CN107057835A - A kind of production method of the cosmetic oil based on almond benevolence - Google Patents

A kind of production method of the cosmetic oil based on almond benevolence Download PDF

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Publication number
CN107057835A
CN107057835A CN201710250934.4A CN201710250934A CN107057835A CN 107057835 A CN107057835 A CN 107057835A CN 201710250934 A CN201710250934 A CN 201710250934A CN 107057835 A CN107057835 A CN 107057835A
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almond
ethanol
ethyl acetate
extraction
oil
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CN201710250934.4A
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Inventor
彭红
郑洪立
张锦胜
巫小丹
王允圃
刘玉环
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Nanchang University
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Nanchang University
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
    • A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/02—Pretreatment
    • C11B1/04—Pretreatment of vegetable raw material
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/104—Production of fats or fatty oils from raw materials by extracting using super critical gases or vapours
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B1/00—Production of fats or fatty oils from raw materials
    • C11B1/10—Production of fats or fatty oils from raw materials by extracting
    • C11B1/108—Production of fats or fatty oils from raw materials by extracting after-treatment, e.g. of miscellae
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00—Preserving by using additives, e.g. anti-oxidants
    • C11B5/0021—Preserving by using additives, e.g. anti-oxidants containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00—Preserving by using additives, e.g. anti-oxidants
    • C11B5/0021—Preserving by using additives, e.g. anti-oxidants containing oxygen
    • C11B5/0035—Phenols; Their halogenated and aminated derivates, their salts, their esters with carboxylic acids
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00—Preserving by using additives, e.g. anti-oxidants
    • C11B5/0042—Preserving by using additives, e.g. anti-oxidants containing nitrogen
    • C11B5/0064—Heterocyclic compounds containing nitrogen in the ring
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00—Preserving by using additives, e.g. anti-oxidants
    • C11B5/0085—Substances of natural origin of unknown constitution, f.i. plant extracts
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B5/00—Preserving by using additives, e.g. anti-oxidants
    • C11B5/0092—Mixtures
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
    • A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
    • A61K2800/52—Stabilizers
    • A61K2800/522—Antioxidants; Radical scavengers

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
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  • Botany (AREA)
  • Dermatology (AREA)
  • Cosmetics (AREA)

Abstract

A kind of production method of the cosmetic oil based on almond benevolence, belongs to cosmetics processing technique field.The present invention by almond benevolence by drying, be crushed to certain particle size；Add after ethanol and the pretreatment of ethyl acetate microwave radiation technology, supercritical CO is carried out using ethanol and ethyl acetate as entrainer2Extraction, pressure is extraction under the conditions of 20~30MPa, 45~50 DEG C of temperature；Then separated in knockout drum at pressure 3MPa~6MPa, 25~30 DEG C of temperature.After reclaiming ethanol and ethyl acetate through vacuum distillation, extraction oil obtains anti-oxidant almond oil by adding carnosine, Tea Polyphenols and lycopene composite antioxidant after solubilising.Extraction rate of the present invention is fast, recovery rate is high, no solvent residue, and the high quality oils water activity of acquisition is low, with anti-oxidant and vegetative cell function, and water retention property and Storage are all good, can be used as in cosmetics of super quality base starting material.

