CN106977630A - A kind of agitating and heating reactor - Google Patents
A kind of agitating and heating reactor Download PDFInfo
- Publication number
- CN106977630A CN106977630A CN201710170034.9A CN201710170034A CN106977630A CN 106977630 A CN106977630 A CN 106977630A CN 201710170034 A CN201710170034 A CN 201710170034A CN 106977630 A CN106977630 A CN 106977630A
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- Prior art keywords
- container
- reaction solution
- liter
- agitating
- key
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/01—Processes of polymerisation characterised by special features of the polymerisation apparatus used
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F2/00—Processes of polymerisation
- C08F2/12—Polymerisation in non-solvents
- C08F2/16—Aqueous medium
- C08F2/22—Emulsion polymerisation
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F220/00—Copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and only one being terminated by only one carboxyl radical or a salt, anhydride ester, amide, imide or nitrile thereof
- C08F220/02—Monocarboxylic acids having less than ten carbon atoms; Derivatives thereof
- C08F220/10—Esters
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00164—Controlling or regulating processes controlling the flow
- B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Physical Or Chemical Processes And Apparatus (AREA)
- Accessories For Mixers (AREA)
Abstract
The present invention relates to chemical test apparatus field, disclose a kind of agitating and heating reactor, reaction solution is contained in liter container, pass through the height of post adjustment container cover, the position of container cover is adjusted by swing arm, close container cover and liter container, liquid feeding is carried out by filling opening and dropwise addition mouth, press start key, motor driving stirring-head is stirred to reaction solution, press stop key, motor stops driving stirring-head and reaction solution is stirred, the mixing speed of motor can be adjusted by rotational speed regulation key, heater strip can be adjusted by temperature adjustment key to heat reaction solution, display screen is to mixing speed, heating-up temperature, the information such as pH value are shown, reaction solution is discharged by floss hole, reaction solution can also be poured out by a liter container of tumbling, simply, cost is low, operability is high, can easily acrylic acid synthesizing resin, develop new product.
Description
The present invention relates to chemical test apparatus field, a kind of specifically agitating and heating reactor.
Background technology
Acrylic resin is the resin being made up of esters of acrylic acid and methyl acrylic ester and other olefinic type monomers copolymerization,
By being constituted from different resin structures, different formulas, production technology and solvent, different type, different performance can be synthesized
With the acrylic resin of different application occasion, acrylic resin can be divided into thermoplasticity third again according to structure and the difference of membrane formation mechanism
Olefin(e) acid resin and thermosetting acrylic resin, with acrylate and the acrylic resin pair of methacrylate monomers copolymerization
The main absworption peak of light is in outside solar spectrum scope, so obtained acrylic resin paint has excellent light resistance and anti-family
Outer ageing properties, can produce acrylic resin by emulsion polymerization, and emulsion polymerization is by monomer, initiator and distilled water
Reactive polymeric is formed together, and general institute's resin is the emulsion that solids content is 50%, is the latex solution containing 50% or so water.
The emulsion being synthesized, typically all milky white blueing（Tyndall phenomenon）, glass transition temperature is according to the design of FOX formula.Therefore such
The emulsion molecular weight of type is big, but solid containing usually 40%-50%, and production industrial requirements control is accurate, and emulsion polymerization is that monomer is borrowed
Assistant for emulsifying agent and mechanical agitation, make monomer dispersion form emulsion in water, add initiator and trigger monomer polymerization, the mode of production
Flexibly, beneficial to new product development, but in order to carry out new product development, it is necessary to design for synthetic test, simply, it is low into
This, the high reactor of operability.
The content of the invention
In order to overcome the deficiencies in the prior art, the present invention provides a kind of agitating and heating reactor, passes through a liter container, heating
Silk, motor, stir it is first-class reaction solution is synthesized, simply, cost is low, operability is high.
The technical solution adopted for the present invention to solve the technical problems：
A kind of agitating and heating reactor, includes chassis, and the rear end on the chassis, which is vertically installed with rear board, the chassis, to be set
It is equipped with rectangle cavity, the chassis and is provided with the rectangle being adapted to rectangle cavity and connects disk, the rectangle connects disk and is provided with two
A liter container is provided with before handle, the rear board with can tumbling, described liter of container both sides are provided with handle, described liter of container
Temperature sensor is provided with, described liter of container bottom, which is provided with floss hole, described liter of container, is provided with heater strip and PH sensings
Liftable column is provided with device, the rear board, rotatably arranged with there is swing arm above the column, before the swing arm
End, which is provided with below motor, the motor, is fixedly connected with container cover, and the container cover is engaged with rising container,
Peephole, condenser pipe, filling opening are provided with the container cover and mouth is added dropwise, the output end of the motor is provided with stirring
Operation device is provided with head, the rear board, described liter of container side is provided with addition mouth, and the addition mouthful is connected with charging
Valve, the material inlet valve is connected with feed hopper, and the filling opening is connected with feed liquor tubule, and the feed liquor tubule is connected with wriggling
Drop-adding device is provided with pump, the dropwise addition mouthful, the operation device is provided with display screen, start key, stop key, rotational speed regulation key
With temperature adjustment key, exhaust outlet and viscosity test device are provided with the container cover, the viscosity test device is filled with operation
Put electrical connection.
