CN107022429A - A kind of preparation method of wood artwork fingerprint surface cleaning agent - Google Patents
A kind of preparation method of wood artwork fingerprint surface cleaning agent Download PDFInfo
- Publication number
- CN107022429A CN107022429A CN201710297784.2A CN201710297784A CN107022429A CN 107022429 A CN107022429 A CN 107022429A CN 201710297784 A CN201710297784 A CN 201710297784A CN 107022429 A CN107022429 A CN 107022429A
- Authority
- CN
- China
- Prior art keywords
- parts
- added
- cooled
- glue
- continue
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000012459 cleaning agent Substances 0.000 title claims abstract description 16
- 239000002023 wood Substances 0.000 title claims abstract description 13
- 238000002360 preparation method Methods 0.000 title claims abstract description 9
- 239000000203 mixture Substances 0.000 claims abstract description 30
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 30
- 239000003292 glue Substances 0.000 claims abstract description 21
- 239000000839 emulsion Substances 0.000 claims abstract description 14
- 238000009413 insulation Methods 0.000 claims abstract description 13
- 239000004831 Hot glue Substances 0.000 claims abstract description 9
- 239000001888 Peptone Substances 0.000 claims abstract description 9
- 108010080698 Peptones Proteins 0.000 claims abstract description 9
- 235000019319 peptone Nutrition 0.000 claims abstract description 9
- 238000001816 cooling Methods 0.000 claims abstract description 5
- 235000013312 flour Nutrition 0.000 claims abstract description 5
- 235000011837 pasties Nutrition 0.000 claims abstract description 5
- 238000003756 stirring Methods 0.000 claims description 28
- 239000003795 chemical substances by application Substances 0.000 claims description 20
- 239000012153 distilled water Substances 0.000 claims description 20
- 239000003822 epoxy resin Substances 0.000 claims description 20
- 229920000647 polyepoxide Polymers 0.000 claims description 20
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 claims description 16
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 16
- 150000002148 esters Chemical class 0.000 claims description 9
- CDBYLPFSWZWCQE-UHFFFAOYSA-L Sodium Carbonate Chemical compound [Na+].[Na+].[O-]C([O-])=O CDBYLPFSWZWCQE-UHFFFAOYSA-L 0.000 claims description 8
- 150000001412 amines Chemical class 0.000 claims description 8
- 229960005070 ascorbic acid Drugs 0.000 claims description 8
- 235000010323 ascorbic acid Nutrition 0.000 claims description 8
- 239000011668 ascorbic acid Substances 0.000 claims description 8
- 230000000740 bleeding effect Effects 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- 239000003999 initiator Substances 0.000 claims description 8
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 claims description 8
- 239000003643 water by type Substances 0.000 claims description 8
- YZCKVEUIGOORGS-IGMARMGPSA-N Protium Chemical group [1H] YZCKVEUIGOORGS-IGMARMGPSA-N 0.000 claims description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 239000005996 Blood meal Substances 0.000 claims description 4
- 229920001131 Pulp (paper) Polymers 0.000 claims description 4
- 239000008280 blood Substances 0.000 claims description 4
- 210000004369 blood Anatomy 0.000 claims description 4
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical class [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims description 4
- 235000011116 calcium hydroxide Nutrition 0.000 claims description 4
- -1 carboxy-propyl Chemical group 0.000 claims description 4
- 239000004359 castor oil Substances 0.000 claims description 4
- 235000019438 castor oil Nutrition 0.000 claims description 4
- 229920002678 cellulose Polymers 0.000 claims description 4
- 235000010980 cellulose Nutrition 0.000 claims description 4
- 239000008367 deionised water Substances 0.000 claims description 4
- 229910021641 deionized water Inorganic materials 0.000 claims description 4
- 239000003995 emulsifying agent Substances 0.000 claims description 4
- 239000006260 foam Substances 0.000 claims description 4
- ZEMPKEQAKRGZGQ-XOQCFJPHSA-N glycerol triricinoleate Natural products CCCCCC[C@@H](O)CC=CCCCCCCCC(=O)OC[C@@H](COC(=O)CCCCCCCC=CC[C@@H](O)CCCCCC)OC(=O)CCCCCCCC=CC[C@H](O)CCCCCC ZEMPKEQAKRGZGQ-XOQCFJPHSA-N 0.000 claims description 4
- 239000003112 inhibitor Substances 0.000 claims description 4
