CN206762869U - A kind of magnetic agitation reactor - Google Patents
A kind of magnetic agitation reactor Download PDFInfo
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- CN206762869U CN206762869U CN201720291599.8U CN201720291599U CN206762869U CN 206762869 U CN206762869 U CN 206762869U CN 201720291599 U CN201720291599 U CN 201720291599U CN 206762869 U CN206762869 U CN 206762869U
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- magnetic agitation
- regulation
- control platform
- reaction bulb
- feed liquor
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Abstract
It the utility model is related to chemical test apparatus field,Disclose a kind of magnetic agitation reactor,Reaction solution is contained in reaction bulb,Close reaction Bottle and bottle cap,The position of reaction bulb can be adjusted by adjusting post and driving headstock,So that reaction bulb is placed on bottle holder,Liquid feeding is carried out by filling opening and feed liquor temperature mouth,Press starting switch,Magnetic agitation drive device drives stirring magnet to be stirred reaction solution,Press stop key,Magnetic agitation drive device stops driving stirring magnet to be stirred reaction solution,Mixing speed can be adjusted by stirring and adjusting knob,The effect that heating plate heated to reaction solution can be adjusted by temperature adjustment knob,Display screen is to mixing speed,The information such as heating-up temperature are shown,Simply,Cost is low,Operability is high,Can easily acrylic acid synthesizing resin,Develop new product.
Description
Technical field
Chemical test apparatus field is the utility model is related to, specifically a kind of magnetic agitation reactor.
Background technology
Acrylic resin is the resin made of esters of acrylic acid and methyl acrylic ester and other olefinic type monomers are copolymerized,
By being formed from different resin structures, different formulas, production technology and solvent, different type, different performance can be synthesized
With the acrylic resin of different application occasion, acrylic resin can be divided into thermoplasticity third again according to structure and the difference of membrane formation mechanism
Olefin(e) acid resin and thermosetting acrylic resin, with acrylate and the acrylic resin pair of methacrylate monomers copolymerization
The main absworption peak of light is in outside solar spectrum scope, so obtained acrylic resin paint has excellent light resistance and anti-family
Outer ageing properties, can produce acrylic resin by emulsion polymerization, and emulsion polymerization is by monomer, initiator and distilled water
Reactive polymeric forms together, and general institute's resin is the emulsion that solids content is 50%, is that the latex containing 50% or so water is molten
Liquid.The emulsion being synthesized, typically milky white blueing (Tyndall phenomenon), glass transition temperature design according to FOX formula.Therefore
The emulsion molecular weight of the type is big, but contains usually 40%-50% admittedly, and production industrial requirements control is accurate, and emulsion polymerization is
Monomer makes monomer dispersion form emulsion in water, adds initiator and trigger monomer polymerization, life by emulsifying agent and mechanical agitation
Production mode is flexible, beneficial to new product development, but in order to carry out new product development, it is necessary to design for synthetic test, simply
, inexpensive, the high reactor of operability.
Utility model content
For overcome the deficiencies in the prior art, the utility model provides a kind of magnetic agitation reactor, by reaction bulb, adds
Hot plate, magnetic agitation drive device, stirring magnet etc. synthesize to reaction solution, and simply, cost is low, operability is high.
The utility model solves technical scheme used by its technical problem：
A kind of magnetic agitation reactor, include base, magnetic agitation drive device, the magnetic are provided with the base
Power mixer drive upper end is provided with heating plate, and reaction bulb is placed with the heating plate, be placed with the heating plate with
The bottle holder of reaction bulb adaptation, the bottle holder are provided with pressure sensor, and the side of the base is connected with regulation and control platform, the regulation and control
Platform is provided with regulation and control panel, is provided with the column of adjustable lifting on the regulation and control platform, rotatably arranged with there is pendulum on the column
Arm, driving headstock is provided with horizontally moveablely in the swing arm, the driving headstock is arranged with main shaft, and the main shaft is arranged with
Bottle cap, the bottle cap are adapted to the reaction bulb, and stirring magnet is provided with the reaction bulb, feed liquor is provided with the bottle cap
Temperature mouth, condensate port, filling opening and exhaust outlet, the condensate port are connected with condensation recovery tube, and the feed liquor temperature mouth is provided with
Electronic thermometer, the feed liquor temperature mouth are connected with feed liquor tubule, and the feed liquor tubule is connected with peristaltic pump, the regulation and control platform with
Heating plate, electronic thermometer, pressure sensor, the electrical connection of magnetic agitation drive device, the regulation and control platform are provided with pressure self-locking
Module, the regulation and control panel are provided with stirring and adjusting knob, display screen, starting switch, shutdown switch, temperature adjustment knob, institute
State filling opening and be connected with Drop-adding device.
Further, the regulation and control platform is provided with timer.
