CN107014663A - Suitable for the sample method for making sample of mineralogy parameter automatic measurement system - Google Patents
Suitable for the sample method for making sample of mineralogy parameter automatic measurement system Download PDFInfo
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- CN107014663A CN107014663A CN201710218947.3A CN201710218947A CN107014663A CN 107014663 A CN107014663 A CN 107014663A CN 201710218947 A CN201710218947 A CN 201710218947A CN 107014663 A CN107014663 A CN 107014663A
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- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N1/00—Sampling; Preparing specimens for investigation
- G01N1/28—Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
- G01N1/36—Embedding or analogous mounting of samples
- G01N2001/364—Embedding or analogous mounting of samples using resins, epoxy
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2223/00—Investigating materials by wave or particle radiation
- G01N2223/07—Investigating materials by wave or particle radiation secondary emission
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N23/00—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00
- G01N23/22—Investigating or analysing materials by the use of wave or particle radiation, e.g. X-rays or neutrons, not covered by groups G01N3/00 – G01N17/00, G01N21/00 or G01N22/00 by measuring secondary emission from the material
- G01N23/2202—Preparing specimens therefor
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- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Pathology (AREA)
- Sampling And Sample Adjustment (AREA)
Abstract
The present invention relates to a kind of sample method for making sample suitable for mineralogy parameter automatic measurement system, belong to method for making sample.Use sample ore hybrid resin glue and carry out cold embedding method, cutting goes out cross section progress secondary resin inlaying process to the resin mating plate of embedding completion cold for the first time again, after resin mating plate after secondary inlay is handled by corase grind, fine grinding, fine grinding, polishing and surface conductance, it is fabricated to that surface grinding face is good, mineral are representative comprehensively and the mineral samplers mating plate with satisfactory electrical conductivity.The sample that the present invention is manufactured using the secondary cold embedding method of hybrid resin glue has good dispersion, clear easily observation, mineral species are covered comprehensively, representative strong the features such as, it is practical and sample making course is simple to operation, it is widely used, the mating plate of making is applicable to automatic mineralogy measuring system detection, is also applied for detecting under electron probe, ESEM and metallographic microscope.
Description
Technical field
The present invention relates to a kind of method of sample preparation, MLA (Mineral liberation Analyser) is applied especially to i.e.
Mineralogy parameter automatic measurement system, is particularly suitable for use in that ore sample granularity is thinner, the making of below 50um testing sample,
It can be used as manufacturing for the Instrument observation sample such as microscope and electron probe, ESEM.
Background technology
With the introducing of mineralogy parameter automatic measurement system, process mineralogy field enters a brand-new epoch, its
Fast and accurately measurement result, makes the development that our daily process mineralogies work get twice the result with half the effort.But early stage measurement sample
Manufacturing process be then most critical in whole measurement process a step, made sample can representativeness be directly connected to subsequently to go out
The data of tool and the order of accuarcy of conclusion.Especially for below 50um mineral product sample, due to its fine size, it is not easy to
The sample for being used under Electronic Speculum and metallographic microscope be available for observation that is scattered, being produced by current method, makes measurement data can not
Really and accurately embody.
The content of the invention
The present invention provides a kind of sample method for making sample suitable for mineralogy parameter automatic measurement system, to solve fine fraction
Ore sample be difficult to detect under mineralogy parameter automatic measurement system and ESEM, electron microscope, measurement data
The problem of inadequate true and accurate.
