CN105950216A - Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method - Google Patents
Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method Download PDFInfo
- Publication number
- CN105950216A CN105950216A CN201610308909.2A CN201610308909A CN105950216A CN 105950216 A CN105950216 A CN 105950216A CN 201610308909 A CN201610308909 A CN 201610308909A CN 105950216 A CN105950216 A CN 105950216A
- Authority
- CN
- China
- Prior art keywords
- chlorinated paraffin
- chlorine
- bubbler
- gas cooling
- bubbling
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The invention provides a method for producing chlorinated paraffin-70 with a bubbling agitating gas cooling or heating method and belongs to the technical field of chlorinated paraffin. Aiming at increasing production speed of chlorinated paraffin-70, the technical scheme adopted by an original 87106851.6 patent is improved as follows: a bubbler is additionally mounted in a device kettle provided in the 87106851.6 patent, chlorine is directly introduced into the bubbler, a heat exchanger is connected in series between a cycle part and the bubbler, and one faster production method is provided.
Description
(1) technical field: the present invention relates to a kind of method producing chlorinated paraffin-70.
(2) background technology: " equipment for preparation of paraffin chloride by forced circulating blast method " (the former patent No.:
87106851.6) its technical scheme is: chlorine is sent into what reactor space, chlorine and reaction generated
Hydrogen chloride gas is extracted out, through ejector pump and hopper, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device,
Fast reaction the most continuously.But it is the most preferable to be used for producing chlorinated paraffin speed, especially produces height
Chlorinated paraffin product, to the reaction later stage, speed eases up.
(3) summary of the invention: the task of the present invention is based on to former 87106851.6 patents of invention
Plant and improve, it is provided that a kind of method of faster production chlorinated paraffin-70, adopt the technical scheme that
Separately add in its reactor and load onto bubbler, chlorine source the chlorine supplied is passed directly into bubbler, to reaction
Still material carries out bubbling.Under forced circulation is agitated, so add bubbling improve response speed.At dress
Put heat exchangers in series between agitation device and cyclic part outlet, advanced to the reacting gas entering agitation device
It is passed through agitation device, it is ensured that optimal reaction temperature after row heating or cooling.
(4) detailed description of the invention: a set of " equipment for preparation of paraffin chloride by forced circulating blast method ", makes
With 500 liters of reactors, add again in its reactor and load onto existing current bubbler.With heat-transfer surface 2.5
Rice2Heat exchanger be connected on agitation device and cyclic part outlet between.
Present invention operation is same with " equipment for preparation of paraffin chloride by forced circulating blast method ".Material temperature is low, changes
Hot device heats, on the contrary cooling.
Claims (1)
1. bubbling agitates air cooling full-boiled process to produce a chlorinated paraffin-70 method, including chlorine and chlorine
Changing hydrogen to extract out, hydrogen chloride gas is only absorbed by the water in ejector pump and hopper, and remaining chlorine drum is pressed into
Agitation device, the most continuously, is characterized in that: chlorine is directly placed into bubbler in still, agitation device and circulation
Heat exchangers in series between section port, is heated or cooled reacting gas.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610308909.2A CN105950216A (en) | 2016-05-01 | 2016-05-01 | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610308909.2A CN105950216A (en) | 2016-05-01 | 2016-05-01 | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN105950216A true CN105950216A (en) | 2016-09-21 |
Family
ID=56911347
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610308909.2A Pending CN105950216A (en) | 2016-05-01 | 2016-05-01 | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN105950216A (en) |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106957691A (en) * | 2017-04-04 | 2017-07-18 | 林群祥 | Bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN107057765A (en) * | 2017-04-04 | 2017-08-18 | 林群祥 | Directly agitate the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN108018124A (en) * | 2017-05-16 | 2018-05-11 | 林群祥 | Bubbling agitates hot -70 method of method production chlorination gutter oil of air cooling |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
-
2016
- 2016-05-01 CN CN201610308909.2A patent/CN105950216A/en active Pending
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN87106851A (en) * | 1987-10-06 | 1988-07-27 | 林群祥 | Equipment for preparation of paraffin chloride by forced circulating blast method |
Non-Patent Citations (1)
| Title |
|---|
| 汪多仁: "氯化石蜡-70的开发与应用", 《聚合物与助剂》 * |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106957691A (en) * | 2017-04-04 | 2017-07-18 | 林群祥 | Bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN107057765A (en) * | 2017-04-04 | 2017-08-18 | 林群祥 | Directly agitate the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
| CN108018124A (en) * | 2017-05-16 | 2018-05-11 | 林群祥 | Bubbling agitates hot -70 method of method production chlorination gutter oil of air cooling |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105838440A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination direct agitating gas heating and cooling method | |
| CN105950216A (en) | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method | |
| CN105925311A (en) | Method for producing chlorinated paraffin-70 through catalyzing, pressurizing and direct gas agitating cold-hot method | |
| CN105885942A (en) | Method for producing chlorinated paraffin-70 by catalyzing and direct gas agitating cold and hot type | |
| CN105838438A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing bubbling agitating gas heating and cooling method | |
| CN105838433A (en) | Pressurized direct bubbling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN105838434A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination bubbling agitating gas heating and cooling method | |
| CN105838436A (en) | Method for producing chlorinated paraffin-70 through catalytic bubbling agitating gas heating and cooling method | |
| CN106010644A (en) | Method for preparing chlorinated paraffin-70 with direct driving gas cold-heat method | |
| CN106010645A (en) | Method for producing chlorinated paraffin-70 in light chlorination direct propelling gas cold-heat mode | |
| CN105838435A (en) | Pressurized bubbling propelling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN106010646A (en) | Method for producing chlorinated paraffin-70 in light chlorination propelling gas cold-heat mode | |
| CN105838437A (en) | Light chlorination bubbling propelling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN106010647A (en) | Method for producing chlorinated paraffin-70 in catalysis propelling gas cold-heat mode | |
| CN105950215A (en) | Method for producing chlorinated paraffin-70 with agitating gas cooling or heating method adopting catalytic pressurization | |
| CN105950217A (en) | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method adopting pressurized photochlorination | |
| CN105838439A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination agitating gas heating and cooling method | |
| CN105925310A (en) | Method for producing chlorinated paraffin-70 through pressurizing and gas agitating cold-hot method | |
| CN106047408A (en) | Method for producing chlorinated paraffin-70 by pressurization photo-chlorination agitation gas cooling-heating method | |
| CN106987272A (en) | Pressurization Light chlorimation bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN105838441A (en) | Pressurized photochlorination direct bubbling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN106995721A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in catalysis pressurization | |
| CN107057765A (en) | Directly agitate the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN106929102A (en) | Method is directly agitated to produce Modified Chlorinated Paraffin method | |
| CN106957691A (en) | Bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20160921 |