CN106978001A - A kind of attapulgite interior wall putty powder and preparation method thereof - Google Patents

A kind of attapulgite interior wall putty powder and preparation method thereof Download PDF

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Publication number
CN106978001A
CN106978001A CN201710231503.3A CN201710231503A CN106978001A CN 106978001 A CN106978001 A CN 106978001A CN 201710231503 A CN201710231503 A CN 201710231503A CN 106978001 A CN106978001 A CN 106978001A
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parts
interior wall
powder
flyash
wall putty
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王琳
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Mingguang City Axa Non Metal Material Factory
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Mingguang City Axa Non Metal Material Factory
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Priority to CN201710231503.3A priority Critical patent/CN106978001A/en
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    • CCHEMISTRY; METALLURGY
    • C09DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
    • C09DCOATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
    • C09D5/00Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
    • C09D5/34Filling pastes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Processing Of Solid Wastes (AREA)
  • Curing Cements, Concrete, And Artificial Stone (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention discloses a kind of attapulgite interior wall putty powder and preparation method thereof, the powder of lacquer putty for use on includes the raw material of following parts by weight:15 28 parts of Concave-convex clay rod, 10 18 parts of white cement, 5 10 parts of calcium oxide, 18 25 parts of dead plaster, 15 parts of polyacrylamide, 0.6 3 parts of carboxylic propyl methocel, 25 parts of flyash, 0.2 0.5 parts of pure iron powder.The powder of lacquer putty for use on of the present invention is using the high Concave-convex clay rod stronger than variable area, adsorptivity, with reference to calcium oxide, dead plaster, polyacrylamide, flyash so that product environment protection health, pure white, adhesion are strong, and acid-alkali-corrosive-resisting, storage is stable.In addition, by adding pure iron powder so that the coefficient of thermal expansion and contraction of powder of lacquer putty for use on reduces more, will not be big because difference variation and be cracked, improve weatherability, moreover it is possible to harmful electromagnetic radiation in absorption chamber.