Description

A kind of production method of the cosmetic oil based on almond benevolence
Technical field
The invention belongs to cosmetics processing technique field, it is related to the production method of cosmetic oil.
Background technology
General principle：Almond benevolence fat oil about oil-containing 55-61%, protein 28%, starch, sugar 10-11%, and contain A small amount of vitamin A, B1, B2 and digestive ferment, the plain enzyme of almond, almond into, calcium, magnesium, sodium, potassium, it is simultaneously micro- containing 18 kinds of iron, cobalt etc. Secondary element.Etc..Simultaneously as containing abundant carrotene, free radical invasion cell is prevented, the effect with pre- preventing tumor. Therefore, multiple biological activities composition is contained in almond oil, for cosmetics can make soft lubrication, skin nutrition cell work With.The effects such as lycopene can promote the growth and regeneration of cell, beauty Eradicates wrinkles, maintenance skin health, anti-aging, can be significantly Improve skin allergy, eliminate dry skin and scratchiness because caused by allergic, make us feeling relaxed happy.Carnosine can Removing makes active oxygen radical formed by the aliphatic acid over oxidation of cell membrane during oxidative stress（ROS）And alpha-beta Unsaturated aldehyde.The effect that the aging and skin that skin can be prevented are brightened, carnosine can prevent free radical from producing, and repair skin and damage Wound, the function with vegetative cell.
The principle of microwave treatment is to penetrate spe medium using frequency electromagnetic waves, reaches the inside for being extracted material, microwave Heat energy can be quickly converted to and make the temperature rapid increase of cell interior.When the pressure of cell interior exceedes the ability to bear of cell When, cell will rupture, and active ingredient is i.e. from intracellular outflow, and be dissolved in spe medium at a lower temperature.
Supercritical CO2The principle of fluid extraction separation is the relation of the solvability using supercritical fluid and its density, Influence i.e. using pressure and temperature to supercritical fluid solvability and extract.In the supercritical state, will be overcritical Fluid is contacted with material to be separated, make its selectively polarity size, boiling point height it is different with molecular size range into Divide and extract successively.Certainly, the extract obtained by each pressure limit of correspondence is unlikely to be single, but can be with control condition The blending constituent of optimal proportion is obtained, then supercritical fluid is become common gases by the method for decompression, heating, is extracted Material is then wholly or substantially separated out, so that the purpose of separating-purifying is reached, so supercritical CO2Fluid extraction process is by extracting Combined with separation process.Supercritical CO2The sharpest edges of fluid extraction are no solvent residues, and natural active matter is obtained It is effectively maintained.In the present invention, ethanol and ethyl acetate are in supercritical CO2Play entrainer during fluid extraction, Extraction efficiency can be improved.And different from general organic solvent, provide that ethanol and ethyl acetate are fair according to GB 2760-96 Perhaps the flavorant used, for cosmetics more without toxic side effect.Extraction under the conditions of 45-60 DEG C, high vacuum carry out The recyclable ethanol of vacuum distillation and ethyl acetate obtain product.The grease extracted at the process conditions has the same of bioactivity When, its antioxidation activity is low, easy oxidation deterioration.Carnosine, Tea Polyphenols and tomato red have extraordinary antioxygenic property, three Also there is synergy in the presence of simultaneously, antioxidation activity is greatly improved.But carnosine and Tea Polyphenols do not dissolve in grease, kind Lycopene is water insoluble, it is impossible to which three is directly added into grease, finds carnosine and Tea Polyphenols being dissolved in after water by studying, plus The binary compound emulsifying agent for entering HLB value 5-6 monoglyceride and HLB value 12-15 nonionic polyoxyethylene monolaurate can To promote lycopene to dissolve, add in grease and form the particulate of Water-In-Oil and dispersed, effect very well, then uses ultrasonic wave Concussion is uniformly mixed so as to obtain the almond oil with antioxidation activity high bioactivity, and it contains abundant nutriment, can be used as The matrix of cosmetic.
The content of the invention
It is an object of the invention to provide a kind of production method of the cosmetic oil based on almond benevolence, for producing cosmetics Matrix oil.Supercritical CO after being pre-processed by microwave radiation technology2Fluid extraction almond oil, addition carnosine, Tea Polyphenols and kind Lycopene improves antioxidation activity, obtains the active almond oil of antioxidation biology of functionalization.
The present invention by almond benevolence by drying, being crushed to after certain particle size；Add ethanol and ethyl acetate microwave radiation technology is pre- Processing, uses supercritical CO under certain process conditions afterwards2Second is reclaimed in fluid extraction vegetable oil and active ingredient, vacuum distillation After alcohol and ethyl acetate, then using raising antioxidation activities such as certain method addition Tea Polyphenols, obtain high with antioxidation activity The almond oil of bioactivity.Main advantages of the present invention are supercritical COs at the process conditions2It is flat obtained by fluid extraction Persic oil, bioactive substance content is high, loses small.Adding has well anti-oxidant after carnosine, Tea Polyphenols and lycopene Characteristic, grease produced by the invention can make the matrix oil of cosmetics, contain a large amount of bioactivity and nutriment.
