | 97.06 | 98.63 | 96.24 |
| Oil yield/% | 41.92 | 42.43 | 38.28 | 40.54 | 36.28 |
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (7)
1. oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues, it is characterised in that by following parts by weight
Raw material be made：25-35 parts of Zanthoxylum essential oil process residues freeze-dried powder, 5-10 parts of modified coal ash, 3-5 parts of furfural dregs freeze-dried powder, sauce
2-3 parts of dregs of fat freeze-dried powder, the root bark of tree peony extract 1-2 parts of residue freeze-dried powder, 1-2 parts of PVPP, pre-gelatinized pueraria starch 0.5-1
Part, 0.5-1 parts of wood powder of Mi leaves immersion, 0.5-1 parts of saleratus power, 0.2-0.3 parts of oxytetracycline calcium, 0.2-0.3 parts of calamine stone.
2. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 1, it is characterised in that：
The Zanthoxylum essential oil process residues freeze-dried powder, furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder and the root bark of tree peony extract the fineness of residue freeze-dried powder
For 60-100 mesh.
3. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 1, it is characterised in that：
Mi leaves immersion wood powder by Mi leaves add water defibrination after immersion wood powder be made, specific preparation method is：Xiang Shuizhong adds powder
The Mi leaves of coarse powder are broken into, using defibrination three times repeatedly of power 1.5kW fiberizers, Mi leaves are filtered to remove, into gained filtrate
Wood powder is added, stirring makes wood powder dispersed, wood powder is filtered after immersion 8-12h, and send into drying in freeze drier, produce Mi
Leaf soaks wood powder.
4. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 3, it is characterised in that：
The weight consumption ratio of the Mi leaves and wood powder is 3-5:1-2.
5. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 1, it is characterised in that
Its preparation method comprises the following steps：
(1) furfural dregs freeze-dried powder, soy sauce residues freeze-dried powder, root bark of tree peony extraction residue is added into Zanthoxylum essential oil process residues freeze-dried powder to freeze
Powder and Mi leaves immersion wood powder, stand 2-3h after being sufficiently mixed, produce powder I；
(2) PVPP, oxytetracycline calcium and calamine stone are added into modified coal ash, and it is mixed to be warming up to 80-90 DEG C of insulation
5-10min is closed, room temperature is then naturally cooled to, produces powder II；
(3) powder II, pre-gelatinized pueraria starch and saleratus power are added into powder I, gained mixture is passed through after being sufficiently mixed
Vacuum compression is blocking, is eventually fabricated granularity 1-2mm particle.
6. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 1, it is characterised in that：
The modified coal ash is formed by flyash through microwave modification, and its method of modifying is：Turpentine oil and hydrogenation are added into flyash
Pentalyn, is sufficiently mixed after microwave treatment 3-5min under microwave frequency 2450MHz, power 700W, adds ten
Six alkyl trimethyl ammonium bromides and erucyl amide, continue microwave treatment 3-5min after being well mixed, then naturally cool to room temperature,
Gained mixture is cooled to -10 DEG C with 10 DEG C/min cooling rate, and powder is made in last size-reduced machine, produces modified fine coal
Ash.
7. oilseed storage auxiliary agent prepared by utilization Zanthoxylum essential oil process residues according to claim 6, it is characterised in that：
The flyash, turpentine oil, hydrogenated rosin pentaerythritol ester, the quality consumption of cetyl trimethylammonium bromide and erucyl amide
Than for 15-20:0.5-1:1-2:0.5-1:0.3-0.5.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710265109.1A CN107094880A (en) | 2017-04-21 | 2017-04-21 | Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710265109.1A CN107094880A (en) | 2017-04-21 | 2017-04-21 | Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues |
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| Publication Number | Publication Date |
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| CN107094880A true CN107094880A (en) | 2017-08-29 |
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ID=59656636
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710265109.1A Pending CN107094880A (en) | 2017-04-21 | 2017-04-21 | Oilseed storage auxiliary agent prepared by a kind of utilization Zanthoxylum essential oil process residues |
Country Status (1)
| Country | Link |
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| CN (1) | CN107094880A (en) |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106172377A (en) * | 2016-06-30 | 2016-12-07 | 全椒县大墅镇刘邦家庭农场 | A kind of legume-seeds storage mothproof mildew preventive |
-
2017
- 2017-04-21 CN CN201710265109.1A patent/CN107094880A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106172377A (en) * | 2016-06-30 | 2016-12-07 | 全椒县大墅镇刘邦家庭农场 | A kind of legume-seeds storage mothproof mildew preventive |
Non-Patent Citations (1)
| Title |
|---|
| 张强: "《面粉质量检测验收标准与生产加工工艺流程新技术实用手册》", 31 August 2003, 北京电子出版物出版中心 * |
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