CN107088402A - The preparation method of environment friendly biological adsorbent - Google Patents

The preparation method of environment friendly biological adsorbent Download PDF

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Publication number
CN107088402A
CN107088402A CN201710506770.7A CN201710506770A CN107088402A CN 107088402 A CN107088402 A CN 107088402A CN 201710506770 A CN201710506770 A CN 201710506770A CN 107088402 A CN107088402 A CN 107088402A
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CN
China
Prior art keywords
preparation
environment friendly
friendly biological
biological adsorbent
boiling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Application number
CN201710506770.7A
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Chinese (zh)
Inventor
张佳佳
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Individual
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Individual
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Publication date
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Priority to CN201710506770.7A priority Critical patent/CN107088402A/en
Publication of CN107088402A publication Critical patent/CN107088402A/en
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    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D53/00Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01JCHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2257/00Components to be removed
    • B01D2257/70Organic compounds not provided for in groups B01D2257/00 - B01D2257/602
    • BPERFORMING OPERATIONS; TRANSPORTING
    • B01PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01DSEPARATION
    • B01D2258/00Sources of waste gases
    • B01D2258/06Polluted air

Abstract

The invention discloses a kind of preparation method of environment friendly biological adsorbent, it is using the fiber and pericarp of plant or fruits and vegetables as primary raw material, sequentially pass through get the raw materials ready, boiling, squeezing, rinsing, alkaline reaction, the step such as drying and crushing are prepared from, raw material sources of the invention are extensively, cheap and easy to get, the recycling of discarded object can be realized, preparation process is simple, and process is easily controllable, easy to operate, the adsorbent of preparation is loose porous, advantages of good adsorption effect.The present invention is suitable as adsorbent and is used for adsorbing gas with foreign flavor or formaldehyde.

Description

The preparation method of environment friendly biological adsorbent
Technical field
The invention belongs to family expenses absorbent fields, it is related to a kind of preparation method of environment friendly biological adsorbent.
Background technology
Indoor air pollutants include some indoor toxic and harmful gas, such as formaldehyde, benzene, ammonia, oxycarbide.Formaldehyde is made One of major pollutants for room air, are also the pollution pollutant that most universal, most serious, people most pay close attention to, and it originates wide It is general.Domestic and international numerous studies show that a large amount of ornament materials, furniture and the coating used in fitment process is room air pollution Main release source, such as building structural materials and ornament materials.Formaldehyde is primarily present in the deep of ornament materials, with release speed Degree is slow, and the feature such as release time length, current adhesive is various in style, in decoration using it is most be arteries and veins urea formaldehyde, mainly Urea and formaldehyde condensation reaction are formed, and it is the main reason for causing formaldehyde in indoor air exceeded.
With the improvement of people's life quality, the problem of indoor air purification turns into people's general concern.And formaldehyde is made For the number one killer of room air, the huge concern of people is caused.It is able to can be sent out in furniture in room, such as cabinet, bookcase Go out formaldehyde, and the volatilization of formaldehyde is a slow process.The formaldehyde of Long Term Contact low concentration, can be caused very to human health Big threat.So solving the most important thing that Formaldehyde Pollution of Indoor Air is Indoor Environment Treatment.
At present, the domestic method except formaldehyde mainly uses the pure PARA FORMALDEHYDE PRILLS(91,95) of some activated carbons sold on the market, diatom to carry out Absorption, but the cost of these materials is higher, and their absorption is limited, easily causes secondary pollution.Therefore I Can be using this not only economical and practical but also healthy material of fragrant citrus pericarp come formaldehyde adsorption.In life we have seen that fragrant citrus pericarp lettuce Bamboo shoot leaf, watermelon peel etc. are not used effectively, and it is both twice laid to be utilized to formaldehyde adsorption, is conducive to human health again.
The content of the invention
In view of the shortcomings of the prior art, the invention provides a kind of preparation method of environment friendly biological adsorbent, raw material sources are extensive, It is cheap and easy to get, the recycling of discarded object can be realized, preparation process is simple, and process is easily controllable, easy to operate, preparation Adsorbent is loose porous, advantages of good adsorption effect.
Technical problem solved by the invention is realized using following technical scheme:
A kind of preparation method of environment friendly biological adsorbent, it is carried out successively according to steps order:
(1)Get the raw materials ready
It is material to choose watermelon peel, fragrant citrus pericarp, sleeve skin, big wheat husk, straw, and segment or fritter are cut into after being cleaned, is obtained A;
(2)Boiling
A is placed in boiling 50min in boiling water;Obtain B;
(3)Squeezing
B is placed in beater, material slag is squeezed into, obtains C;
(4)Rinsing
C is filtered, and is taken filter residue to be rinsed with circulating water to neutrality, is obtained D;
(5)Alkaline reaction
By the cornstarch of D weight 1/2 and the water of D weight 1/2 in pot, it is gelatinized at 30 DEG C;
Take D to be soaked in the alkali lye that PH is 12, add dextrin, in the lower reaction 6h of 60 DEG C of stirrings, obtain E;
In this step, graft reaction occurs for rich fibrous filter residue and the corn of gelatinization, generates the vapour with spatial networks The spacial framework in oilhole road;
(6)Dry
It is placed in after E is taken out in drying box in drying 24h at 80 DEG C, obtains F;
(7)Crush
After F is crushed, produce.
It is used as the restriction of the present invention:
Step(5)In, described alkali lye is NaOH;
Step(5)In, described gelatinization time is 20min.
The present invention also has a kind of restriction, step(7)In, 100 mesh sieves are crossed after crushing.
Compared with prior art, the advantage of the invention is that:The preparation method for the environment friendly biological adsorbent that the present invention is provided, Raw material sources are extensively, cheap and easy to get, can realize the recycling of discarded object, and preparation process is simple, and process is easily controllable, behaviour Make easy, the adsorbent of preparation is loose porous, advantages of good adsorption effect.
The present invention is applied to gas with foreign flavor and formaldehyde in adsorption chamber.
Embodiment
In order that technological means, creation characteristic, workflow, application method reached purpose and effect of the present invention are easy to bright It is white to understand, the present invention is further elucidated below.
A kind of preparation method of environment friendly biological adsorbent of embodiment 1
A kind of preparation method of environment friendly biological adsorbent of the present embodiment, it is carried out successively according to steps order:
(1)Get the raw materials ready
It is material to choose watermelon peel, fragrant citrus pericarp, sleeve skin, big wheat husk, straw, and segment or fritter are cut into after being cleaned, is obtained A;
(2)Boiling
A is placed in boiling 50min in boiling water;Obtain B;
(3)Squeezing
B is placed in beater, material slag is squeezed into, obtains C;
(4)Rinsing
C is filtered, and is taken filter residue to be rinsed with circulating water to neutrality, is obtained D;
(5)Alkaline reaction
Take 15g cornstarch and 15g water in pot, be gelatinized 20min at 30 DEG C;
Take 30g D to be soaked in the NaOH alkali lye that PH is 12, add dextrin, in the lower reaction 6h of 60 DEG C of stirrings, obtain E;
In this step, graft reaction occurs for rich fibrous filter residue and the corn of gelatinization, generates the vapour with spatial networks The spacial framework in oilhole road;
(6)Dry
It is placed in after E is taken out in drying box in drying 24h at 80 DEG C, obtains F;
(7)Crush
F is crushed, 100 mesh sieves are crossed after crushing and are produced.
The preparation method for the environment friendly biological adsorbent that the present embodiment is provided, raw material sources are extensively, cheap and easy to get, can realize The recycling of discarded object, preparation process is simple, and process is easily controllable, easy to operate, and the adsorbent of preparation is loose porous, inhales Attached effect is good.
Above-described embodiment, is only presently preferred embodiments of the present invention, is not other forms made for the present invention Limit, any those skilled in the art are changed or be modified as enlightenment possibly also with above-mentioned technology contents equivalent The equivalent embodiment of change.In every case it is the technical spirit without departing from the claims in the present invention, the letter to made by above example Single modification, equivalent variations and remodeling, still fall within the scope of the claims in the present invention protection.