The present invention is adopted the technical scheme that：Comprise the following steps：
(1) ore sample for taking 1g-3g representative, it is ensured that ore sample drying loads prior without being mixed after caking
Painting is wiped in the mould of adhesion protective oil, and the mould of sample used in automatic mineralogy parameter measurement system is internal diameter 30mm, height 30mm
Cylindric plastic mould；
(2) resin glue is proportionally prepared, a resin mating plate needs to prepare 7ml resin glue, by the resin prepared
Glue, which is sufficiently mixed, to be stirred, and in order to reduce bubble formation, the process of stirring will be slowly stirred in one direction；
(3) resin glue stirred is injected in the mould equipped with ore sample, is gently mixed in one direction, it is ensured that
Sample ore is not bonded to bottom and mould corner, sample ore is sufficiently mixed uniformly with resin glue；
(4) mould after step (3) is stirred is put into ultrasonic oscillation device, shakes 30min, the effect of concussion be in order to
Minute bubbles in Scavenger resin glue mixture, make sample ore be sufficiently mixed and disperse wherein with resin glue；
(5) mould is taken out after the completion of shaking, then moves into baking oven, 50 DEG C of baking 2h will ensure mould when mould is put into baking oven
Has bottom level；
(6) mould in baking oven is taken out after 2h and 30~40min is cooled down, after thing to be mixed cooling completely, resin glue mixing
When thing is fully hardened, texture is hard, resin mating plate one is taken out in first time sample preparation success, the demoulding；
(7) by the resin mating plate one being made in step (6) with slicer it is longitudinally cutting, i.e., along with the diameter of resin mating plate one
Parallel and distance with the diameter is located longitudinally cutting for 0.5~1.0mm, chooses and under cutting, relatively small is used as resin mating plate
Two, its cutaway section is rectangle AA ' B ' B, is cut again with slicer at the plane away from 3~3.3mm of the rectangle cutaway section,
It regard the resin mating plate two of cutting twice interplanar as resin mating plate three；
(8) cutting plane of resin mating plate three, by cutting described in step (7) after qualified is clean with alcohol washes, after drying
Loading is coated in the mould of adhesion protective oil, and the mould is the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter
30mm, height 30mm cylindric the modern designs of plastics；Cutting cross section AA ' B ' B are ensured when placing resin mating plate three all the time down, then
The small paper slip for being trimmed to 10mm × 20mm is taken, sample number into spectrum and title is finished writing, label is made and is placed on resin mating plate three；
(9) the same step of resin glue (2) prepared during secondary sample preparation, after the completion of resin glue is prepared, pours into and is equipped with step (8)
In the mould of cutting resin mating plate three and label, then mould sent into baking oven, it is cold that 50 DEG C of bakings take out mould after 2 hours, 2 hours
But, be cooled to resin mating plate it is hard after, then be stripped taking-up resin mating plate, complete the making of resin mating plate four.
(10) the resin mating plate four made face as shown in Figure 4, after corase grind, fine grinding, fine grinding and polishing, then to table
Spray carbon processing is done in face, and so far mineralogy parameter automatic measurement system detection is completed with sample making.
The present invention uses sample ore hybrid resin glue and carries out cold embedding method, and the resin mating plate of first time cold embedding completion is again
Cutting, carries out secondary resin inlaying process, can so avoid the mineral grain weight layering due to being caused when first time inlays, inspection
Survey the incomplete problem of interval scale.Resin mating plate after secondary inlay passes through corase grind, fine grinding, fine grinding, polishing and surface
After conductive processing, it is fabricated to that surface grinding face is good, mineral are representative comprehensively and the mineral samplers mating plate with satisfactory electrical conductivity, this
The mating plate that the method for kind makes is applicable to automatic mineralogy measuring system detection, is also applied for electron probe, ESEM and gold
Detected under phase microscope.
The sample that the present invention is manufactured using the secondary cold embedding method of hybrid resin glue has good dispersion, clear easily to see
Examine, mineral species are covered comprehensively, the features such as representative strong, and sample making course is simple to operation, practical, is widely used.Adopt
Method for making sample with the present invention be at present since a kind of most easy and effective, and easy-operating process.
The method for making sample of the present invention can solve fine-graded ore sample and be difficult to observe this difficult, institute's sample preparation under mirror
Product can be not only used for the measurement of mineralogy parameter automatic measurement system, it can also be used to electron probe, ESEM and other
Various metallographic microscope observations, the made resin mating plate facet of the method is good, and mineral species and granularity cover comprehensively, with very strong
Representativeness.It is practical and sample making course is simple to operation, it is widely used.
Brief description of the drawings
Fig. 1 is the stereogram of resin mating plate one being made after once inlaying the demoulding, and dashed part is that step (7) is cut
Line of cut when cutting；
Fig. 2 is the schematic diagram for once inlaying the resin light three being made, and its cutaway section is rectangle AA ' B ' B；
Fig. 3 is the ABB'A' section top views of resin mating plate three, there is mineral weight particle lamination；
Fig. 4 is the face to be detected by the mineral samplers resin mating plate four after the completion of secondary inlay.