Further, the main shaft is provided with gravity sensor.
Further, clamping bar is vertically installed with the regulation and control platform, the clamping bar can be provided with straight skidding
Gripping block.
Further, it is provided with viscosity test device on the bottle cap.
The beneficial effects of the utility model are：Reaction solution is contained in reaction bulb, closes reaction Bottle and bottle cap, passes through tune
Section column and driving headstock can adjust the position of reaction bulb, and reaction bulb is placed on bottle holder, by filling opening and enter liquid temperature
Spend mouth and carry out liquid feeding, press starting switch, magnetic agitation drive device drives stirring magnet to be stirred reaction solution, presses and stop
Only key, magnetic agitation drive device stop driving stirring magnet to be stirred reaction solution, can adjusted by stirring and adjusting knob
Mixing speed is saved, the effect that heating plate heated to reaction solution can be adjusted by temperature adjustment knob, display screen is to stirring
The information such as speed, heating-up temperature are shown, simple, cost is low, operability is high, can easily acrylic acid synthesizing tree
Fat, develop new product.
Brief description of the drawings
The utility model is further illustrated with reference to the accompanying drawings and examples.
Fig. 1 is structural representation of the present utility model.
Embodiment
Reference picture 1, a kind of magnetic agitation reactor, include base 1, magnetic agitation drive device is provided with base 1
2, driven and stirred by magnetic agitation drive device 2, the upper end of magnetic agitation drive device 2 is provided with heating plate 3, in heating plate 3
Reaction bulb 4 is placed with, reaction solution in reaction bulb 4 is heated by heating plate 3, is placed with heating plate 3 suitable with reaction bulb 4
The bottle holder 31 matched somebody with somebody, bottle holder 31 play positioning action to reaction bulb 4, and bottle holder 31 is provided with pressure sensor, can be passed by pressure
Sensor detects pressure of the reaction bulb 4 to bottle holder 31, and the side of base 1 is connected with regulation and control platform 5, regulated and controled by regulating and controlling platform 5,
Regulation and control platform 5 is provided with regulation and control panel 51, regulates and controls and the column 52 of adjustable lifting is provided with platform 5, on column 52 rotatably arranged with
There is swing arm 53, be provided with driving headstock 54 in swing arm 53 horizontally moveablely, driving headstock 54 is arranged with main shaft 55, under main shaft 55
Bottle cap 6 is provided with, bottle cap 6 is adapted to reaction bulb 4, and stirring magnet 7 is provided with reaction bulb 4, feed liquor temperature is provided with bottle cap 6
Mouth 61, condensate port 62, filling opening 63 and exhaust outlet 68, condensate port 62 is connected with condensation recovery tube 64, by condensing recovery tube 64
Condensed, feed liquor temperature mouth 61 is provided with electronic thermometer 65, by electronic thermometer 65 to reacting liquid temperature in reaction bulb 4
Detected, feed liquor temperature mouth 61 is connected with feed liquor tubule 66, and feed liquor tubule 66 is connected with peristaltic pump 67, and peristaltic pump 67 is by entering
Liquid tubule 66 conveys reaction solution into feed liquor temperature mouth 61, regulation and control platform 5 and heating plate 3, electronic thermometer 65, pressure sensor,
Magnetic agitation drive device 2 is electrically connected, and heating plate 3, magnetic agitation drive device 2 are regulated and controled by regulating and controlling platform 5, pass through tune
Control platform 5 is collected to the information of electronic thermometer 65, pressure sensor, and regulation and control platform 5 is provided with pressure self-locking module, and pressure passes
Sensor detects reaction bulb 4 and reaches certain value to the pressure of bottle holder 31, and pressure self-locking module starts, column 52 and driving headstock 54
Stopping acts, and prevents from damaging by pressure reaction bulb 4, regulation and control panel 51 be provided with stirring and adjusting knob 56, display screen 57, starting switch 58,
Shutdown switch 59, temperature adjustment knob 510, mixing speed is adjusted by stirring and adjusting knob 56, shown by display screen 57
Show, work is started by starting switch 58, is stopped and resets by shutdown switch 59, adjusted by temperature adjustment knob 510
Heating-up temperature is saved, filling opening 63 is connected with Drop-adding device 69, can conveyed reaction solution into filling opening 63 by Drop-adding device 69.
