CN107033959A - Pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling - Google Patents
Pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling Download PDFInfo
- Publication number
- CN107033959A CN107033959A CN201710242334.3A CN201710242334A CN107033959A CN 107033959 A CN107033959 A CN 107033959A CN 201710242334 A CN201710242334 A CN 201710242334A CN 107033959 A CN107033959 A CN 107033959A
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- China
- Prior art keywords
- chlorinated paraffin
- kettle
- production method
- air cooling
- paraffin
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Title of the present invention is that pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling, belong to chlorinated paraffin technical field, in order to improve chlorinated paraffin speed of production, based on it is improved former 87106851.6 patent adopt the technical scheme that pressure increases to 1 kg/cm in kettle, install light source in kettle additional, heat exchangers in series between cyclic part and agitation device, starting paraffin is heated to certain temperature (110 DEG C or so), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then chlorination in input kettle, and ensure polyethylene as fusing shape using heat, a kind of faster production method is provided.
Description
(1) technical field：The present invention relates to a kind of method for producing Modified Chlorinated Paraffin -70.
(2) background technology：" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.：87106851.6) its
Technical scheme is：By chlorine feeding reactor space, the hydrogen chloride gas of chlorine and reaction generation is extracted out, through jet pump and reservoir
Groove, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device, so continuous fast reaction.But for producing chlorinated paraffin speed also not
Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention：The task of the present invention be based on to former 87106851.6 patent of invention it is a kind of improve there is provided
A kind of method of faster production Modified Chlorinated Paraffin -70, adopts the technical scheme that device is improved in pressure, kettle and installs glazing additional
Source, so agitates lower raising reaction speed in forced circulation.The heat exchangers in series between device agitation device and cyclic part outlet,
Agitation device is passed through after the reacting gas for entering agitation device is first heated or cooled down, it is ensured that optimal reaction temperature, raw material
Heating paraffin is to certain temperature (110 DEG C or so), and then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage,
Then chlorination in input kettle, and ensure polyethylene as fusing shape using heat.
(4) embodiment：A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactions
Kettle, makes pressure in device bring up to 1 kg/cm, installs 1000 watts of mercury lamps in its reactor additional.With 2.5 meters of heat-transfer surface2's
Heat exchanger is connected between agitation device and cyclic part outlet, starting paraffin is heated to certain temperature (110 DEG C or so), then
By a certain percentage (5% or so) add polyethylene carry out heating fusing, then put into kettle in chlorination, and using heat ensure polyethylene as
Melt shape.
With " equipment for preparation of paraffin chloride by forced circulating blast method " together, material temperature is low for present invention operation, and heat exchanger heating is on the contrary
Cooling.
Claims (1)
1. one kind pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin -70 of air cooling, including chlorine and hydrogen chloride gas
Body is extracted out, and hydrogen chloride gas is only absorbed by the water in jet pump and hopper, and remaining chlorine drum is pressed into agitation device, and so continuous, it is special
Levying is：Increase reaction pressure, kettle is built with light source chlorination, heat exchangers in series between agitation device and cyclic part outlet, to reaction
Gas is heated or cooled, and starting paraffin is heated to certain temperature (110 DEG C or so), and then (5% or so) adds by a certain percentage
Enter polyethylene and carry out heating fusing, then put into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242334.3A CN107033959A (en) | 2017-04-04 | 2017-04-04 | Pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242334.3A CN107033959A (en) | 2017-04-04 | 2017-04-04 | Pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107033959A true CN107033959A (en) | 2017-08-11 |
Family
ID=59535950
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710242334.3A Withdrawn CN107033959A (en) | 2017-04-04 | 2017-04-04 | Pressurization Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107033959A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN106047408A (en) * | 2016-05-01 | 2016-10-26 | 林群祥 | Method for producing chlorinated paraffin-70 by pressurization photo-chlorination agitation gas cooling-heating method |
-
2017
- 2017-04-04 CN CN201710242334.3A patent/CN107033959A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN106047408A (en) * | 2016-05-01 | 2016-10-26 | 林群祥 | Method for producing chlorinated paraffin-70 by pressurization photo-chlorination agitation gas cooling-heating method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170811 |
|
| WW01 | Invention patent application withdrawn after publication |