Embodiment
Embodiment 1
Comprise the following steps：
(1) ore sample for taking 1g representative, it is ensured that ore sample drying loads and smeared in advance without being mixed after caking
In the mould of good adhesion protective oil, the mould of sample used in automatic mineralogy parameter measurement system is internal diameter 30mm, height 30mm circle
Column plastic mould；
(2) resin glue is proportionally prepared, a resin mating plate needs to prepare 7ml resin glue, by the resin prepared
Glue, which is sufficiently mixed, to be stirred, and in order to reduce bubble formation, the process of stirring will be slowly stirred in one direction；
(3) resin glue stirred is injected in the mould equipped with ore sample, is gently mixed in one direction, it is ensured that
Sample ore is not bonded to bottom and mould corner, sample ore is sufficiently mixed uniformly with resin glue；
(4) mould after step (3) is stirred is put into ultrasonic oscillation device, shakes 30min, the effect of concussion be in order to
Minute bubbles in Scavenger resin glue mixture, make sample ore be sufficiently mixed and disperse wherein with resin glue；
(5) mould is taken out after the completion of shaking, then moves into baking oven, 50 DEG C of baking 2h will ensure mould when mould is put into baking oven
Has bottom level；
(6) mould in baking oven is taken out after 2h and 30min is cooled down, after thing to be mixed cooling completely, resin glue mixture is
When fully hardened, texture is hard, resin mating plate 1 is taken out in first time sample preparation success, the demoulding；
(7) by the resin mating plate one being made in step (6) with slicer it is longitudinally cutting, i.e., along with the diameter of resin mating plate one
Parallel and distance with the diameter is located longitudinally cutting for 0.5mm, chooses under cutting, relatively small as resin mating plate 22, its
Cutaway section is rectangle AA ' B ' B, is cut again with slicer at the plane away from rectangle cutaway section 3mm, by cutting twice
The resin mating plate two of interplanar is used as resin mating plate 33；Referring to Fig. 1, Fig. 2 and Fig. 3；
(8) cutting plane of resin mating plate three, by cutting described in step (7) after qualified is clean with alcohol washes, after drying
Loading is coated in the mould of adhesion protective oil, and the mould is the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter
30mm, height 30mm cylindric the modern designs of plastics；Cutting cross section AA ' B ' B are ensured when placing resin mating plate three all the time down, then
The small paper slip for being trimmed to 10mm × 20mm is taken, sample number into spectrum and title is finished writing, label is made and is placed on resin mating plate 33；
(9) the same step of resin glue (2) prepared during secondary sample preparation, after the completion of resin glue is prepared, pours into and is equipped with step (8)
In the mould of cutting resin mating plate three and label, then mould sent into baking oven, it is cold that 50 DEG C of bakings take out mould after 2 hours, 2 hours
But, be cooled to resin mating plate it is hard after, then be stripped taking-up resin mating plate, complete the making of resin mating plate 44.
(10) the resin mating plate four made, face, after corase grind, fine grinding, fine grinding and polishing, then gives as shown in Figure 4
Spray carbon processing is done on surface, and so far mineralogy parameter automatic measurement system detection is completed with sample making.
