CN107099331A - The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization - Google Patents
The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization Download PDFInfo
- Publication number
- CN107099331A CN107099331A CN201710242125.9A CN201710242125A CN107099331A CN 107099331 A CN107099331 A CN 107099331A CN 201710242125 A CN201710242125 A CN 201710242125A CN 107099331 A CN107099331 A CN 107099331A
- Authority
- CN
- China
- Prior art keywords
- chlorinated paraffin
- chlorine
- agitation device
- production method
- kettle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G73/00—Recovery or refining of mineral waxes, e.g. montan wax
- C10G73/38—Chemical modification of petroleum
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Title of the present invention is that the hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization, belong to chlorinated paraffin technical field, in order to improve the speed of production of chlorinated paraffin 70, based on it is improved former 87106851.6 patent adopt the technical scheme that reaction pressure increases to 1 kg/cm in kettle, chlorine source chlorine is directly placed into agitation device through heat exchanger, heat exchangers in series between cyclic part and agitation device, starting paraffin is heated to certain temperature (110 DEG C or so), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then chlorination in input kettle, and ensure polyethylene as fusing shape using heat, a kind of faster production method is provided.
Description
(1) technical field：The present invention relates to a kind of method for producing Modified Chlorinated Paraffin -70.
(2) background technology：" equipment for preparation of paraffin chloride by forced circulating blast method " (former patent No.：87106851.6) its
Technical scheme is：By chlorine feeding reactor space, the hydrogen chloride gas of chlorine and reaction generation is extracted out, through jet pump and reservoir
Groove, is only absorbed by the water, and remaining chlorine drum is pressed into agitation device, so continuous fast reaction.But for producing chlorinated paraffin speed also not
Enough ideals, especially produce high chlorinated paraffin product, and to the reaction later stage, speed eases up.
(3) content of the invention：The task of the present invention be based on to former 87106851.6 patent of invention it is a kind of improve there is provided
A kind of method of faster production Modified Chlorinated Paraffin -70, adopts the technical scheme that device improves reaction pressure, is supplied by chlorine source
The chlorine answered is passed directly into agitation device through heat exchanger, and material in reactor is agitated.In device agitation device and cyclic part
Heat exchangers in series between outlet, agitation device is passed through after the reacting gas for entering agitation device is first heated or cooled down, it is ensured that
Starting paraffin, is heated to certain temperature (110 DEG C or so) by optimal reaction temperature, and then (5% or so) is added by a certain percentage
Polyethylene carries out heating fusing, then puts into chlorination in kettle, and ensure polyethylene as fusing shape using heat.
(4) embodiment：A set of " equipment for preparation of paraffin chloride by forced circulating blast method ", uses 500 liters of reactions
Kettle, makes pressure in device bring up to 1 kg/cm.Chlorine source chlorine is passed directly into agitation device through heat exchanger, uses heat-transfer surface
2.5 rice2Heat exchanger be connected on agitation device and cyclic part outlet between, starting paraffin is heated to certain temperature (110 DEG C of left sides
It is right), then (5% or so) adds polyethylene and carries out heating fusing by a certain percentage, then puts into chlorination in kettle, and ensure with heat
Polyethylene is fusing shape.
With " equipment for preparation of paraffin chloride by forced circulating blast method " together, material temperature is low for present invention operation, and heat exchanger heating is on the contrary
Cooling.
Claims (1)
1. the hot method production method of Modified Chlorinated Paraffin -70 of air cooling is directly agitated in one kind pressurization, including chlorine and hydrogen chloride gas
Extract out, hydrogen chloride gas is only absorbed by the water in jet pump and hopper, remaining chlorine drum is pressed into agitation device, so continuous, its feature
It is：Increase reaction pressure, chlorine source chlorine is directly placed into agitation device in kettle through heat exchanger, gone here and there between agitation device and cyclic part outlet
Join heat exchanger, reacting gas is heated or cooled, starting paraffin certain temperature (110 DEG C or so) is heated to, then by certain
Ratio (5% or so) adds polyethylene and carries out heating fusing, then puts into chlorination in kettle, and ensure polyethylene as fusing using heat
Shape.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242125.9A CN107099331A (en) | 2017-04-04 | 2017-04-04 | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710242125.9A CN107099331A (en) | 2017-04-04 | 2017-04-04 | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107099331A true CN107099331A (en) | 2017-08-29 |
Family
ID=59674952
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710242125.9A Withdrawn CN107099331A (en) | 2017-04-04 | 2017-04-04 | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107099331A (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN105838433A (en) * | 2016-05-04 | 2016-08-10 | 林群祥 | Pressurized direct bubbling gas cooling-heating method for producing chlorinated paraffin-70 |
-
2017
- 2017-04-04 CN CN201710242125.9A patent/CN107099331A/en not_active Withdrawn
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1105372A (en) * | 1994-01-12 | 1995-07-19 | 林群祥 | Chlorinated polyvinyl paraffin wax |
| CN105838433A (en) * | 2016-05-04 | 2016-08-10 | 林群祥 | Pressurized direct bubbling gas cooling-heating method for producing chlorinated paraffin-70 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105838440A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination direct agitating gas heating and cooling method | |
| CN105925311A (en) | Method for producing chlorinated paraffin-70 through catalyzing, pressurizing and direct gas agitating cold-hot method | |
| CN105838438A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing bubbling agitating gas heating and cooling method | |
| CN105838433A (en) | Pressurized direct bubbling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN105950216A (en) | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method | |
| CN105838436A (en) | Method for producing chlorinated paraffin-70 through catalytic bubbling agitating gas heating and cooling method | |
| CN106010645A (en) | Method for producing chlorinated paraffin-70 in light chlorination direct propelling gas cold-heat mode | |
| CN106010647A (en) | Method for producing chlorinated paraffin-70 in catalysis propelling gas cold-heat mode | |
| CN107099331A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in pressurization | |
| CN105838435A (en) | Pressurized bubbling propelling gas cooling-heating method for producing chlorinated paraffin-70 | |
| CN106995721A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is directly agitated in catalysis pressurization | |
| CN106010646A (en) | Method for producing chlorinated paraffin-70 in light chlorination propelling gas cold-heat mode | |
| CN106987272A (en) | Pressurization Light chlorimation bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN106010644A (en) | Method for preparing chlorinated paraffin-70 with direct driving gas cold-heat method | |
| CN105950215A (en) | Method for producing chlorinated paraffin-70 with agitating gas cooling or heating method adopting catalytic pressurization | |
| CN105838439A (en) | Method for producing chlorinated paraffin-70 through catalytic pressurizing photo-chlorination agitating gas heating and cooling method | |
| CN107099333A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is agitated in pressurization | |
| CN106047408A (en) | Method for producing chlorinated paraffin-70 by pressurization photo-chlorination agitation gas cooling-heating method | |
| CN106929102A (en) | Method is directly agitated to produce Modified Chlorinated Paraffin method | |
| CN107057759A (en) | Pressurization bubbling agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN105950217A (en) | Method for producing chlorinated paraffin-70 with bubbling agitating gas cooling or heating method adopting pressurized photochlorination | |
| CN107033956A (en) | Pressurization Light chlorimation directly agitates the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN107033957A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is agitated in catalysis pressurization | |
| CN107057765A (en) | Directly agitate the hot method production method of Modified Chlorinated Paraffin 70 of air cooling | |
| CN106978210A (en) | The hot method production method of Modified Chlorinated Paraffin 70 of air cooling is agitated in catalysis |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WW01 | Invention patent application withdrawn after publication | ||
| WW01 | Invention patent application withdrawn after publication |
Application publication date: 20170829 |