CN107028805A - Emulsifying anti-acne mildy wash and preparation method thereof - Google Patents
Emulsifying anti-acne mildy wash and preparation method thereof Download PDFInfo
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- CN107028805A CN107028805A CN201710435729.5A CN201710435729A CN107028805A CN 107028805 A CN107028805 A CN 107028805A CN 201710435729 A CN201710435729 A CN 201710435729A CN 107028805 A CN107028805 A CN 107028805A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/89—Polysiloxanes
- A61K8/891—Polysiloxanes saturated, e.g. dimethicone, phenyl trimethicone, C24-C28 methicone or stearyl dimethicone
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0241—Containing particulates characterized by their shape and/or structure
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/37—Esters of carboxylic acids
- A61K8/375—Esters of carboxylic acids the alcohol moiety containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
- A61K8/442—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof substituted by amido group(s)
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/81—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions involving only carbon-to-carbon unsaturated bonds
- A61K8/8141—Compositions of homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides or nitriles thereof; Compositions of derivatives of such polymers
- A61K8/8147—Homopolymers or copolymers of acids; Metal or ammonium salts thereof, e.g. crotonic acid, (meth)acrylic acid; Compositions of derivatives of such polymers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/84—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds obtained by reactions otherwise than those involving only carbon-carbon unsaturated bonds
- A61K8/86—Polyethers
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/04—Topical preparations for affording protection against sunlight or other radiation; Topical sun tanning preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/70—Biological properties of the composition as a whole
- A61K2800/72—Hypo-allergenic
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Abstract
The present invention relates to emulsifying anti-acne mildy wash and preparation method thereof, the emulsifying anti-acne mildy wash is made up of the component of following percentage by weight：Monoglyceride：1% ~ 6%, dimethyl silicone polymer：1% ~ 8%, isopropyl myristate：2% ~ 10%, the alcohol of C16 ~ 18：1% ~ 10%, self-emulsifying monoglyceride：0.1% ~ 6%, Acritamer 940：0.2% ~ 1%, glycerine：1% ~ 10%, Cocoamidopropyl betaine：5% ~ 20%, AEO：1% ~ 10%, PH conditioning agents：0.1% ~ 1%, preservative：0.3% ~ 1.1%, Nano-Zinc：1% ~ 10%, essence：0.01% ~ 0.3%, Yi Jishui：Surplus；Each component sum is 100%.The emulsifying anti-acne mildy wash preparation technology of the present invention is simple, and prepared emulsifying anti-acne mildy wash has superior anti-acne effect, and product is gently non-stimulated, with good skin effect.
Description
Technical field
The present invention relates to a kind of mildy wash and preparation method thereof, belong to cosmetic field；More particularly, it relates to one
Plant emulsifying anti-acne mildy wash containing Nano-Zinc and preparation method thereof.
Background technology
With the quickening pace of modern life, work and the increase of life stress, along with environmental pollution and food security are asked
Topic takes place frequently, and the incidence of disease of whelk rises year by year.Whelk is a kind of common chronic pilosebaceous inflammations disease, good hair
In vigorous positions of sebum secretion such as face, shirtfront and upper backs, course of disease length, easily recurrence often show as Whiteheads, blackhead powder
Thorn or inflamed papules, serious has useless fellow, tubercle, tumour or scar.If inflammation substantially, can more cause pain or touch pain,
And with seborrhea, or even there is tangerine peel face.Whelk incidence in youth of both sexes crowd is high, and it not only has a strong impact on
Face it is attractive in appearance, and influence people social and psychology, make patient occur it is not self-confident, awkward, lose, anxiety, anxiety, irritability and
The negative emotions such as depression, so as to influence quality of life.