Reaction solution is contained in reaction bulb 4, closes reaction bulb 4 and bottle cap 6, can by adjusting post 52 and driving headstock 54
To adjust the position of reaction bulb 4, reaction bulb 4 is placed on bottle holder 31, carried out by filling opening 63 and feed liquor temperature mouth 61
Liquid feeding, presses starting switch 58, and magnetic agitation drive device 2 drives stirring magnet 7 to be stirred reaction solution, presses stop key
27, magnetic agitation drive device 2 stops driving stirring magnet 7 to be stirred reaction solution, can be with by stirring and adjusting knob 56
Mixing speed is adjusted, the effect that heating plate 3 heated to reaction solution, display screen can be adjusted by temperature adjustment knob 510
The information such as 57 pairs of mixing speeds, heating-up temperatures show, simple, cost is low, operability is high, can easily close
Into acrylic resin, new product is developed.
In the present embodiment, it is preferred that regulation and control platform 5 is provided with timer 511, and mixing time can be set.
In the present embodiment, it is preferred that main shaft 55 is provided with gravity sensor, can detect reaction solution in reaction bulb 4
Weight.
In the present embodiment, it is preferred that on regulation and control platform 5 be vertically installed with clamping bar 512, clamping bar 512 can straight skidding
Gripping block 513 is provided with, Drop-adding device 69 or condensation recovery tube 64 can be clamped by gripping block 513.
In the present embodiment, it is preferred that viscosity test device 610 is provided with bottle cap 6, viscosity test device can be passed through
The viscosity of 610 pairs of reaction solutions measures.
It is described above, simply better embodiment of the present utility model, but the utility model is not limited to above-mentioned reality
Example is applied, as long as it reaches technique effect of the present utility model with any same or similar means, should all be fallen into of the present utility model
Within protection domain.
Claims (5)
- A kind of 1. magnetic agitation reactor, it is characterised in that：Include base (1), magnetic agitation is provided with the base (1) Drive device (2), magnetic agitation drive device (2) upper end are provided with heating plate (3), are placed with the heating plate (3) Reaction bulb (4), the bottle holder (31) being adapted to reaction bulb (4) is placed with the heating plate (3), the bottle holder (31) is provided with pressure Force snesor, the side of the base (1) are connected with regulation and control platform (5), and the regulation and control platform (5) is provided with regulation and control panel (51), institute The column (52) that adjustable lifting is provided with regulation and control platform (5) is stated, rotatably arranged with having swing arm (53), institute on the column (52) State and be provided with driving headstock (54) in swing arm (53) horizontally moveablely, the driving headstock (54) is arranged with main shaft (55), described Main shaft (55) is arranged with bottle cap (6), and the bottle cap (6) is adapted to the reaction bulb (4), is provided with the reaction bulb (4) Magnet (7) is stirred, feed liquor temperature mouth (61), condensate port (62), filling opening (63) and exhaust outlet are provided with the bottle cap (6) (68), the condensate port (62) is connected with condensation recovery tube (64), and the feed liquor temperature mouth (61) is provided with electronic thermometer (65), the feed liquor temperature mouth (61) is connected with feed liquor tubule (66), and the feed liquor tubule (66) is connected with peristaltic pump (67), institute State regulation and control platform (5) to electrically connect with heating plate (3), electronic thermometer (65), pressure sensor, magnetic agitation drive device (2), institute State regulation and control platform (5) and be provided with pressure self-locking module, the regulation and control panel (51) is provided with stirring and adjusting knob (56), display screen (57), starting switch (58), shutdown switch (59), temperature adjustment knob (510), the filling opening (63) are connected with Drop-adding device (69)。
- A kind of 2. magnetic agitation reactor according to claim 1, it is characterised in that：The regulation and control platform (5) is provided with meter When device (511).
- A kind of 3. magnetic agitation reactor according to claim 1 or 2, it is characterised in that：The main shaft (55) is provided with Gravity sensor.
- A kind of 4. magnetic agitation reactor according to claim 1 or 2, it is characterised in that：It is vertical on the regulation and control platform (5) Clamping bar (512) is provided with, the clamping bar (512) can be provided with gripping block (513) straight skidding.
- A kind of 5. magnetic agitation reactor according to claim 1 or 2, it is characterised in that：It is provided with the bottle cap (6) Viscosity test device (610).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720291599.8U CN206762869U (en) | 2017-03-21 | 2017-03-21 | A kind of magnetic agitation reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720291599.8U CN206762869U (en) | 2017-03-21 | 2017-03-21 | A kind of magnetic agitation reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206762869U true CN206762869U (en) | 2017-12-19 |
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ID=60633707
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720291599.8U Active CN206762869U (en) | 2017-03-21 | 2017-03-21 | A kind of magnetic agitation reactor |
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| CN (1) | CN206762869U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106861577A (en) * | 2017-03-21 | 2017-06-20 | 江门市聚力化工科技有限公司 | A kind of magnetic agitation reactor |
-
2017
- 2017-03-21 CN CN201720291599.8U patent/CN206762869U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106861577A (en) * | 2017-03-21 | 2017-06-20 | 江门市聚力化工科技有限公司 | A kind of magnetic agitation reactor |
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