Further, the operation device is provided with timer.
Further, it is provided with gravity sensor in described liter of container.
Further, the rectangle connects disk and is made up of stainless steel material.
Further, the handle is by integrally moulded.
The beneficial effects of the invention are as follows：Reaction solution is contained in liter container, by the height of post adjustment container cover, led to
The position that swing arm adjusts container cover is crossed, container cover is closed with container is risen, liquid feeding is carried out by filling opening and dropwise addition mouth, will be required
Material puts feed hopper into, opens material inlet valve, and material requested is entered in liter container by adding mouth, presses start key, drives
Motor driving stirring-head is stirred to reaction solution, presses stop key, and motor stops driving stirring-head to be carried out to reaction solution
Stirring, the mixing speed of motor can be adjusted by rotational speed regulation key, heater strip pair can be adjusted by temperature adjustment key
Reaction solution is heated, and display screen is shown to information such as mixing speed, heating-up temperature, pH values, will be reacted by floss hole
Liquid is discharged, and can also be poured out reaction solution by a liter container of tumbling, and simple, cost is low, operability is high, can be easily
Acrylic acid synthesizing resin, develops new product.
Brief description of the drawings
The present invention is further described with reference to the accompanying drawings and examples.
Fig. 1 is the structural representation of the present invention.
Embodiment
A kind of reference picture 1, agitating and heating reactor includes chassis 1, and the rear end on chassis 1 is vertically installed with rear board 2,
It is provided with chassis 1 and is provided with the rectangle being adapted to rectangle cavity on rectangle cavity, chassis 1 and connects disk 3, rectangle is connect into disk 3 places
In rectangle cavity, rectangle connects disk 3 and is provided with two handles 31, is easy to pick up taking-up rectangle and connect to incline before disk 3, rear board 2
Plough and be provided with liter container 4, rise the both sides of container 4 and be provided with handle 41, be easy to that liter container 4 is tumbled or ajusted, rise container 4
Temperature sensor is inside provided with, temperature sensor is monitored to reacting liquid temperature in liter container 4, rises the bottom of container 4 and be provided with
Floss hole 42, rises in container 4 and is provided with heater strip and PH sensors, reaction solution is heated by heater strip, PH sensors
The pH value of reaction solution is detected, liftable column 5 is provided with rear board 2, the top of column 5 is rotatably arranged with there is pendulum
Arm 51, the front end of swing arm 51 is provided with motor 52, and the lower section of motor 52 is fixedly connected with container cover 6, container cover 6 with
Rise container 4 to be engaged, peephole 61, condenser pipe 62, filling opening 63 are provided with container cover 6 and mouth 66 is added dropwise, passes through peephole
61 pairs rise reaction solution in container 4 and observe, and are condensed by condenser pipe 62, the output end of motor 52 is provided with stirring
First 53, the driving stirring-head 53 of motor 52 is stirred to reaction solution, and operation device 21 is provided with rear board 2, passes through behaviour
Make device 21 and carry out overall regulation and control, rise the side of container 4 and be provided with addition mouth 43, can material needed for by adding the addition reaction of mouth 43
Material, addition mouth 43 is connected with material inlet valve 44, and material inlet valve 44 is connected with feed hopper 45, and filling opening 63 is connected with feed liquor tubule
64, feed liquor tubule 64 is connected with peristaltic pump 65, is added dropwise on mouth 66 and is provided with Drop-adding device 67, will by peristaltic pump 65 or Drop-adding device 67
Reaction solution is added in liter container 4, and operation device 21 is provided with display screen 22, start key 26, stop key 27, rotational speed regulation key 23
With temperature adjustment key 24, exhaust outlet 68 and viscosity test device 69 are provided with container cover 6, and container 4 will be risen by exhaust outlet 68
Interior gas is discharged, and viscosity test device 69 is electrically connected with operation device 21, viscous to reaction solution by viscosity test device 69
Degree is monitored, and operation device 21 includes reaction solution viscosity number on display screen 22.
Reaction solution is contained in liter container 4, the height of container cover 6 is adjusted by column 5, container is adjusted by swing arm 51
The position of lid 6, closes container cover 6 and liter container 4, carries out liquid feeding by filling opening 63 and dropwise addition mouth 66, material requested is put
Enter feed hopper 45, open material inlet valve 44, material requested is entered in liter container 4 by adding mouth 43, presses start key 26, drive
The dynamic driving of motor 52 stirring-head 53 is stirred to reaction solution, presses stop key 27, and motor 52 stops driving stirring-head 53
Reaction solution is stirred, the mixing speed of motor 52 can be adjusted by rotational speed regulation key 23, passes through temperature adjustment key
24 can adjust heater strip is heated to reaction solution, and display screen 22 is shown to information such as mixing speed, heating-up temperature, pH values
Show, discharged reaction solution by floss hole 42, can also be poured out reaction solution by liter container 4 of tumbling, simple, cost is low, can
It is operational high, can easily acrylic acid synthesizing resin, develop new product.