- 235000012054 meals Nutrition 0.000 claims description 4
- 229910000029 sodium carbonate Inorganic materials 0.000 claims description 4
- 239000004094 surface-active agent Substances 0.000 claims description 4
- DCKVNWZUADLDEH-UHFFFAOYSA-N sec-butyl acetate Chemical compound CCC(C)OC(C)=O DCKVNWZUADLDEH-UHFFFAOYSA-N 0.000 claims description 3
- PYBNTRWJKQJDRE-UHFFFAOYSA-L dodecanoate;tin(2+) Chemical class [Sn+2].CCCCCCCCCCCC([O-])=O.CCCCCCCCCCCC([O-])=O PYBNTRWJKQJDRE-UHFFFAOYSA-L 0.000 claims description 2
- 210000000481 breast Anatomy 0.000 claims 1
- LUZSPGQEISANPO-UHFFFAOYSA-N butyltin Chemical compound CCCC[Sn] LUZSPGQEISANPO-UHFFFAOYSA-N 0.000 claims 1
- 239000007788 liquid Substances 0.000 claims 1
- 230000006378 damage Effects 0.000 abstract description 3
- 239000012535 impurity Substances 0.000 abstract description 2
- 231100000252 nontoxic Toxicity 0.000 abstract description 2
- 230000003000 nontoxic effect Effects 0.000 abstract description 2
- YZCKVEUIGOORGS-OUBTZVSYSA-N Deuterium Chemical group [2H] YZCKVEUIGOORGS-OUBTZVSYSA-N 0.000 description 2
- 239000013530 defoamer Substances 0.000 description 2
- AYOHIQLKSOJJQH-UHFFFAOYSA-N dibutyltin Chemical compound CCCC[Sn]CCCC AYOHIQLKSOJJQH-UHFFFAOYSA-N 0.000 description 2
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000002425 crystallisation Methods 0.000 description 1
- 230000008025 crystallization Effects 0.000 description 1
- 230000003631 expected effect Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/268—Carbohydrates or derivatives thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D11/00—Special methods for preparing compositions containing mixtures of detergents
- C11D11/0082—Special methods for preparing compositions containing mixtures of detergents one or more of the detergent ingredients being in a liquefied state, e.g. slurry, paste or melt, and the process resulting in solid detergent particles such as granules, powders or beads
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D17/00—Detergent materials or soaps characterised by their shape or physical properties
- C11D17/0008—Detergent materials or soaps characterised by their shape or physical properties aqueous liquid non soap compositions
- C11D17/003—Colloidal solutions, e.g. gels; Thixotropic solutions or pastes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/263—Ethers
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/265—Carboxylic acids or salts thereof
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/26—Organic compounds containing oxygen
- C11D7/266—Esters or carbonates
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/32—Organic compounds containing nitrogen
- C11D7/3209—Amines or imines with one to four nitrogen atoms; Quaternized amines
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D7/00—Compositions of detergents based essentially on non-surface-active compounds
- C11D7/22—Organic compounds
- C11D7/40—Products in which the composition is not well defined
- C11D7/46—Animal products
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
- C11D2111/00—Cleaning compositions characterised by the objects to be cleaned; Cleaning compositions characterised by non-standard cleaning or washing processes
- C11D2111/10—Objects to be cleaned
- C11D2111/14—Hard surfaces
Landscapes
- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Emergency Medicine (AREA)
- Dispersion Chemistry (AREA)
- Zoology (AREA)
- Molecular Biology (AREA)
- Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
- Dry Formation Of Fiberboard And The Like (AREA)
Abstract
A kind of preparation method of wood artwork fingerprint surface cleaning agent, prepare pre-emulsion, the glue peptone shape object prepared is mixed with 50% pre-emulsion again, the hot glue prepared is mixed with 50% pre-emulsion, 30 32 parts of flour are taken, not dilute pasty state cannot be tuned into dryly with cold water, mixture one is added with mixture two and mixed, is stirred, uniformly, 45 DEG C of insulations, obtain cleaning agent.Cleaning agent is applied on wood artwork, after cooling, forms glue, i.e. adsorbable fingerprint is torn, it is easy and effective, it will not penetrate into inside wooden product, meanwhile, this product is nontoxic, wooden product surface nondestructive is done harm to, forms after glue, can also effectively remove the fine impurities on wooden product surface.