The cosmetics internal structure that traditional handicraft is obtained is micelle shape or micellelike, its a diameter of micron, to Cutaneous permeation
Ability is very weak, is difficult to be absorbed by epidermal cell.And skin outermost layer has hydrophobicity cuticula, thus water-soluble substances and big point
Sub- material is quite difficult by the absorption of epidermal absorption and pilosebaceous follicle.
The content of the invention
To overcome traditional handicraft cosmetics defect as described above, developed the invention provides a kind of use nanometer technology
Cosmetics, it can be suitable by composition specially treated most powerful in cosmetics into this extremely small structure of nanoscale
Profit penetrates to the skin internal layer, plays skin care with getting twice the result with half the effort, treats skin effect, the cosmetic defect obtained to traditional handicraft is carried out very
Good improvement.
In an aspect, the invention provides a kind of emulsifying anti-acne mildy wash, by the component of following percentage by weight
Constitute：Monoglyceride：1% ~ 6%, dimethyl silicone polymer：1% ~ 8%, isopropyl myristate：2% ~ 10%, the alcohol of C16 ~ 18：1%~10%、
Self-emulsifying monoglyceride：0.1% ~ 6%, Acritamer 940：0.2% ~ 1%, glycerine：1% ~ 10%, Cocoamidopropyl betaine：5%~20%、
AEO：1% ~ 10%, PH conditioning agents：0.1% ~ 1%, preservative：0.3% ~ 1.1%, Nano-Zinc：1% ~ 10%, essence：
0.01% ~ 0.3%, Yi Jishui：Surplus；Each component sum is 100%.
In a preferred embodiment, the preservative be methyl hydroxybenzoate 0.1% ~ 0.5%, propylben 0.1% ~
0.3% and double hydroxy imidazole ureines 0.1% ~ 0.3%.
In a preferred embodiment, the pH adjusting agent is triethanolamine.
In a preferred embodiment, emulsifying anti-acne mildy wash of the invention by following percentage by weight component structure
Into：Monoglyceride：2%th, dimethyl silicone polymer：1%th, isopropyl myristate：4%th, the alcohol of C16 ~ 18：7%th, self-emulsifying monoglyceride：
0.3%th, Acritamer 940：0.3%th, glycerine：4%th, Cocoamidopropyl betaine：10%th, AEO：3%th, three ethanol
Amine：0.3%th, methyl hydroxybenzoate：0.1%th, propylben：0.1%th, double hydroxy imidazole ureines：0.1%th, Nano-Zinc：2.7%th, it is fragrant
Essence：0.05%th, Yi Jishui：65.05%.
In a preferred embodiment, emulsifying anti-acne mildy wash of the invention by following percentage by weight component structure
Into：Monoglyceride：6%th, dimethyl silicone polymer：8%th, isopropyl myristate：2%th, the alcohol of C16 ~ 18：1%th, self-emulsifying monoglyceride：2%、
Acritamer 940：1%th, glycerine：1%th, Cocoamidopropyl betaine：6%th, AEO：1.8%th, triethanolamine：1%、
Methyl hydroxybenzoate：0.5%th, propylben：0.3%th, double hydroxy imidazole ureines：0.3%th, Nano-Zinc：8%th, essence：0.3%th, with
And water：60.8%.
In a preferred embodiment, emulsifying anti-acne mildy wash of the invention by following percentage by weight component structure
Into：Monoglyceride：4%th, dimethyl silicone polymer：4.7%th, isopropyl myristate：8.8%th, the alcohol of C16 ~ 18：5%th, self-emulsifying list is sweet
Ester：5%th, Acritamer 940：0.6%th, glycerine：9%th, Cocoamidopropyl betaine：17%th, AEO：1%th, three second
Hydramine：0.1%th, methyl hydroxybenzoate：0.2%th, propylben：0.2%th, double hydroxy imidazole ureines：0.2%th, Nano-Zinc：1%th, it is fragrant
Essence：0.1%th, Yi Jishui：43.1%.