In the present embodiment, it is preferred that operation device 21 is provided with timer 25, mixing time can be set.
In the present embodiment, it is preferred that rise in container 4 and be provided with gravity sensor, reaction solution in liter container 4 can be detected
Weight.
In the present embodiment, it is preferred that rectangle connects disk 3 and is made up of stainless steel material, corrosion is prevented, it is durable in use.
In the present embodiment, it is preferred that handle 41 is anti-scald by integrally moulded, shaping is simple, and cost is low.
It is described above, the simply better embodiment of the present invention, but the present invention is not limited to above-described embodiment, as long as
It reaches the technique effect of the present invention with any same or similar means, should all fall under the scope of the present invention.
Claims (5)
1. a kind of agitating and heating reactor, it is characterised in that：Include chassis（1）, the chassis（1）Rear end be vertically installed with
Rear board（2）, the chassis（1）On be provided with rectangle cavity, the chassis（1）On be provided with the rectangle being adapted to rectangle cavity
Connect disk（3）, the rectangle connects disk（3）It is provided with two handles（31）, the rear board（2）It is provided with a liter appearance with can above tumbling
Device（4）, described liter of container（4）Both sides are provided with handle（41）, described liter of container（4）Inside it is provided with temperature sensor, the liter
Container（4）Bottom is provided with floss hole（42）, described liter of container（4）Inside it is provided with heater strip and PH sensors, the rear board
（2）On be provided with liftable column（5）, the column（5）Top is rotatably arranged with there is swing arm（51）, the swing arm（51）
Front end be provided with motor（52）, the motor（52）Lower section be fixedly connected with container cover（6）, the container cover
（6）With a liter container（4）It is engaged, the container cover（6）On be provided with peephole（61）, condenser pipe（62）, filling opening（63）With
Mouth is added dropwise（66）, the motor（52）Output end be provided with stirring-head（53）, the rear board（2）On be provided with operation
Device（21）, described liter of container（4）Side is provided with addition mouth（43）, the addition mouth（43）It is connected with material inlet valve（44）,
The material inlet valve（44）It is connected with feed hopper（45）, the filling opening（63）It is connected with feed liquor tubule（64）, the feed liquor is thin
Pipe（64）It is connected with peristaltic pump（65）, the dropwise addition mouth（66）On be provided with Drop-adding device（67）, the operation device（21）Set
There is display screen（22）, start key（26）, stop key（27）, rotational speed regulation key（23）With temperature adjustment key（24）, the container cover
（6）On be provided with exhaust outlet（68）And viscosity test device（69）, the viscosity test device（69）With operation device（21）Electricity
Connection.
2. a kind of agitating and heating reactor according to claim 1, it is characterised in that：The operation device（21）It is provided with
Timer（25）.
3. a kind of agitating and heating reactor according to claim 1 or 2, it is characterised in that：Described liter of container（4）It is interior to set
There is gravity sensor.
4. a kind of agitating and heating reactor according to claim 1 or 2, it is characterised in that：The rectangle connects disk（3）By not
Rust Steel material is made.
5. a kind of agitating and heating reactor according to claim 1 or 2, it is characterised in that：The handle（41）By plastics
It is integrally formed.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710170034.9A CN106977630A (en) | 2017-03-21 | 2017-03-21 | A kind of agitating and heating reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710170034.9A CN106977630A (en) | 2017-03-21 | 2017-03-21 | A kind of agitating and heating reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106977630A true CN106977630A (en) | 2017-07-25 |
Family
ID=59338097
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710170034.9A Pending CN106977630A (en) | 2017-03-21 | 2017-03-21 | A kind of agitating and heating reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106977630A (en) |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2396881Y (en) * | 1999-12-03 | 2000-09-20 | 中国科学院南京土壤研究所 | Mixed reactor |
| CN101735342A (en) * | 2009-12-25 | 2010-06-16 | 同济大学 | Macromolecular synthetic reaction device |
| CN103240142A (en) * | 2013-05-22 | 2013-08-14 | 南京林业大学 | Resin synthesis reactor |
-
2017
- 2017-03-21 CN CN201710170034.9A patent/CN106977630A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN2396881Y (en) * | 1999-12-03 | 2000-09-20 | 中国科学院南京土壤研究所 | Mixed reactor |
| CN101735342A (en) * | 2009-12-25 | 2010-06-16 | 同济大学 | Macromolecular synthetic reaction device |
| CN103240142A (en) * | 2013-05-22 | 2013-08-14 | 南京林业大学 | Resin synthesis reactor |
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| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20170725 |