Description
Technical field：
Field is maintained the present invention relates to a kind of handicraft, and in particular to a kind of system of wood artwork fingerprint surface cleaning agent
Preparation Method.
Background technology：
Handicraft is always the conventional outlet product of China, makes fineness and cost is low, can go with the current of the times, so in America and Europe
There is broad mass market always.Chinese Art and Craft goods are abundant in content colorful, and vivid and interesting is cheap, and development prospect is considerable；
Handicraft creates the value higher than life from life.It is people's crystallization of wisdom, is fully demonstrated
The creativeness and artistry of the mankind, is the priceless treasure of the mankind.Many people have bought wood carving craft, all like taking wet rag to wipe
Wipe, if often taking wet rag to wipe, moisture can be made to be deep into woodcarving, will gradually damage woodcarving, and with the hair with water
Towel is wiped, and can so be made wood carving craft excessively moist, expected effect not reached on the contrary, but also injured them.
The content of the invention：
The technical problems to be solved by the invention are to overcome a kind of wood artwork fingerprint surface of prior art offer clear
Clean dose of preparation method.
The technical problems to be solved by the invention are realized using following technical scheme.
A kind of preparation method of wood artwork fingerprint surface cleaning agent, it is characterised in that：Comprise the following steps：
Step 1：Start the agitator of reactor, rotating speed is 30r/min, while adding 50-60 parts of deionized water；
Step 2：After 5-10min, 1-2 parts of emulsifying agents are added；
Step 3：After 5-10min, 3-6 parts of epoxy resin and 2-3 parts of methyl epoxy resin is added；
Step 4：After 5-10min, 6-9 parts of epoxy resin esters and 1-2 parts of methyl epoxy resin esters and epoxy resin fourth are added
The mixture of ester；
Step 5：After 5-10min, 0.5-1 parts of chain-transferring agent is added；
Step 6：The initiator of 1-2 parts of addition, is added after initiator, rotating speed increases to 85r/min, time 30min, obtains
Pre-emulsion；
Step 7：Take 30-35 parts of blood meals to be immersed in distilled water, keep distilled water temperature control at 28-30 DEG C, immersion
Long 4-5 hours, amount of distilled water is four times of blood meal；The aqueous sodium carbonate of 6-12 parts 20% is added in distilled water, 2-3 is stirred
Hour；3-6 parts of calcium hydroxides of allotment and 15-23 parts of distilled water, stir simultaneously, and mixing speed 20-30r/min divides per 3-5
Clock is stirred once, duration 3 minutes, and surfactant foam is removed at any time, and wood pulp to be mixed proposes glue surface, and defluent glue is immediately
Silk is broken into glue peptone shape, cools down；
Step 8：Take 50% pre-emulsion and glue peptone shape object to stir mix, heating is stirred, temperature control at 60-70 DEG C,
3min, adds 10-12 parts of deionized waters, continues the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 9：After insulation terminates, 70 DEG C are cooled to, 3-5 parts of hydrogen peroxide and 1-2 parts of ascorbic acid are sequentially added；
Step 10：Continue to cool, be cooled to 60 DEG C, sequentially add 3-6 parts of bleeding agents and 1-2 parts of defoamers；
Step 11：Continue to drop, temperature is cooled to 50 DEG C, and 1-2 parts of amine curing agents obtain mixture one；
Step 12：13-15 parts of castor oil and 6-8 parts of carboxy-propyl celluloses are taken, are added in reactor, vavuum pump is started and stirs
Device is mixed, reactor internal pressure is less than 2666pa, is evacuated 2 hours at 100-120 DEG C, is cooled to room temperature, adds 1-3 parts of tin dilaurates
Dibutyl tin, 1-2 part mould inhibitor, start vavuum pump and agitator, reactor internal pressure is less than 2666pa, are heated to 90 DEG C, guarantor
Hold 20 minutes, be cooled to room temperature, obtain hot glue；
Step 13：Take 50% pre-emulsion and hot glue to stir mix, heating is stirred, temperature control is at 60-70 DEG C, 3min,
10-12 parts of deionized waters are added, continue the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 14：After insulation terminates, 70 DEG C are cooled to, 3-5 parts of hydrogen peroxide and 1-2 parts of ascorbic acid are sequentially added；
Step 15：Continue to cool, be cooled to 60 DEG C, sequentially add 3-6 parts of bleeding agents and 1-2 parts of defoamers；
Step 16：Continue to drop, temperature is cooled to 50 DEG C, and 1-2 parts of amine curing agents obtain mixture two；
Step 17：30-32 parts of flour are taken, not dilute pasty state cannot be tuned into dryly with cold water, mixture one and mixture two are added
Enter mixing, stirring, uniformly, 45 DEG C of insulations obtain cleaning agent.