In a preferred embodiment, the water is light water, high purity water, distilled water, reverse osmosis water or small-micelle water；
Preferably high purity water, distilled water, reverse osmosis water or small-micelle water；More preferably small-micelle water.
In another aspect, the invention provides a kind of preparation method of emulsifying anti-acne mildy wash, including following step
Suddenly：
Carbomer dissolves：Acritamer 940 is weighed, part aqueous solution is used；
It is prepared by oil phase thing：Monoglyceride, dimethyl silicone polymer, isopropyl myristate, the alcohol of C16 ~ 18, self-emulsifying monoglyceride are mixed
Close, the heating stirring under the conditions of 70-80 DEG C, it is all melted and obtain liquid oil phase thing；
It is prepared by aqueous-phase material：By glycerine, Cocoamidopropyl betaine, AEO, PH conditioning agents and remainder
Water is mixed, and heating stirring obtains aqueous-phase material under the conditions of 70-80 DEG C；
Emulsification：The oil phase thing is slowly added into progress emulsification in the aqueous-phase material and is cooled to about 40 DEG C, preservative, nanometer is added
Zinc, essence and the solution obtained by carbomer dissolving step, continue to emulsify, are cooled to room temperature, obtain the emulsifying anti-acne
Mildy wash；
Wherein, by weight percentage, each component sum is 100% to each component.
In a preferred embodiment, the preservative is methyl hydroxybenzoate, propylben and double hydroxy imidazole alkyl
Urea；The PH conditioning agents are triethanolamine.
In a preferred embodiment, mixing speed is 600-1000rpm, preferably 600-800rpm, more preferably
700-800rpm；Mixing time is 10-30min；Emulsification times are 10-20min.
Wherein, the water can be light water, high purity water, distilled water, reverse osmosis water or the small molecule such as running water
Group's water；Preferably high purity water, distilled water, reverse osmosis water or small-micelle water；More preferably small-micelle water.Small-micelle water has
There are high osmosis, high diffusibility and highly dissoluble, more moisture and nutrition can be brought into cell, while by waste and poisonous substance
Preferably discharge.Because small-micelle water more easily can be absorbed and be utilized by internal cell, so its biology utilization rate
It is more much higher than light water, the information transmission between efficiency and function, enhancing cell and the surrounding tissue of metabolism can be strengthened,
The transmission supply of nutrition of whole body material is obviously improved, transport capacity of whole body oxygen etc. is improved.
Nano-Zinc is a kind of multi-functional new inorganic material.Due to the granular of crystal grain, its Electronic Structure and
Crystal structure changes, and generates skin effect, bulk effect, quantum size effect and macroscopic view that macro object does not have
The features such as tunnel-effect and the high grade of transparency, polymolecularity.The outstanding feature of Nano-Zinc is that product pellet is nanoscale, simultaneously
Double grading with nano material and conventional oxidation zinc.Nanometer Zinc material heat endurance is good, can adsorb, suppresses and kill thin
Bacterium, the features such as with good anti-bacterial effect, timeliness length, safe, reasonable price, in oral anxious toxicity, skin irritatin, sensitiveness
Confirmed in experiment, with tight security and antimicrobial long-acting ability.
Nanometer zinc particles used in the present invention and preparation method thereof, will here by reference referring to CN104014814A
Entire contents are incorporated herein.The toner of the present invention, as active component, can be substituted existing using Nano-Zinc as described above
There is the active component in anti-acne toner in technology, and in the case of without being cooperated with other anti-acne active components,
Can just play that effect is more preferable and the effect of more comprehensive anti-acne, acne-removing significantly, it is quick, persistently, safety；And and skin
With good compatibility, it can be absorbed by the skin rapidly, it is safe, gentle, do not cause stimulation, allergy etc. to be reacted, skin does not have yet
Burden.Nano-Zinc active component in toner of the present invention can suppress the microbial growths such as bacterium, fungi, slow down even
Eliminate inflammation and complication caused by small pox.