Claims (4)

1. a kind of preparation method of environment friendly biological adsorbent, it is characterised in that:It is carried out successively according to steps order:
(1)Get the raw materials ready
It is material to choose watermelon peel, fragrant citrus pericarp, sleeve skin, big wheat husk, straw, and segment or fritter are cut into after being cleaned, is obtained A;
(2)Boiling
A is placed in boiling 50min in boiling water;Obtain B;
(3)Squeezing
B is placed in beater, material slag is squeezed into, obtains C;
(4)Rinsing
C is filtered, and is taken filter residue to be rinsed with circulating water to neutrality, is obtained D;
(5)Alkaline reaction
By the cornstarch of D weight 1/2 and the water of D weight 1/2 in pot, it is gelatinized at 30 DEG C;
Take D to be soaked in the alkali lye that PH is 12, add dextrin, in the lower reaction 6h of 60 DEG C of stirrings, obtain E;
(6)Dry
It is placed in after E is taken out in drying box in drying 24h at 80 DEG C, obtains F;
(7)Crush
After F is crushed, produce.
2. the preparation method of environment friendly biological adsorbent according to claim 1, it is characterised in that:Step(5)In, it is described Alkali lye is NaOH.
3. the preparation method of environment friendly biological adsorbent according to claim 1, it is characterised in that:Step(5)In, it is described Gelatinization time is 20min.
4. the preparation method of the environment friendly biological adsorbent according to any one in claim 1-3, it is characterised in that:Step (7)In, 100 mesh sieves are crossed after crushing.
CN201710506770.7A 2017-06-28 2017-06-28 The preparation method of environment friendly biological adsorbent Withdrawn CN107088402A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201710506770.7A CN107088402A (en) 2017-06-28 2017-06-28 The preparation method of environment friendly biological adsorbent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201710506770.7A CN107088402A (en) 2017-06-28 2017-06-28 The preparation method of environment friendly biological adsorbent

Publications (1)

Publication Number Publication Date
CN107088402A true CN107088402A (en) 2017-08-25

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201710506770.7A Withdrawn CN107088402A (en) 2017-06-28 2017-06-28 The preparation method of environment friendly biological adsorbent

Country Status (1)

Country Link
CN (1) CN107088402A (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108014624A (en) * 2018-01-11 2018-05-11 史书亭 The preparation method of green smell scavenger and its application method and its application

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108014624A (en) * 2018-01-11 2018-05-11 史书亭 The preparation method of green smell scavenger and its application method and its application

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Application publication date: 20170825