Description

A kind of attapulgite interior wall putty powder and preparation method thereof
Technical field
The present invention relates to decorating interior wall building material field, and in particular to a kind of attapulgite interior wall putty powder and its preparation side Method.
Background technology
Powder of lacquer putty for use on is one kind of building and ornament materials, and main component is talcum powder and glue.The rough house table just purchased The white putty of one layer of face, the whiteness of usual putty is more than 90, and fineness is more than 330.Putty is divided into two kinds of interior wall and exterior wall, Exterior wall putty, which will be resisted, exposes to the weather so colloidality is big, intensity is high, and environmentally friendly index is slightly lower.Inner wall putty composite index preferably, is good for Kang Huanbao, so interior wall not external application, exterior wall is not interior to be used.Putty is usually to be made up of base-material, filler, water and auxiliary agent etc..Base-material, Claim binding agent, be the most critical component of putty, mainly play bonding etc. various.The most frequently used binding agent of putty is cement and had Machine polymer, organic polymer has point of emulsion and latex powder again.Cement is that caking property is good, durable and cost performance is reasonably bonded Agent, but tensile strength and crack resistance are poor.Organic polymer can be modified and toughness reinforcing to it, so as to improve putty performance.Filler master Filling effect is played, conventional has calcium carbonate, talcum powder and quartz sand etc..Auxiliary agent has thickener, water-loss reducer etc..
Authorization Notice No. CN103351132B discloses a kind of Environmentally-frieinterior interior wall putty powder, and the powder of lacquer putty for use on is in parts by weight It is made up of following component:15-18 parts of white cement, 3-5 parts of sierozem power, 6- parts of cassava gelatinized starch, 320 mesh powdered whiting 22- 26 parts, 200 3-5 parts of mesh expanded perlites, 1.5-2.5 parts of 3-5mm polypropylene fibres, 2-4 parts of polyvinyl alcohol, carboxymethyl cellulose It is plain 2-3 parts, 2.5-3.5 parts of three-level flyash, 5-7 parts of sodium bentonite, 1-2 parts of prodan, 2-4 parts of dispersant, defoamer 0.4-0.6 parts, 0.2-0.4 parts of mould inhibitor.Powder of lacquer putty for use on freedom from cracking, the non-scale, without poisonous and harmful substance, but composition is more multiple Miscellaneous, cost is higher.
The content of the invention
For the defect of prior art, it is an object of the invention to provide a kind of attapulgite interior wall putty powder and its preparation side Method, the powder of lacquer putty for use on has good water resistance and caking property, weatherability, and composition asepsis environment-protecting.
The present invention solves technical problem and adopted the following technical scheme that:
The invention provides a kind of attapulgite interior wall putty powder, include the raw material of following parts by weight:Concave-convex clay rod 15-28 Part, 10-18 parts of white cement, 5-10 parts of calcium oxide, 18-25 parts of dead plaster, 1-5 parts of polyacrylamide, carboxylic hydroxypropyl methyl are fine Tie up 0.6-3 parts of element, 2-5 parts of flyash, 0.2-0.5 parts of pure iron powder.
Preferably, the inner wall putty powder includes the raw material of following parts by weight:22 parts of Concave-convex clay rod, white cement 16 Part, 8 parts of calcium oxide, 22 parts of dead plaster, 3 parts of polyacrylamide, 1 part of carboxylic propyl methocel, 2 parts of flyash, pure iron 0.5 part of powder.
Preferably, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second.
Preferably, the flyash is one-level or second class powered coal ash.
The preparation method of above-mentioned attapulgite interior wall putty powder, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filtrate is dried after filtering, and the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)80-100 mesh sieves will be crossed after calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder co-grinding, obtained To mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, stirred Mix after 1-2 hours, packed after discharging.
Preferably, the step 1)Dry to dry 3-4 hours at 50-60 DEG C.
Preferably, the step 2)Crushed using micronizer.
Preferably, the step 3)The rotating speed of stirring is 600-800 revs/min.
Compared with prior art, the present invention has following beneficial effect:
The powder of lacquer putty for use on of the present invention is using the high Concave-convex clay rod stronger than variable area, adsorptivity so that powder of lacquer putty for use on has good Adsorption effect, with reference to calcium oxide, dead plaster, polyacrylamide, flyash so that product environment protection health, pure white, adhesion By force, acid-alkali-corrosive-resisting, storage is stable.In addition, by add pure iron powder so that powder of lacquer putty for use on coefficient of thermal expansion and contraction reduce it is more, Weatherability will not be improved because difference variation is big and is cracked, moreover it is possible to the electromagnetic radiation being harmful in absorption chamber.
Embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without In limitation the scope of the present invention.
Embodiment 1.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:22 parts of Concave-convex clay rod, 16 parts of white cement, oxygen Change 8 parts of calcium, 22 parts of dead plaster, 3 parts of polyacrylamide, 1 part of carboxylic propyl methocel, 2 parts of flyash, pure iron powder 0.5 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 2 hours in 50 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 600 revs/min of rotating speed, packed after discharging.
Embodiment 2.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:15 parts of Concave-convex clay rod, 12 parts of white cement, oxygen Change 5 parts of calcium, 20 parts of dead plaster, 3 parts of polyacrylamide, 1 part of carboxylic propyl methocel, 2 parts of flyash, pure iron powder 0.5 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 2 hours in 50 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 600 revs/min of rotating speed, packed after discharging.
Embodiment 3.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:18 parts of Concave-convex clay rod, 15 parts of white cement, oxygen Change 8 parts of calcium, 22 parts of dead plaster, 3 parts of polyacrylamide, 1 part of carboxylic propyl methocel, 2 parts of flyash, pure iron powder 0.2 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 700 revs/min of rotating speed, packed after discharging.
Embodiment 4.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:20 parts of Concave-convex clay rod, 12 parts of white cement, oxygen Change 5 parts of calcium, 18 parts of dead plaster, 1 part of polyacrylamide, 0.8 part of carboxylic propyl methocel, 3 parts of flyash, pure iron powder 0.3 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 700 revs/min of rotating speed, packed after discharging.
Embodiment 5.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:22 parts of Concave-convex clay rod, 14 parts of white cement, oxygen Change 7 parts of calcium, 22 parts of dead plaster, 3 parts of polyacrylamide, 0.8 part of carboxylic propyl methocel, 3 parts of flyash, pure iron powder 0.3 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 800 revs/min of rotating speed, packed after discharging.
Embodiment 6.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:25 parts of Concave-convex clay rod, 15 parts of white cement, oxygen Change 5 parts of calcium, 20 parts of dead plaster, 1.5 parts of polyacrylamide, 0.8 part of carboxylic propyl methocel, 3 parts of flyash, straight iron powder 0.3 part of end, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour Coal ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 800 revs/min of rotating speed, packed after discharging.
Embodiment 7.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:25 parts of Concave-convex clay rod, 18 parts of white cement, oxygen Change 8 parts of calcium, 22 parts of dead plaster, 3 parts of polyacrylamide, 0.8 part of carboxylic propyl methocel, 3 parts of flyash, pure iron powder 0.3 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 800 revs/min of rotating speed, packed after discharging.
Embodiment 8.
A kind of attapulgite interior wall putty powder, includes the raw material of following parts by weight:28 parts of Concave-convex clay rod, 12 parts of white cement, oxygen Change 8 parts of calcium, 22 parts of dead plaster, 3 parts of polyacrylamide, 0.8 part of carboxylic propyl methocel, 5 parts of flyash, pure iron powder 0.5 part, wherein, the viscosity of the carboxylic propyl methocel is 50-100 handkerchiefs/second, and the flyash is one-level or second patent flour coal Ash.
The preparation method of above-mentioned powder of lacquer putty for use on, comprises the following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filter, filtrate is dried 1 hour in 60 DEG C, the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)Calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder are mixed, mistake after micronizer is crushed 80-100 mesh sieves, obtain mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, with After stirring 1-2 hours of 800 revs/min of rotating speed, packed after discharging.
The powder of lacquer putty for use on environment protection health of the present invention, pure white, adhesion are strong, and acid-alkali-corrosive-resisting, storage is stable, and weatherability is strong, The electromagnetic radiation being harmful in energy absorption chamber.
Performance test:According to JG/T 3049-1998 quality standard to the resistance to of the embodiment 1-8 inner wall putty powders prepared Aqueous, adhesion strength, low tempertaure storage stability are detected that concrete outcome see the table below.
As can be seen from the above table, the water resistance of the inner wall putty powder of the embodiment of the present invention was bonded better than 48 hours of standard Intensity is more than the 0.25MPa of standard, and low tempertaure storage stability is good.
The specific embodiment of the present invention is described above.It is to be appreciated that the invention is not limited in above-mentioned Particular implementation, those skilled in the art can make various deformations or amendments within the scope of the claims, this not shadow Ring the substantive content of the present invention.