Dimethyl silicone polymer in mildy wash of the present invention has greasy property, anti-ultraviolet effect, good permeability, tool
There is obvious dust reduction capability, with preferable flexibility, the permeability to skin is very good；Added in the mildy wash of the present invention poly-
After dimethyl siloxane, make that there is smooth refreshing experience after washing one's face on skin, increase the flexibility of skin.
Isopropyl myristate in mildy wash of the present invention plays a part of moisturizing and skin care, and skin is to myristic acid
The absorbability of isopropyl ester preferably, can effectively be contacted with hair follicle in cortex, penetrate into cortex depths, and by the activearm in mildy wash
Divide and bring into, give full play to the effect of active ingredient.
Cocoamidopropyl betaine in mildy wash of the present invention is a kind of amphoteric surfactant, with good clear
Wash, bubble, opsonic action, it is good with anion, cation and nonionic surfactant compatibility；Excitant is small, moderate performance,
Foam is fine and smooth and stably, can strengthen the flexibility to skin.
AEO in mildy wash of the present invention be ehter bond in nonionic surfactant, molecule be difficult by
Acid, alkali destruction, stability are higher, water-soluble preferable, electrolyte-resistant, it is easy to biodegradable, and foam is small；AEO
Compatibility with Cocoamidopropyl betaine is good, low temperature performance well insensitive to hard water.Preservative in Essence of the present invention
Using methyl hydroxybenzoate, Phenoxyethanol and double hydroxy imidazole ureine compounding uses, the anti-corrosion of toner can be effectively improved
Performance, extends pot-life of toner etc..
The emulsifying anti-acne mildy wash of the present invention has good compatibility with skin, can effectively cleaning skin, and effect
Composition can be absorbed by the skin rapidly, safe, gentle, not cause stimulation, allergy etc. to be reacted, skin is not also born.Cleaning face
Afterwards, promote the absorption of the compositions such as Nano-Zinc, effectively dispel small pox, slow down and diminish inflammation and sequelae, promote wound healing, it is light
Change and eliminate acne print and scar, promote moisturizing, moisturizing, anti-acne, the absorption of nutritional ingredient while face cleaning, alleviate and eliminate cleaning
Rear face is tight.The present invention from Bergamot Mint Extract, dissolution angular embolization, suppress bacterial multiplication, repair scar, resistance ultraviolet, disappear
Pigmentation, promotion anti-acne composition percutaneous absorbtion, promotion whelk wound are cured after inflammation, antiallergy, anti-oxidant, moisturizing, anti-inflammatory
In terms of conjunction, comprehensive and significant anti-acne effect is played, skin is recovered normal fine and smooth soft and smooth.After deactivation, the symptom such as whelk
Uneasy to recur, acne-removing is notable, quick, lasting, safety.The emulsifying anti-acne mildy wash preparation technology of the present invention is simple, institute
The emulsifying anti-acne mildy wash of preparation has superior anti-acne effect, and product is gently non-stimulated, with good skin effect.
The functional component in emulsifying anti-acne mildy wash is smoothly penetrated to the skin internal layer using nanometer technology development, thing half
Work(plays skin care, treats skin effect again, and the cosmetic defect obtained to traditional handicraft is improved well.
Embodiment
Embodiments of the invention will be hereafter further described, wherein, each embodiment is only that the present invention is exemplary
Embodiment, it is not intended to constitute limiting the scope of the invention.Those skilled in the art can according to explanation above with
And following description of the embodiments makes a variety of different improvement and deformation, it is without departing from spirit and substance of the present invention.
Accordingly, the scope of the present invention is intended merely to be defined by every claim scope claimed.
