CN107011943A - Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling - Google Patents
Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling Download PDFInfo
- Publication number
- CN107011943A CN107011943A CN201710242333.9A CN201710242333A CN107011943A CN 107011943 A CN107011943 A CN 107011943A CN 201710242333 A CN201710242333 A CN 201710242333A CN 107011943 A CN107011943 A CN 107011943A
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- CN
- China
- Prior art keywords
- chlorinated paraffin
- production method
- air cooling
- kettle
- modified chlorinated
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
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- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Title of the present invention is that Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling, belong to chlorinated paraffin technical field, in order to improve the speed of production of chlorinated paraffin 70, upper light source is installed in kettle additional based on improving it to former 87106851.6 patent and adopting the technical scheme that, heat exchangers in series between cyclic part and agitation device, starting paraffin is heated to certain temperature (110 DEG C or so), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then chlorination in input kettle, and ensure polyethylene as fusing shape using heat, a kind of faster production method is provided.
Description
(1) technical field：The present invention relates to a kind of method for producing Modified Chlorinated Paraffin -70.
(2) background technology：" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.：87106851.6) its
Technical scheme is：By chlorine feeding reactor space, the hydrogen chloride gas of chlorine and reaction generation is extracted out, through jet pump and reservoir
Groove, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device, so continuous fast reaction.But for producing chlorinated paraffin speed also not
Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention：The task of the present invention be based on to former 87106851.6 patent of invention it is a kind of improve there is provided
A kind of method of faster production Modified Chlorinated Paraffin -70, adopts the technical scheme that and installs light source in kettle additional, agitated in device
Heat exchangers in series between device and cyclic part outlet, is passed through after the reacting gas for entering agitation device is first heated or cooled down
Starting paraffin, is heated to certain temperature (110 DEG C or so), then by a certain percentage by agitation device, it is ensured that optimal reaction temperature
(5% or so) add polyethylene and carry out heating fusing, then put into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
(4) embodiment：A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactions
Install 1000 watts of mercury lamps in kettle, its reactor additional.With 2.5 meters of heat-transfer surface2Heat exchanger be connected on agitation device and cyclic part and export
Between, starting paraffin is heated to certain temperature (110 DEG C or so), then (5% or so) addition polyethylene enters by a certain percentage
Row heating fusing, then puts into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
With " equipment for preparation of paraffin chloride by forced circulating blast method " together, material temperature is low for present invention operation, and heat exchanger heating is on the contrary
Cooling.
Claims (1)
1. a kind of Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin -70 of air cooling, including chlorine and hydrogen chloride gas are taken out
Go out, hydrogen chloride gas is only absorbed by the water in jet pump and hopper, remaining chlorine drum is pressed into agitation device, so continuous, it is characterized in that：
Kettle is built with light source chlorination, and heat exchangers in series between agitation device and cyclic part outlet reacting gas is heated or cooled, original
Work stone wax is heated to certain temperature (110 DEG C or so), and then the progress heating of (5% or so) addition polyethylene is molten by a certain percentage
Change, then put into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242333.9A CN107011943A (en) | 2017-04-04 | 2017-04-04 | Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242333.9A CN107011943A (en) | 2017-04-04 | 2017-04-04 | Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107011943A true CN107011943A (en) | 2017-08-04 |
Family
ID=59445462
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710242333.9A Withdrawn CN107011943A (en) | 2017-04-04 | 2017-04-04 | Light chlorimation agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107011943A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN106010646A (en) * | 2016-05-01 | 2016-10-12 | 林群祥 | Method for producing chlorinated paraffin-70 in light chlorination propelling gas cold-heat mode |
-
2017
- 2017-04-04 CN CN201710242333.9A patent/CN107011943A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN106010646A (en) * | 2016-05-01 | 2016-10-12 | 林群祥 | Method for producing chlorinated paraffin-70 in light chlorination propelling gas cold-heat mode |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170804 |