Beneficial effect：Cleaning agent is applied on wood artwork, after cooling, forms glue, i.e. adsorbable fingerprint is torn, letter
It is single effectively to penetrate into inside wooden product, meanwhile, this product is nontoxic, and wooden product surface nondestructive is done harm to, formed after glue,
The fine impurities on wooden product surface can also effectively be removed.
Contrast existing cleaning agent：
Embodiment：
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1：A kind of preparation method of wood artwork fingerprint surface cleaning agent, comprises the following steps：
Step 1：Start the agitator of reactor, rotating speed is 30r/min, while adding 50 parts of deionized water；
Step 2：After 5-10min, 1 part of emulsifying agent is added；
Step 3：After 5-10min, 3 parts of epoxy resin and 2 parts of methyl epoxy resin is added；
Step 4：After 5-10min, 6 parts of epoxy resin esters and 1 part of methyl epoxy resin ester and epoxy resin butyl ester are added
Mixture；
Step 5：After 5-10min, 0.5 part of chain-transferring agent is added；
Step 6：The initiator of 1 part of addition, is added after initiator, rotating speed increases to 85r/min, time 30min, obtains pre-
Emulsion；
Step 7：Take 30 parts of blood meals to be immersed in distilled water, keep distilled water temperature control at 28-30 DEG C, soak duration 4-
5 hours, amount of distilled water was four times of blood meal；6 part of 20% aqueous sodium carbonate is added in distilled water, stirred 2-3 hours；Together
When allotment 3 parts of calcium hydroxides and 15 parts of distilled water, stir, mixing speed 20-30r/min was stirred once per 3-5 minutes,
Duration 3 minutes, removes surfactant foam at any time, and wood pulp to be mixed proposes glue surface, and silk is broken into glue peptone to defluent glue immediately
Shape, cooling；
Step 8：Take 50% pre-emulsion and glue peptone shape object to stir mix, heating is stirred, temperature control at 60-70 DEG C,
3min, adds 10 parts of deionized waters, continues the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 9：After insulation terminates, 70 DEG C are cooled to, 3 parts of hydrogen peroxide and 1 part of ascorbic acid are sequentially added；
Step 10：Continue to cool, be cooled to 60 DEG C, sequentially add 3 parts of bleeding agents and 1 part of defoamer；
Step 11：Continue to drop, temperature is cooled to 50 DEG C, and 1 part of amine curing agent obtains mixture one；
Step 12：13 parts of castor oil and 6 parts of carboxy-propyl celluloses are taken, adds in reactor, starts vavuum pump and agitator,
Reactor internal pressure is less than 2666pa, be evacuated 2 hours at 100-120 DEG C, be cooled to room temperature, add 1 part of di lauric dibutyl
Tin, 1 part of mould inhibitor, start vavuum pump and agitator, reactor internal pressure is less than 2666pa, are heated to 90 DEG C, are kept for 20 minutes,
It is cooled to room temperature, obtains hot glue；
Step 13：Take 50% pre-emulsion and hot glue to stir mix, heating is stirred, temperature control is at 60-70 DEG C, 3min,
10 parts of deionized waters are added, continue the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 14：After insulation terminates, 70 DEG C are cooled to, 3 parts of hydrogen peroxide and 1 part of ascorbic acid are sequentially added；
Step 15：Continue to cool, be cooled to 60 DEG C, sequentially add 3 parts of bleeding agents and 1 part of defoamer；
Step 16：Continue to drop, temperature is cooled to 50 DEG C, and 1 part of amine curing agent obtains mixture two；
Step 17：30 parts of flour are taken, not dilute pasty state cannot be tuned into dryly with cold water, mixture one and mixture two are added mixed
Close, stirring, uniformly, 45 DEG C of insulations obtain cleaning agent.
