CN106955657A - A kind of Western medicine production and processing processes stirring reaction equipment with decoction - Google Patents
A kind of Western medicine production and processing processes stirring reaction equipment with decoction Download PDFInfo
- Publication number
- CN106955657A CN106955657A CN201710290545.4A CN201710290545A CN106955657A CN 106955657 A CN106955657 A CN 106955657A CN 201710290545 A CN201710290545 A CN 201710290545A CN 106955657 A CN106955657 A CN 106955657A
- Authority
- CN
- China
- Prior art keywords
- discharge nozzle
- kettle
- decoction
- western medicine
- condenser
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/18—Stationary reactors having moving elements inside
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0006—Controlling or regulating processes
- B01J19/0013—Controlling the temperature of the process
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0053—Details of the reactor
- B01J19/0066—Stirrers
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J4/00—Feed or outlet devices; Feed or outlet control devices
- B01J4/001—Feed or outlet devices as such, e.g. feeding tubes
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J2219/00049—Controlling or regulating processes
- B01J2219/00051—Controlling the temperature
- B01J2219/00074—Controlling the temperature by indirect heating or cooling employing heat exchange fluids
- B01J2219/00087—Controlling the temperature by indirect heating or cooling employing heat exchange fluids with heat exchange elements outside the reactor
- B01J2219/00094—Jackets
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The invention discloses a kind of Western medicine production and processing stirring reaction equipment is processed with decoction, including kettle, upper lid, motor, agitating shaft, axle envelope, milling cutter, arc puddler, cooling jacket, refrigerant inlet, refrigerant outlet, pipeline is connected, pipe bundle condenser, measuring tank, 3rd condenser, vavuum pump, upper lid is provided with charging aperture, the top of kettle is provided with discharge nozzle, discharge nozzle bottom is provided with stop valve, discharging inside pipe wall is fixed with annular fastener, stretching tube is provided with annular fastener, stretching tube top is provided with circular cover, stretching tube bottom is provided with annular locating ring along girth.The present invention is simple and reasonable, easy to use, and material is well mixed, and is improved the effect of stirring, is greatly improved the condensing agent rate of recovery, cost-effective, reduces the waste of condensing agent；Facilitate discharge.
Description
Technical field
The present invention relates to a kind of reactor, specifically a kind of Western medicine production and processing processes stirring reaction equipment with decoction.
Background technology
Western medicine, for motherland's traditional Chinese medicine, refers to the medicine of modern medicine, is typically made of chemical synthesis process
Or obtain through refining and form from natural products；Including aspirin, penicillin, tablet for alleviating pain etc..Western medicine is organic chemical, inorganization
Learn medicine and biological products.See that its specification then has more accurate than Chinese medicine on chemical name, structural formula, dosage, generally in terms of milligram.
The production and processing of Western medicine needs to use various equipment, in the extractive process to part material often by they
Composition carries out hybrid reaction stirring, and in order to which the normal table for ensureing reaction is carried out in order to which guarantee period accuracy can be selected closed
Environment in carry out, will at this time use various reaction stirred tanks, existing reactor operationally, because rabbling mechanism is big
Mostly simple slurry, or barred body, often stir uneven, typically can all be produced in chemical reaction process substantial amounts of
Heat, is now accomplished by condensing agent and carries out overall cooling to reactor；And the condensing agent rate of recovery after use is relatively low, waste tighter
Weight, and the condensing agent of discharge carries substantial amounts of heat, it is necessary to timely cool to condensing agent；Simultaneously in reactor end operation
When, often discharged by the discharging opening of reactor bottom, impurity may be contained inside it but some chemically react, this
If when want take out solution and without impurity, it is often highly difficult.
The content of the invention
Stirring reaction equipment is processed with decoction it is an object of the invention to provide a kind of Western medicine production and processing, it is above-mentioned to solve
The problem of being proposed in background technology.
To achieve the above object, the present invention provides following technical scheme：
A kind of Western medicine production and processing processes stirring reaction equipment, including kettle with decoction, and the kettle is provided with upper lid, on
Tops are provided with motor, and the rotating shaft end of motor is connected with agitating shaft, and agitating shaft is located in kettle, the company of agitating shaft and kettle
The place of connecing is provided with axle envelope, and the lower end of agitating shaft is threaded with milling cutter, agitating shaft to be set by driving the universal joint of power apparatus
There is arc puddler, kettle is wrapped with cooling jacket, and the left side top of cooling jacket offers refrigerant inlet, right side top
Offer and be connected at refrigerant outlet, refrigerant outlet with spiral plate condenser by pipeline, spiral plate condenser passes through pipeline
Pipe bundle condenser is connected with, pipe bundle condenser, which is connected with measuring tank, measuring tank, is provided with the 3rd condenser, and measuring tank opposite side is also
It is connected with vavuum pump；The upper lid is provided with charging aperture, and the top of kettle is provided with discharge nozzle, and discharge nozzle bottom is provided with cut-off
Valve, the discharging inside pipe wall first half is also fixed with annular fastener, annular fastener provided with size and annular fastener internal diameter
The stretching tube that is adapted and can be moved up and down in annular fastener, stretching tube top is provided with circular cover, cover plate and discharge nozzle
Top is in same level, and stretching tube bottom is additionally provided with annular locating ring along girth, and locating ring is located at stop valve top, lid
Plate is adapted with positioning ring diameter with discharging bore.