Embodiment 1：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：0.3% Acritamer 940 is weighed, is dissolved with 10% water；
It is prepared by oil phase thing：By 2% monoglyceride, 1% dimethyl silicone polymer, 4% isopropyl myristate, the alcohol of 7%C16 ~ 18,0.3% from
Monoglyceride mixing is emulsified, the heating stirring under the conditions of 75 DEG C makes it all melt and obtains liquid oil phase thing；
It is prepared by aqueous-phase material：By 4% glycerine, 10% Cocoamidopropyl betaine, 3% AEO, 0.3% triethanolamine
With the mixing of 55.05% water, heating stirring 20min obtains aqueous-phase material under the conditions of 75 DEG C；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 10min, be cooled to about 40 DEG C, add 0.1% methyl hydroxybenzoate, 0.1% propylben, the 0.1% pair of hydroxy imidazole ureine,
2.7% Nano-Zinc, 0.05% essence and the mixture obtained by carbomer dissolving step, continue to emulsify 10min, are cooled to room
Temperature, obtains emulsifying anti-acne mildy wash.
Embodiment 2：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：1% Acritamer 940 is weighed, is dissolved with 6% water；
It is prepared by oil phase thing：By 6% monoglyceride, 8% dimethyl silicone polymer, 2% isopropyl myristate, the alcohol of 1%C16 ~ 18,2% from breast
Change monoglyceride mixing, the heating stirring under the conditions of 75 DEG C makes it all melt and obtains liquid oil phase thing；
It is prepared by aqueous-phase material：By 1% glycerine, 6% Cocoamidopropyl betaine, 1.8% AEO, 1% triethanolamine
With the mixing of 54.8% water, heating stirring 20min obtains aqueous-phase material under the conditions of 75 DEG C；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 10min, be cooled to about 40 DEG C, add 0.5% methyl hydroxybenzoate, 0.3% propylben, the 0.3% pair of hydroxy imidazole ureine,
8% Nano-Zinc, 0.3% essence and the solution obtained by carbomer dissolving step, continue to emulsify 10min, are cooled to room temperature, obtain
The emulsifying anti-acne mildy wash of the present embodiment.
Embodiment 3：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：0.6% Acritamer 940 is weighed, is dissolved with 5% water；
It is prepared by oil phase thing：By 4% monoglyceride, 4.7% dimethyl silicone polymer, 8.8% isopropyl myristate, the alcohol of 5%C16 ~ 18,5%
Self-emulsifying monoglyceride is mixed, the heating stirring under the conditions of 75 DEG C, it is all melted and is obtained liquid oil phase thing；
It is prepared by aqueous-phase material：By 9% glycerine, 17% Cocoamidopropyl betaine, 1% AEO, 0.1% triethanolamine
With the mixing of 38.1% water, heating stirring 20min obtains aqueous-phase material under the conditions of 75 DEG C；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 10min, be cooled to about 40 DEG C, add 0.2% methyl hydroxybenzoate, 0.2% propylben, the 0.2% pair of hydroxy imidazole ureine,
1% Nano-Zinc, 0.1% essence and the solution obtained by carbomer dissolving step, continue to emulsify 10min, are cooled to room temperature, obtain
Emulsifying anti-acne mildy wash.
Embodiment 4：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：0.2% Acritamer 940 is weighed, the dissolving of 10% small molecule is added（Dissolve the small-micelle water of Acritamer 940
Amount adds a small amount of small-micelle water dissolving to dissolve Acritamer 940, on the high side inclined no more than total water ratio
Few not influence to prepare, ratio illustrates only for convenience of description, is not limitation foundation）；
It is prepared by oil phase thing：By 1% monoglyceride, 2% dimethyl silicone polymer, 10% isopropyl myristate, the alcohol of 10%C16 ~ 18,0.1%
Self-emulsifying monoglyceride is mixed, at 70-80 DEG C（Such as 70 DEG C, 75 DEG C, 80 DEG C）Under the conditions of heating stirring, make its all fusing obtain
Liquid oil phase thing；
It is prepared by aqueous-phase material：By 10% glycerine, 5% Cocoamidopropyl betaine, 10% AEO, 0.6% 3 ethanol
Amine and the mixing of 28% small-micelle water, at 30-80 DEG C（Oil phase thing is not solidified from temperature, can select in 30-80 DEG C
Arbitrary temp value realized, being matched with oil phase thing temperature preferably）Under the conditions of heating stirring 30min obtain aqueous-phase material；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 20min, be cooled to less than 45 DEG C（Such as 40 DEG C or so, or directly it is down to room temperature）, add 0.3% methyl hydroxybenzoate, 0.15% Buddhist nun
The golden propyl ester of pool, the 0.15% pair of hydroxy imidazole ureine, 10% Nano-Zinc, 0.01% essence and obtained by carbomer dissolving step
Solution, continues to emulsify 20min, is cooled to room temperature, obtain emulsifying anti-acne mildy wash.