The present invention is achieved by the following technical solutions.
A kind of production method of cosmetic oil based on almond benevolence of the present invention, as follows.
1）By almond benevolence by drying, be crushed to certain particle size.
2）Ethanol and the pretreatment of ethyl acetate microwave radiation technology.
3）Using ethanol and ethyl acetate as entrainer supercritical CO2Fluid extraction.
4）Ethanol and ethyl acetate are reclaimed in vacuum distillation.
5）Add carnosine, Tea Polyphenols and lycopene and improve anti-oxidation characteristics.
The microwave radiation technology pretreatment, refers to and is handled 5-10 minutes in 2450MHz with Microwave Extraction reaction system.
The supercritical CO2Fluid extraction, refers in extractor under the conditions of pressure is 20~30MPa, 45~50 DEG C of temperature Extraction；Separated in knockout drum at pressure 3MPa~5MPa, 25~30 DEG C of temperature.
The raising inoxidizability.Refer to and carnosine and Tea Polyphenols are dissolved in distilled water, add HLB value 5-6 monoglyceride and HLB The binary compound emulsifying agent of value 12-15 nonionic polyoxyethylene monolaurate, adds lycopene and heats 30-40 DEG C, It is allowed to be completely dissolved, above-mentioned solution is slowly added dropwise into the 4th）Walk in the almond oil obtained by extraction and quickly stir, be dispersed into Uniform single-phase oily liquids, is mixed with ultrasonic oscillation；Carnosine, Tea Polyphenols and the lycopene total content in grease（Quality Than）It is not less than 0.01%, obtains the active almond oil of antioxidation biology of functionalization.
The main principle steps of the present invention：1. by almond benevolence by drying, be crushed to certain particle size；2. ethanol and acetic acid second Ester microwave radiation technology is pre-processed；3. carry out supercritical CO using ethanol and ethyl acetate as entrainer in certain process conditions2Fluid extracts Take.4. ethanol and ethyl acetate are reclaimed in vacuum distillation；5. adding carnosine, Tea Polyphenols and lycopene improves anti-oxidation characteristics.With The major advantage of this method is supercritical CO at the process conditions2Almond oil obtained by fluid extraction, bioactive substance Content is high, loses small, adding has high anti-oxidation characteristic after carnosine, Tea Polyphenols and lycopene, improves storage phase, prevents from becoming Matter.The grease of this method production can make the matrix oil of cosmetics, contain a large amount of bioactivity and nutriment.
Beneficial effects of the present invention：The present invention provides a kind of objectively high bioactivity cosmetics with antioxidation activity With the production method of oil.This method can efficiently extract high activity almond oil with objective, have compared to solvent extraction without molten The characteristic of agent residual, has high anti-oxidation activity by adding composite antioxidant, can be used for the life of cosmetic base oil Production.
Embodiment
The present invention will be described further by following examples.
Microwave Extraction reaction system used in the embodiment of the present invention is the SOS-1100 series of products of French PR OLABO companies, Supercritical CO used2Equipment is the U.S. morning 300L type in Guangzhou.
Embodiment 1.
1）By almond benevolence by drying, be crushed to 30 mesh sieve.
2）Ethanol and ethyl acetate submergence are added, is handled 5-10 minutes in 2450MHz with Microwave Extraction reaction system.
3）Then by said mixture supercritical CO2Equipment extracts 3h, extraction conditions：In extractor pressure be 25MPa, Extracted under the conditions of 45~50 DEG C of temperature；Separated in knockout drum at pressure 3MPa, 25 DEG C of temperature.
4）The lipidic compounds that 3) step is obtained, are vacuumized at 40-50 DEG C, and ethanol and ethyl acetate are reclaimed in vacuum distillation.
5) inoxidizability will be improved.Carnosine and Tea Polyphenols are dissolved in distilled water, HLB value 5-6 monoglyceride and HLB value is added The binary compound emulsifying agent of 12-15 nonionic polyoxyethylene monolaurate, adds lycopene and heats 30-40 DEG C, make Be completely dissolved, above-mentioned solution is slowly added dropwise into the 3rd）Walk in the almond oil obtained by extraction and quickly stir, be dispersed into Even single-phase oily liquids, is mixed with ultrasonic oscillation；Carnosine, Tea Polyphenols and the lycopene total content in grease（Mass ratio） It is not less than 0.01%, obtains the active almond oil of antioxidation biology of functionalization.
Embodiment 2.
1）By almond benevolence by drying, be crushed to 30 mesh sieve.
2）Ethanol and ethyl acetate submergence are added, is handled 8 minutes in 2450MHz with Microwave Extraction reaction system.
3）Then by said mixture supercritical CO2Equipment extracts 2h, extraction conditions：In extractor pressure be 25MPa, Extracted under the conditions of temperature 45 C；Separated in knockout drum at pressure 3MPa, 25 DEG C of temperature.
4）The lipidic compounds that 3) step is obtained, are vacuumized at 50 DEG C, and ethanol and ethyl acetate are reclaimed in vacuum distillation.
5) inoxidizability will be improved.Carnosine and Tea Polyphenols are dissolved in distilled water, HLB value 5-6 monoglyceride and HLB value is added The binary compound emulsifying agent of 12-15 nonionic polyoxyethylene monolaurate, adds lycopene and heats 40 DEG C, be allowed to Fully dissolved, above-mentioned solution is slowly added dropwise into the 4th）Walk in the almond oil obtained by extraction and quickly stir, be dispersed into uniform Single-phase oily liquids, is mixed with ultrasonic oscillation；Carnosine, Tea Polyphenols and the lycopene total content in grease（Mass ratio）It is not low In 0.3%, the active almond oil of antioxidation biology of functionalization is obtained.