Claims (8)

1. a kind of attapulgite interior wall putty powder, it is characterised in that include the raw material of following parts by weight:Concave-convex clay rod 15-28 Part, 10-18 parts of white cement, 5-10 parts of calcium oxide, 18-25 parts of dead plaster, 1-5 parts of polyacrylamide, carboxylic hydroxypropyl methyl are fine Tie up 0.6-3 parts of element, 2-5 parts of flyash, 0.2-0.5 parts of pure iron powder.
2. attapulgite interior wall putty powder according to claim 1, it is characterised in that the inner wall putty powder includes following weight Measure the raw material of part:22 parts of Concave-convex clay rod, 16 parts of white cement, 8 parts of calcium oxide, 22 parts of dead plaster, polyacrylamide 3 Part, 1 part of carboxylic propyl methocel, 2 parts of flyash, 0.5 part of pure iron powder.
3. attapulgite interior wall putty powder according to claim 1, it is characterised in that the carboxylic propyl methocel it is viscous Spend for 50-100 handkerchiefs/second.
4. attapulgite interior wall putty powder according to claim 1, it is characterised in that the flyash is one-level or second patent flour Coal ash.
5. the preparation method of the attapulgite interior wall putty powder according to claim 1-4 any one, it is characterised in that including Following steps:
1)Concave-convex clay rod is taken, is soaked using 20-25 times of clear water of its quality, is heated to 40-50 DEG C, stirs 20-30 minutes Afterwards, filtrate is dried after filtering, and the Concave-convex clay rod that 200-300 mesh sieves are purified is crossed after crushing;
2)80-100 mesh sieves will be crossed after calcium oxide, dead plaster, polyacrylamide, flyash, pure iron powder co-grinding, obtained To mixture A;
3)Mixture A, attapulgite clay after purification, white cement, carboxylic propyl methocel are added into stirrer for mixing, stirred Mix after 1-2 hours, packed after discharging.
6. the preparation method of attapulgite interior wall putty powder according to claim 5, it is characterised in that the step 1)Drying To be dried 3-4 hours at 50-60 DEG C.
7. the preparation method of attapulgite interior wall putty powder according to claim 5, it is characterised in that the step 2)Use Micronizer is crushed.
8. the preparation method of attapulgite interior wall putty powder according to claim 5, it is characterised in that the step 3)Stirring Rotating speed be 600-800 revs/min.
CN201710231503.3A 2017-04-11 2017-04-11 A kind of attapulgite interior wall putty powder and preparation method thereof Pending CN106978001A (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110396317A (en) * 2019-08-07 2019-11-01 芜湖塑荣建筑材料有限公司 Imitation ceramic internal wall powder of lacquer putty for use on and preparation method thereof

Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101503286A (en) * 2009-03-27 2009-08-12 解云 Attapulgite putty powder for exterior wall
CN101585684A (en) * 2009-03-27 2009-11-25 解云 Attapulgite interior wall putty powder
CN102850835A (en) * 2012-08-30 2013-01-02 苏州市德莱尔建材科技有限公司 Putty powder capable of adsorbing foreign gas
CN103351132A (en) * 2013-06-25 2013-10-16 天长市开林化工有限公司 Environmentally-friendly interior wall putty powder
CN105199464A (en) * 2015-10-23 2015-12-30 广西兴安县桂兴矿粉厂 Green interior wall waterproof putty powder and preparation method and application method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101503286A (en) * 2009-03-27 2009-08-12 解云 Attapulgite putty powder for exterior wall
CN101585684A (en) * 2009-03-27 2009-11-25 解云 Attapulgite interior wall putty powder
CN102850835A (en) * 2012-08-30 2013-01-02 苏州市德莱尔建材科技有限公司 Putty powder capable of adsorbing foreign gas
CN103351132A (en) * 2013-06-25 2013-10-16 天长市开林化工有限公司 Environmentally-friendly interior wall putty powder
CN105199464A (en) * 2015-10-23 2015-12-30 广西兴安县桂兴矿粉厂 Green interior wall waterproof putty powder and preparation method and application method thereof

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110396317A (en) * 2019-08-07 2019-11-01 芜湖塑荣建筑材料有限公司 Imitation ceramic internal wall powder of lacquer putty for use on and preparation method thereof

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