Embodiment 2：A kind of preparation method of wood artwork fingerprint surface cleaning agent, comprises the following steps：
Step 1：Start the agitator of reactor, rotating speed is 30r/min, while adding 60 parts of deionized water；
Step 2：After 5-10min, 2 parts of emulsifying agents are added；
Step 3：After 5-10min, 6 parts of epoxy resin and 3 parts of methyl epoxy resin is added；
Step 4：After 5-10min, 9 parts of epoxy resin esters and 2 parts of methyl epoxy resin esters and epoxy resin butyl ester are added
Mixture；
Step 5：After 5-10min, 1 part of chain-transferring agent is added；
Step 6：The initiator of 2 parts of addition, is added after initiator, rotating speed increases to 85r/min, time 30min, obtains pre-
Emulsion；
Step 7：Take 35 parts of blood meals to be immersed in distilled water, keep distilled water temperature control at 28-30 DEG C, soak duration 4-
5 hours, amount of distilled water was four times of blood meal；12 part of 20% aqueous sodium carbonate is added in distilled water, stirred 2-3 hours；
6 parts of calcium hydroxides and 23 parts of distilled water are allocated simultaneously, are stirred, mixing speed 20-30r/min, the stirring one per 3-5 minutes
Secondary, duration 3 minutes removes surfactant foam at any time, and wood pulp to be mixed proposes glue surface, and silk is broken into glue to defluent glue immediately
Peptone shape, cooling；
Step 8：Take 50% pre-emulsion and glue peptone shape object to stir mix, heating is stirred, temperature control at 60-70 DEG C,
3min, adds 12 parts of deionized waters, continues the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 9：After insulation terminates, 70 DEG C are cooled to, 5 parts of hydrogen peroxide and 2 parts of ascorbic acid are sequentially added；
Step 10：Continue to cool, be cooled to 60 DEG C, sequentially add 6 parts of bleeding agents and 2 parts of defoamers；
Step 11：Continue to drop, temperature is cooled to 50 DEG C, and 2 parts of amine curing agents obtain mixture one；
Step 12：15 parts of castor oil and 8 parts of carboxy-propyl celluloses are taken, adds in reactor, starts vavuum pump and agitator,
Reactor internal pressure is less than 2666pa, be evacuated 2 hours at 100-120 DEG C, be cooled to room temperature, add 3 parts of di lauric dibutyls
Tin, 2 parts of mould inhibitors, start vavuum pump and agitator, reactor internal pressure is less than 2666pa, are heated to 90 DEG C, are kept for 20 minutes,
It is cooled to room temperature, obtains hot glue；
Step 13：Take 50% pre-emulsion and hot glue to stir mix, heating is stirred, temperature control is at 60-70 DEG C, 3min,
12 parts of deionized waters are added, continue the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 14：After insulation terminates, 70 DEG C are cooled to, 5 parts of hydrogen peroxide and 2 parts of ascorbic acid are sequentially added；
Step 15：Continue to cool, be cooled to 60 DEG C, sequentially add 6 parts of bleeding agents and 2 parts of defoamers；
Step 16：Continue to drop, temperature is cooled to 50 DEG C, and 2 parts of amine curing agents obtain mixture two；
Step 17：32 parts of flour are taken, not dilute pasty state cannot be tuned into dryly with cold water, mixture one and mixture two are added mixed
Close, stirring, uniformly, 45 DEG C of insulations obtain cleaning agent.