Claims (1)

1. a kind of production method of the cosmetic oil based on almond benevolence, it is characterized in that as follows：
（1）By almond benevolence by drying, be crushed to certain particle size；
（2）Appropriate ethanol and ethyl acetate is added in the almond benevolence of crushing, Microwave Pretreatment 3-10 minutes breaks cell Wall；
（3）By step（2）The mixture of gained uses supercritical CO using ethanol and ethyl acetate as entrainer2With pressure in extractor Extracted under the conditions of 20~30MPa of power, 45~50 DEG C of temperature；Then with pressure 3MPa~4MPa, temperature in knockout drum Separated at 25~30 DEG C；
（4）By step（3）Grease is obtained, at 45-60 DEG C, pumping high vacuum carries out vacuum distillation and reclaims removing ethanol and acetic acid second Ester, obtains almond oil；
（5）Carnosine and Tea Polyphenols are dissolved in distilled water, HLB value 5-6 monoglyceride is added and the non-ionic of HLB value 12-15 is gathered The binary compound emulsifying agent of oxygen ethene monolaurate, adds lycopene and heats 30-40 DEG C, be allowed to be completely dissolved, will be above-mentioned Solution is slowly added dropwise into step（4）Stir in almond oil obtained by extraction and quickly, be dispersed into uniform single-phase oily liquids, Mixed with ultrasonic oscillation；Carnosine, Tea Polyphenols and the lycopene mass ratio of total content in grease are not less than 0.01%, obtain The active almond oil of the antioxidation biology of functionalization.
CN201710250934.4A 2017-04-18 2017-04-18 A kind of production method of the cosmetic oil based on almond benevolence Withdrawn CN107057835A (en)

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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111437231A (en) * 2020-04-18 2020-07-24 北温草生物科技(上海)有限公司 Chinese herbal medicine composition for resisting wrinkles and resisting aging

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111437231A (en) * 2020-04-18 2020-07-24 北温草生物科技(上海)有限公司 Chinese herbal medicine composition for resisting wrinkles and resisting aging

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