Embodiment 2
Comprise the following steps：
(1) ore sample for taking 2g representative, it is ensured that ore sample drying loads and smeared in advance without being mixed after caking
In the mould of good adhesion protective oil, the mould of sample used in automatic mineralogy parameter measurement system is internal diameter 30mm, height 30mm circle
Column plastic mould；
(2) resin glue is proportionally prepared, a resin mating plate needs to prepare 7ml resin glue, by the resin prepared
Glue, which is sufficiently mixed, to be stirred, and in order to reduce bubble formation, the process of stirring will be slowly stirred in one direction；
(3) resin glue stirred is injected in the mould equipped with ore sample, is gently mixed in one direction, it is ensured that
Sample ore is not bonded to bottom and mould corner, sample ore is sufficiently mixed uniformly with resin glue；
(4) mould after step (3) is stirred is put into ultrasonic oscillation device, shakes 30min, the effect of concussion be in order to
Minute bubbles in Scavenger resin glue mixture, make sample ore be sufficiently mixed and disperse wherein with resin glue；
(5) mould is taken out after the completion of shaking, then moves into baking oven, 50 DEG C of baking 2h will ensure mould when mould is put into baking oven
Has bottom level；
(6) mould in baking oven is taken out after 2h and 35min is cooled down, after thing to be mixed cooling completely, resin glue mixture is
When fully hardened, texture is hard, resin mating plate 1 is taken out in first time sample preparation success, the demoulding；
(7) by the resin mating plate one being made in step (6) with slicer it is longitudinally cutting, i.e., along with the diameter of resin mating plate one
Parallel and distance with the diameter is located longitudinally cutting for 0.7mm, chooses under cutting, relatively small as resin mating plate 22, its
Cutaway section is rectangle AA ' B ' B, is cut, will cut twice with slicer again at the plane away from rectangle cutaway section 3.1mm
Resin mating plate two between cutting plane is used as resin mating plate 33；Referring to Fig. 1, Fig. 2 and Fig. 3；
(8) cutting plane of resin mating plate three, by cutting described in step (7) after qualified is clean with alcohol washes, after drying
Loading is coated in the mould of adhesion protective oil, and the mould is the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter
30mm, height 30mm cylindric the modern designs of plastics；Cutting cross section AA ' B ' B are ensured when placing resin mating plate three all the time down, then
The small paper slip for being trimmed to 10mm × 20mm is taken, sample number into spectrum and title is finished writing, label is made and is placed on resin mating plate three；
(9) the same step of resin glue (2) prepared during secondary sample preparation, after the completion of resin glue is prepared, pours into and is equipped with step (8)
In the mould of cutting resin mating plate three and label, then mould sent into baking oven, it is cold that 50 DEG C of bakings take out mould after 2 hours, 2 hours
But, be cooled to resin mating plate it is hard after, then be stripped taking-up resin mating plate, complete the making of resin mating plate 44.
(10) the resin mating plate four made, face, after corase grind, fine grinding, fine grinding and polishing, then gives as shown in Figure 4
Spray carbon processing is done on surface, and so far mineralogy parameter automatic measurement system detection is completed with sample making.
Embodiment 3
Comprise the following steps：
(1) ore sample for taking 3g representative, it is ensured that ore sample drying loads and smeared in advance without being mixed after caking
In the mould of good adhesion protective oil, the mould of sample used in automatic mineralogy parameter measurement system is internal diameter 30mm, height 30mm circle
Column plastic mould；
(2) resin glue is proportionally prepared, a resin mating plate needs to prepare 7ml resin glue, by the resin prepared
Glue, which is sufficiently mixed, to be stirred, and in order to reduce bubble formation, the process of stirring will be slowly stirred in one direction；
(3) resin glue stirred is injected in the mould equipped with ore sample, is gently mixed in one direction, it is ensured that
Sample ore is not bonded to bottom and mould corner, sample ore is sufficiently mixed uniformly with resin glue；
(4) mould after step (3) is stirred is put into ultrasonic oscillation device, shakes 30min, the effect of concussion be in order to
Minute bubbles in Scavenger resin glue mixture, make sample ore be sufficiently mixed and disperse wherein with resin glue；
(5) mould is taken out after the completion of shaking, then moves into baking oven, 50 DEG C of baking 2h will ensure mould when mould is put into baking oven
Has bottom level；
(6) mould in baking oven is taken out after 2h and 40min is cooled down, after thing to be mixed cooling completely, resin glue mixture is
When fully hardened, texture is hard, resin mating plate 1 is taken out in first time sample preparation success, the demoulding；
(7) it is the resin mating plate being made in step (6) is longitudinally cutting with slicer, i.e., along with the diameter of resin mating plate one
Parallel and distance with the diameter is located longitudinally cutting for 1.0mm, chooses under cutting, relatively small as resin mating plate 22, its
Cutaway section is rectangle AA ' B ' B, is cut, will cut twice with slicer again at the plane away from rectangle cutaway section 3.3mm
Resin mating plate two between cutting plane is used as resin mating plate three；Referring to Fig. 1, Fig. 2 and Fig. 3；
(8) cutting plane of resin mating plate three, by cutting described in step (7) after qualified is clean with alcohol washes, after drying
Loading is coated in the mould of adhesion protective oil, and the mould is the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter
30mm, height 30mm cylindric the modern designs of plastics；Cutting cross section AA ' B ' B are ensured when placing resin mating plate three all the time down, then
The small paper slip for being trimmed to 10mm × 20mm is taken, sample number into spectrum and title is finished writing, label is made and is placed on resin mating plate three；
(9) the same step of resin glue (2) prepared during secondary sample preparation, after the completion of resin glue is prepared, pours into and is equipped with step (8)
In the mould of cutting resin mating plate three and label, then mould sent into baking oven, it is cold that 50 DEG C of bakings take out mould after 2 hours, 2 hours
But, be cooled to resin mating plate it is hard after, then be stripped taking-up resin mating plate, complete the making of resin mating plate 44.