Embodiment 5：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：0.8% Acritamer 940 is weighed, the dissolving of 10% small molecule is added（Dissolve the small-micelle water of Acritamer 940
Amount adds a small amount of small-micelle water dissolving to dissolve Acritamer 940, on the high side inclined no more than total water ratio
Few not influence to prepare, ratio illustrates only for convenience of description, is not limitation foundation）；
It is prepared by oil phase thing：By 3% monoglyceride, 3% dimethyl silicone polymer, 6% isopropyl myristate, the alcohol of 8%C16 ~ 18,6% from breast
Change monoglyceride mixing, at 70-80 DEG C（Such as 70 DEG C, 75 DEG C, 80 DEG C）Under the conditions of heating stirring, make its all fusing obtain liquid
Oil phase thing；
It is prepared by aqueous-phase material：By 6% glycerine, 20% Cocoamidopropyl betaine, 5% AEO, 0.4% triethanolamine
Mixed with 25.95% small-micelle water, at 30-80 DEG C（Oil phase thing is not solidified from temperature, can select in 30-80 DEG C
Arbitrary temp value realized, being matched with oil phase thing temperature preferably）Under the conditions of heating stirring 10-30min obtain aqueous phase
Thing；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 10-20min, be cooled to less than 45 DEG C（Such as 40 DEG C or so, or directly it is down to room temperature）, 0.15% methyl hydroxybenzoate of addition,
0.25% propylben, the 0.25% pair of hydroxy imidazole ureine, 5% Nano-Zinc, 0.2% essence and obtained by carbomer dissolving step
The solution obtained, continues to emulsify 15min, is cooled to room temperature, obtain emulsifying anti-acne mildy wash.
Embodiment 6：
Preparing for the emulsifying anti-acne mildy wash of the present embodiment is as follows：
Carbomer dissolves：0.4% Acritamer 940 is weighed, the dissolving of 10% small molecule is added（Dissolve the small-micelle water of Acritamer 940
Amount adds a small amount of small-micelle water dissolving to dissolve Acritamer 940, on the high side inclined no more than total water ratio
Few not influence to prepare, ratio illustrates only for convenience of description, is not limitation foundation）；
It is prepared by oil phase thing：By 4% monoglyceride, 4% dimethyl silicone polymer, 5% isopropyl myristate, the alcohol of 6%C16 ~ 18,1% from breast
Change monoglyceride mixing, at 70-80 DEG C（Such as 70 DEG C, 75 DEG C, 80 DEG C）Under the conditions of heating stirring, make its all fusing obtain liquid
Oil phase thing；
It is prepared by aqueous-phase material：By 4% glycerine, 12% Cocoamidopropyl betaine, 6% AEO, 0.5% triethanolamine
Mixed with 40.57% small-micelle water, at 30-80 DEG C（Oil phase thing is not solidified from temperature, can select in 30-80 DEG C
Arbitrary temp value realized, being matched with oil phase thing temperature preferably）Under the conditions of heating stirring 10-30min obtain aqueous phase
Thing；
Emulsification：Oil phase thing is slowly added into aqueous-phase material and emulsified, then by thus obtained mixture in homogenizer it is newborn
Change 10-20min, be cooled to less than 45 DEG C（Such as 40 DEG C or so, or directly it is down to room temperature）, add 0.25% methyl hydroxybenzoate, 0.1%
Propylben, the 0.1% pair of hydroxy imidazole ureine, 6% Nano-Zinc, 0.08% essence and obtained by carbomer dissolving step
Solution, continues to emulsify 10-20min（Such as 15min, 10min, 20min）, room temperature is cooled to, emulsifying anti-acne face cleaning is obtained
Breast.