General principle, principal character and the advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (1)
1. a kind of preparation method of wood artwork fingerprint surface cleaning agent, it is characterised in that：Comprise the following steps：
Step 1：Start the agitator of reactor, rotating speed is 30r/min, while adding 50-60 parts of deionized water；
Step 2：After 5-10min, 1-2 parts of emulsifying agents are added；
Step 3：After 5-10min, 3-6 parts of epoxy resin and 2-3 parts of methyl epoxy resin is added；
Step 4：After 5-10min, 6-9 parts of epoxy resin esters and 1-2 parts of methyl epoxy resin esters and epoxy resin butyl ester are added
Mixture；
Step 5：After 5-10min, 0.5-1 parts of chain-transferring agent is added；
Step 6：The initiator of 1-2 parts of addition, is added after initiator, rotating speed increases to 85r/min, time 30min, obtains pre- breast
Change liquid；
Step 7：Take 30-35 parts of blood meals to be immersed in distilled water, keep distilled water temperature control at 28-30 DEG C, soak duration 4-5
Hour, amount of distilled water is four times of blood meal；The aqueous sodium carbonate of 6-12 parts 20% is added in distilled water, stirred 2-3 hours；
3-6 parts of calcium hydroxides of allotment and 15-23 parts of distilled water, stir simultaneously, and mixing speed 20-30r/min is every to stir within 3-5 minutes
Mix once, duration 3 minutes, surfactant foam is removed at any time, wood pulp to be mixed proposes glue surface, and silk breaks defluent glue immediately
Into glue peptone shape, cooling；
Step 8：Take 50% pre-emulsion and glue peptone shape object to stir mix, heating is stirred, temperature control is at 60-70 DEG C, 3min,
10-12 parts of deionized waters are added, continue the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 9：After insulation terminates, 70 DEG C are cooled to, 3-5 parts of hydrogen peroxide and 1-2 parts of ascorbic acid are sequentially added；
Step 10：Continue to cool, be cooled to 60 DEG C, sequentially add 3-6 parts of bleeding agents and 1-2 parts of defoamers；
Step 11：Continue to drop, temperature is cooled to 50 DEG C, and 1-2 parts of amine curing agents obtain mixture one；
Step 12：13-15 parts of castor oil and 6-8 parts of carboxy-propyl celluloses are taken, adds in reactor, starts vavuum pump and stirring
Device, makes reactor internal pressure be less than 2666pa, is evacuated 2 hours at 100-120 DEG C, is cooled to room temperature, adds 1-3 parts of tin dilaurates two
Butyl tin, 1-2 part mould inhibitor, start vavuum pump and agitator, reactor internal pressure is less than 2666pa, are heated to 90 DEG C, holding
20 minutes, it is cooled to room temperature, obtains hot glue；
Step 13：Take 50% pre-emulsion to stir with hot glue to mix, heating stirring, temperature control is at 60-70 DEG C, and 3min is added
10-12 parts of deionized waters, continue the stirring that heats up, temperature control is at 90-98 DEG C, and 3min is incubated 30min afterwards；
Step 14：After insulation terminates, 70 DEG C are cooled to, 3-5 parts of hydrogen peroxide and 1-2 parts of ascorbic acid are sequentially added；
Step 15：Continue to cool, be cooled to 60 DEG C, sequentially add 3-6 parts of bleeding agents and 1-2 parts of defoamers；
Step 16：Continue to drop, temperature is cooled to 50 DEG C, and 1-2 parts of amine curing agents obtain mixture two；
Step 17：30-32 parts of flour are taken, not dilute pasty state cannot be tuned into dryly with cold water, mixture one and mixture two are added mixed
Close, stirring, uniformly, 45 DEG C of insulations obtain cleaning agent.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710297784.2A CN107022429A (en) | 2017-04-29 | 2017-04-29 | A kind of preparation method of wood artwork fingerprint surface cleaning agent |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710297784.2A CN107022429A (en) | 2017-04-29 | 2017-04-29 | A kind of preparation method of wood artwork fingerprint surface cleaning agent |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN107022429A true CN107022429A (en) | 2017-08-08 |