(10) the resin mating plate four made, face, after corase grind, fine grinding, fine grinding and polishing, then gives as shown in Figure 4
Spray carbon processing is done on surface, and so far mineralogy parameter automatic measurement system detection is completed with sample making.
The present invention also can continue the multiple cross sections of cutting according to the actual requirements, the thickness of cutting cross section 3mm with
On, maximize retain transversal cutting plane while, can be according to cutting away other corner parts, it is ensured that cutting plane can be put into mould
Interior, according to different demands several samples can be made with cutting into several cutting planes in a resin sheet.
Claims (3)
1. a kind of sample method for making sample suitable for mineralogy parameter automatic measurement system, comprises the following steps：
(1) ore sample for taking 1g-3g representative, it is ensured that ore sample drying loads and smeared in advance without being mixed after caking
In the mould of good adhesion protective oil；
(2) resin glue is proportionally prepared, a resin mating plate needs to prepare 7ml resin glue, the resin glue prepared is filled
Divide and be mixed evenly, the process of stirring will be slowly stirred in one direction；
(3) resin glue stirred is injected in the mould equipped with ore sample, be gently mixed in one direction, it is ensured that sample ore
Bottom and mould corner are not bonded to, sample ore is sufficiently mixed uniformly with resin glue；
It is characterized in that：
(4) mould after step (3) is stirred is put into ultrasonic oscillation device, shakes 30min, sample ore is fully mixed with resin glue
Merge and disperse wherein；
(5) mould is taken out after the completion of shaking, then moves into baking oven, 50 DEG C of baking 2h will ensure mould bottom when mould is put into baking oven
Portion's level；
(6) mould in baking oven is taken out after 2h and 30~40min is cooled down, after thing to be mixed cooling completely, resin glue mixture is
When fully hardened, texture is hard, resin mating plate one is taken out in first time sample preparation success, the demoulding；
(7) by the resin mating plate one being made in step (6) with slicer it is longitudinally cutting, i.e., along with the diameter parallel of resin mating plate one
And locate with the distance of the diameter for 0.5~1.0mm longitudinally cutting, choose under cutting, relatively small as resin mating plate two, its
Cutaway section is rectangle AA ' B ' B, is cut again with slicer at the plane away from 3~3.3mm of the rectangle cutaway section, by two
Resin mating plate two between secondary cutting planes is used as resin mating plate three；
(8) cutting plane of resin mating plate three, by cutting described in step (7) after qualified is clean with alcohol washes, loads after drying
Coat in the mould of adhesion protective oil；Cutting cross section AA ' B ' B are ensured when placing resin mating plate three all the time down, then takes and is trimmed to
10mm × 20mm small paper slip, finishes writing sample number into spectrum and title, and label is made and is placed on resin mating plate three；
(9) the same step of resin glue (2) prepared during secondary sample preparation, after the completion of resin glue is prepared, pours into and cutting is housed in step (8)
In the mould of resin mating plate three and label, then mould sent into baking oven, 50 DEG C of bakings take out mould cooling after 2 hours, 2 hours,
Be cooled to resin mating plate it is hard after, then be stripped taking-up resin mating plate, complete the making of resin mating plate four.
(10) the resin mating plate four made face as shown in Figure 4, does after corase grind, fine grinding, fine grinding and polishing, then to surface
Spray carbon processing.
2. a kind of sample method for making sample suitable for mineralogy parameter automatic measurement system according to claim 1, it is special
Levy and be：Step (1) mould therefor uses the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter 30mm, high
Spend 30mm cylindric plastic mould.