Wherein, water involved in embodiment 1-6 can be for example, the light water of running water etc., high purity water, distilled water,
Reverse osmosis water, small-micelle water etc.；Preferably high purity water, distilled water, reverse osmosis water；More preferably small-micelle water.
Claims (10)
1. a kind of emulsifying anti-acne mildy wash, it is characterised in that be made up of the component of following percentage by weight：Monoglyceride：1%~
6%th, dimethyl silicone polymer：1% ~ 8%, isopropyl myristate：2% ~ 10%, the alcohol of C16 ~ 18：1% ~ 10%, self-emulsifying monoglyceride：
0.1% ~ 6%, Acritamer 940：0.2% ~ 1%, glycerine：1% ~ 10%, Cocoamidopropyl betaine：5% ~ 20%, fatty alcohol polyoxy second
Alkene ether：1% ~ 10%, PH conditioning agents：0.1% ~ 1%, preservative：0.3% ~ 1.1%, Nano-Zinc：1% ~ 10%, essence：0.01%~0.3%、
And water：Surplus；Each component sum is 100%.
2. emulsifying anti-acne mildy wash according to claim 1, it is characterised in that the preservative is methyl hydroxybenzoate
0.1% ~ 0.5%, propylben 0.1% ~ 0.3% and double hydroxy imidazole ureines 0.1% ~ 0.3%.
3. emulsifying anti-acne mildy wash according to claim 1 or 2, it is characterised in that the PH conditioning agents are three ethanol
Amine.
4. the emulsifying anti-acne mildy wash according to any one of claims 1 to 3, it is characterised in that by following weight percent
The component of ratio is constituted：Monoglyceride：2%th, dimethyl silicone polymer：1%th, isopropyl myristate：4%th, the alcohol of C16 ~ 18：7%th, self-emulsifying
Monoglyceride：0.3%th, Acritamer 940：0.3%th, glycerine：4%th, Cocoamidopropyl betaine：10%th, AEO：
3%th, triethanolamine：0.3%th, methyl hydroxybenzoate：0.1%th, propylben：0.1%th, double hydroxy imidazole ureines：0.1%th, nanometer
Zinc：2.7%th, essence：0.05%th, Yi Jishui：65.05%.
5. the emulsifying anti-acne mildy wash according to any one of claims 1 to 3, it is characterised in that by following weight percent
The component of ratio is constituted：Monoglyceride：6%th, dimethyl silicone polymer：8%th, isopropyl myristate：2%th, the alcohol of C16 ~ 18：1%th, self-emulsifying
Monoglyceride：2%th, Acritamer 940：1%th, glycerine：1%th, Cocoamidopropyl betaine：6%th, AEO：1.8%th, three
Monoethanolamine：1%th, methyl hydroxybenzoate：0.5%th, propylben：0.3%th, double hydroxy imidazole ureines：0.3%th, Nano-Zinc：8%th, it is fragrant
Essence：0.3%th, Yi Jishui：60.8%.