Family
ID=59527575
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710297784.2A Pending CN107022429A (en) | 2017-04-29 | 2017-04-29 | A kind of preparation method of wood artwork fingerprint surface cleaning agent |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN107022429A (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013169994A2 (en) * | 2012-05-11 | 2013-11-14 | President And Fellows Of Harvard College | Reconfigurable surfaces for information security and protection of physical biometrics |
| CN103740504A (en) * | 2013-12-10 | 2014-04-23 | 李翠 | Cleaning agent used for cleaning surfaces of file cabinets |
| CN103849471A (en) * | 2014-03-17 | 2014-06-11 | 苏州龙腾万里化工科技有限公司 | Cleaning agent for fingerprint oil stains |
| CN104531390A (en) * | 2014-12-27 | 2015-04-22 | 湖北吉隆表面工程有限公司 | Fingerprint cleaning fluid |
-
2017
- 2017-04-29 CN CN201710297784.2A patent/CN107022429A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| WO2013169994A2 (en) * | 2012-05-11 | 2013-11-14 | President And Fellows Of Harvard College | Reconfigurable surfaces for information security and protection of physical biometrics |
| CN103740504A (en) * | 2013-12-10 | 2014-04-23 | 李翠 | Cleaning agent used for cleaning surfaces of file cabinets |
| CN103849471A (en) * | 2014-03-17 | 2014-06-11 | 苏州龙腾万里化工科技有限公司 | Cleaning agent for fingerprint oil stains |
| CN104531390A (en) * | 2014-12-27 | 2015-04-22 | 湖北吉隆表面工程有限公司 | Fingerprint cleaning fluid |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN105767932B (en) | A kind of production method of fast food type fermented glutinous rice egg or bird's nest | |
| CN102125511B (en) | Tendering, whitening and moisturizing cream and preparation method thereof | |
| CN104892970A (en) | Method for directly preparing membrane through wood fiber | |
| CN101601494B (en) | Safe high-efficiency green bean product preservative and production method thereof | |
| CN101601495A (en) | Safe high-efficiency green Bread and Cakes antistaling agent and production method thereof | |
| CN107022429A (en) | A kind of preparation method of wood artwork fingerprint surface cleaning agent | |
| CN106811349A (en) | A kind of emulsifying cleaning agent and preparation method | |
| CN104387480A (en) | Preparation method of waxy corn modified starch capable of improving quality of frozen food | |
| CN106551021A (en) | A kind of processing method of seasoning black tea | |
| CN104073217A (en) | Formula and preparation process of high-quality blood glue | |
| CN106978279A (en) | A kind of preparation method of wood artwork surface oil stain cleanser | |
| CN104172321A (en) | Pork soup stock and preparation method thereof | |
| CN106831939A (en) | A kind of tussah silk protein extracting method | |
| CN107057637A (en) | Suitable for wooden and other irregular handicraft surface dust cleanings cleaning agent preparation methods | |
| CN110897110A (en) | High-calcium fish gelatin cake and preparation method thereof | |
| CN102952632A (en) | Method for refining prickly ash seed oil | |
| CN109645103A (en) | A kind of preparation method of grape drying promoter | |
| CN106942570A (en) | A kind of fresh goat milk removes the biological method having a strong smell | |
| CN107474990A (en) | A kind of environmentally friendly glass cleaner and preparation method thereof | |
| CN103315306B (en) | A kind of sugared butcher's meat | |
| CN109651757A (en) | A kind of preparation method of high-performance modified phenolic resin cold-storage insulation board | |
| CN105567421A (en) | Degumming technology of fragrant oil-tea camellia seed oil | |
| CN104473854A (en) | Skin whitening emulsion and preparation method thereof | |
| CN110305343A (en) | A kind of PVC glove and preparation method thereof | |
| CN104207036B (en) | Producing technology of oil-fried broad bean tin |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170808 |
|
| RJ01 | Rejection of invention patent application after publication |