3. a kind of sample method for making sample suitable for mineralogy parameter automatic measurement system according to claim 1, it is special
Levy and be：Step (8) mould therefor uses the mould of sample used in automatic mineralogy parameter measurement system, is internal diameter 30mm, high
Spend 30mm cylindric plastic mould.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710218947.3A CN107014663A (en) | 2017-04-05 | 2017-04-05 | Suitable for the sample method for making sample of mineralogy parameter automatic measurement system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710218947.3A CN107014663A (en) | 2017-04-05 | 2017-04-05 | Suitable for the sample method for making sample of mineralogy parameter automatic measurement system |
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| CN107014663A true CN107014663A (en) | 2017-08-04 |
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| CN201710218947.3A Pending CN107014663A (en) | 2017-04-05 | 2017-04-05 | Suitable for the sample method for making sample of mineralogy parameter automatic measurement system |
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Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109708937A (en) * | 2018-12-28 | 2019-05-03 | 南京钢铁股份有限公司 | A kind of application diameter or thickness are less than the method for embedding of 2mm or less product |
| CN112378940A (en) * | 2020-09-30 | 2021-02-19 | 长春黄金研究院有限公司 | Method for measuring gold content of gold-loaded mineral |
| CN113092467A (en) * | 2020-11-06 | 2021-07-09 | 长江大学 | Intelligent microscopic identification quantitative system for whole rock slide |
| CN113252417A (en) * | 2021-05-12 | 2021-08-13 | 合肥工业大学 | Method for preparing resin target sheet for TIMA mineral analysis system from industrial mineral fine powder |
| CN113432943A (en) * | 2021-06-17 | 2021-09-24 | 攀钢集团攀枝花钢铁研究院有限公司 | Preparation method of rock and ore sample transmission light sheet |
| CN114112616A (en) * | 2021-11-23 | 2022-03-01 | 云南磷化集团有限公司 | Method for preparing MLA (Multi-layer array) testing resin polished section by collophanite powder sample |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103411807A (en) * | 2013-08-01 | 2013-11-27 | 同济大学 | Sample preparation method for inorganic nonmetal powder material for backscattered electron image and energy spectrum study |
| CN103492851A (en) * | 2011-04-22 | 2014-01-01 | Fei公司 | Automated sample preparation |
| CN104142261A (en) * | 2014-07-14 | 2014-11-12 | 中国矿业大学 | Method and device for rapidly manufacturing pulverized coal polished section by ultrasonic defoaming |
| JP2016050919A (en) * | 2014-09-02 | 2016-04-11 | 住友金属鉱山株式会社 | Sample preparation method |
-
2017
- 2017-04-05 CN CN201710218947.3A patent/CN107014663A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103492851A (en) * | 2011-04-22 | 2014-01-01 | Fei公司 | Automated sample preparation |
| CN103411807A (en) * | 2013-08-01 | 2013-11-27 | 同济大学 | Sample preparation method for inorganic nonmetal powder material for backscattered electron image and energy spectrum study |
| CN104142261A (en) * | 2014-07-14 | 2014-11-12 | 中国矿业大学 | Method and device for rapidly manufacturing pulverized coal polished section by ultrasonic defoaming |
| JP2016050919A (en) * | 2014-09-02 | 2016-04-11 | 住友金属鉱山株式会社 | Sample preparation method |
Non-Patent Citations (6)
| Title |
|---|
| A331917223: "MLA岩相样品制备", 《百度文库：HTTPS://WENKU.BAIDU.COM/VIEW/E5D23E410066F5335A81217C.HTML》 * |
| MOSTAFA REDWAN等: "UNDERSTANDING MICRO-ENVIRONMENT DEVELOPMENT IN MINE TAILINGS USING MLA AND IMAGE ANALYSIS", 《PROCEEDINGS OF THE 10TH INTERNATIONAL CONGRESS》 * |
| 庞建涛等: "ＭＬＡ系统在磷块岩工艺矿物学研究中的应用", 《化工矿物与加工》 * |
| 彭永忠: "铜箔缺陷分析技术探索与应用", 《铜业工程》 * |
| 谢菱芳: "砂粒矿物的光片及薄片制备工艺", 《云南冶金》 * |
| 韩德伟等: "《金相试样制备与显示技术 第二版》", 31 May 2014, 中南大学出版社 * |
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