6. the emulsifying anti-acne mildy wash according to any one of claims 1 to 3, it is characterised in that by following weight percent
The component of ratio is constituted：Monoglyceride：4%th, dimethyl silicone polymer：4.7%th, isopropyl myristate：8.8%th, the alcohol of C16 ~ 18：5%th, certainly
Emulsify monoglyceride：5%th, Acritamer 940：0.6%th, glycerine：9%th, Cocoamidopropyl betaine：17%th, AEO：
1%th, triethanolamine：0.1%th, methyl hydroxybenzoate：0.2%th, propylben：0.2%th, double hydroxy imidazole ureines：0.2%th, nanometer
Zinc：1%th, essence：0.1%th, Yi Jishui：43.1%.
7. the emulsifying anti-acne mildy wash according to any one of claim 1 to 6, it is characterised in that：The water be light water,
High purity water, distilled water, reverse osmosis water or small-micelle water；Preferably high purity water, distilled water, reverse osmosis water or small-micelle water；
More preferably small-micelle water.
8. a kind of preparation method of emulsifying anti-acne mildy wash according to any one of claim 1 to 7, it is characterised in that
Comprise the following steps：
Carbomer dissolves：Acritamer 940 is weighed, part aqueous solution is used；
It is prepared by oil phase thing：Monoglyceride, dimethyl silicone polymer, isopropyl myristate, the alcohol of C16 ~ 18, self-emulsifying monoglyceride are mixed
Close, the heating stirring under the conditions of 70-80 DEG C, it is all melted and obtain liquid oil phase thing；
It is prepared by aqueous-phase material：By glycerine, Cocoamidopropyl betaine, AEO, PH conditioning agents and remainder
Water is mixed, and heating stirring obtains aqueous-phase material under the conditions of 70-80 DEG C；
Emulsification：The oil phase thing is slowly added into progress emulsification in the aqueous-phase material and is cooled to about 40 DEG C, preservative, nanometer is added
Zinc, essence and the solution obtained by carbomer dissolving step, continue to emulsify, are cooled to room temperature, obtain the emulsifying anti-acne
Mildy wash；
Wherein, by weight percentage, each component sum is 100% to each component.
9. the preparation method of emulsifying anti-acne mildy wash according to claim 8, it is characterised in that the preservative is Buddhist nun
Moor tortoise beetle ester, propylben and double hydroxy imidazole ureines；The PH conditioning agents are triethanolamine.
10. the preparation method of emulsifying anti-acne mildy wash according to claim 8 or claim 9, it is characterised in that mixing speed is
600-1000rpm, preferably 600-800rpm, more preferably 700-800rpm；Mixing time is 10-30min；Emulsification times are
10-20min。
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111543442A (en) * | 2020-06-11 | 2020-08-18 | 杭州云昇科技有限公司 | Composite sterilization liquid based on traditional Chinese medicine volatile oil and preparation method thereof |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1927158A (en) * | 2005-09-08 | 2007-03-14 | 天津市世雄科技发展有限公司 | Milky wash containing ginseng and barbados aloe |
| CN105380815A (en) * | 2015-11-24 | 2016-03-09 | 刘勇 | Acne-removing facial cleanser |
| CN105708718A (en) * | 2016-04-13 | 2016-06-29 | 广州丹奇日用化工厂有限公司 | Acne-removal cosmetic composition containing nano-zinc |
-
2017
- 2017-06-12 CN CN201710435729.5A patent/CN107028805A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1927158A (en) * | 2005-09-08 | 2007-03-14 | 天津市世雄科技发展有限公司 | Milky wash containing ginseng and barbados aloe |
| CN105380815A (en) * | 2015-11-24 | 2016-03-09 | 刘勇 | Acne-removing facial cleanser |
| CN105708718A (en) * | 2016-04-13 | 2016-06-29 | 广州丹奇日用化工厂有限公司 | Acne-removal cosmetic composition containing nano-zinc |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111543442A (en) * | 2020-06-11 | 2020-08-18 | 杭州云昇科技有限公司 | Composite sterilization liquid based on traditional Chinese medicine volatile oil and preparation method thereof |
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