It is used as further scheme of the invention：3rd condenser is half coiled tube condenser.
It is used as further scheme of the invention：The annular fastener is highly at the top of 15~20cm, annular fastener
Distance at the top of to discharge nozzle is equal with the height of cover plate, discharge nozzle first half side provided be vertically arranged and through discharge nozzle with
The strip groove of annular fastener, groove is highly 10~15cm, the distance at groove two ends and corresponding annular fastener two ends
Equal, groove bottom is provided with pull bar, and pull bar one end is fixedly connected with stretching drum outer wall, and the other end is extended to outside discharge nozzle
Side.
It is used as further scheme of the invention：The stretching tube is uniformly provided with aperture on the cylinder at the top of pull bar
1~2cm through hole, stretching tube side is provided with the seal area of correspondence groove.
It is used as further scheme of the invention：The distance between the pull bar and locating ring top are more than pull bar and cover plate
The distance between bottom.
Compared with prior art, the beneficial effects of the invention are as follows：Simple and reasonable, easy to use, the Ke Yitong of the present invention
The angle that universal joint adjusts puddler is crossed, so that material is well mixed, while puddler is arc, further increases and stirs
The effect mixed, it is also possible that the condensing agent of reactor discharge is condensed out, and is stored into measuring tank, after after total condensation,
Extracted out further according to demand, greatly improve the condensing agent rate of recovery, it is cost-effective, reduce the waste of condensing agent；When needing discharge, beat
Stop valve is opened, by moving up the pull bar in groove, pull bar, which drives, draws stretching to move up, and the cover plate at the top of stretching tube will be anti-
The material top in bottom portion is answered to open, the through hole on liquid drawn cylinder in reactor is flowed into stretching tube, then from discharge nozzle discharge,
Because the stretching tube first half is provided with the less reason of some through holes and aperture, what liquid was produced when via through holes are flowed into stretching tube
Power is just smaller so that being deposited in the material of reactor bottom can discharge together with liquid；Due to logical on stretching tube cylinder
Hole is arranged at the top of pull bar, and pull bar is more than pull bar and the distance of plectane bottom with the distance at the top of locating ring so that pull bar energy
Smoothly be moved at the top of groove so that liquid will not via through holes flow on groove, in not discharge, mutually fitted with discharging bore
The cover plate matched somebody with somebody also can be by fluid isolation in reactor.
Brief description of the drawings
Fig. 1 is the structural representation that Western medicine production and processing decoction processes stirring reaction equipment；
Fig. 2 is the mplifying structure schematic diagram that Western medicine production and processing decoction processes discharge nozzle in stirring reaction equipment；
In figure：Lid, the stirring of 3- motors, 4- axle envelopes, 5- agitating shafts, 6- milling cutters, 7- universal joints, 8- arcs on 1- kettlies, 2-
Bar, 9- cooling jackets, 10- refrigerant inlets, 11- refrigerant outlets, 12- pipelines, 13- spiral plates condenser, the condensation of 14- tubulations
Device, 15- vavuum pumps, 16- measuring tanks, the condensers of 17- the 3rd, 18- charging apertures, 19- discharge nozzles, 20- stop valves, 21- annulars
Fastener, 22- stretching tubes, 23- cover plates, 24- locating rings, 25- grooves, 26- pull bars, 27- through holes, 28- seal areas.
Embodiment
The technical scheme of this patent is described in more detail with reference to embodiment.
Fig. 1-2 is referred to, a kind of Western medicine production and processing processes stirring reaction equipment, including kettle 1, the kettle with decoction
1 is provided with upper lid 2, and the upper top of lid 2 is provided with motor 3, and the rotating shaft end of motor 3 is connected with agitating shaft 5, and agitating shaft 5 is located in kettle
In body 1, the junction of agitating shaft 5 and kettle 1 is provided with axle envelope 4, and the lower end of agitating shaft 5 is threaded with milling cutter 6, agitating shaft 5
On be provided with some arc puddlers 8 by driving the universal joint 7 of power apparatus, kettle 1 is wrapped with cooling jacket 9, cooling folder
The left side top of set 9 offers refrigerant inlet 10, and right side top is offered at refrigerant outlet 11, refrigerant outlet 11 and spiral shell
Rotating plate condenser 13 is connected by pipeline 12, and spiral plate condenser 13 is connected with pipe bundle condenser 14 by pipeline 12, and tubulation is cold
Condenser 14 is connected with measuring tank 16, is provided with the 3rd condenser 17 in measuring tank 16, the opposite side of measuring tank 16 also with the phase of vavuum pump 15
Connection, the condensing agent that cooling jacket 9 is discharged is condensed out, and is stored into measuring tank 16, after after total condensation, further according to demand
Extract out, greatly improve the condensing agent rate of recovery, it is cost-effective, reduce the waste of condensing agent.
3rd condenser 17 is half coiled tube condenser.
The upper lid 2 is provided with charging aperture 18, and the top of kettle 1 is provided with discharge nozzle 19, and the bottom of discharge nozzle 19 is provided with cut-off
Valve 20, the inwall first half of discharge nozzle 19, which is also fixed with annular fastener 21, annular fastener 21, is provided with size and annular
The stretching tube 22 that the internal diameter of fastener 21 is adapted, the stretching tube 22 can be moved up and down in annular fastener 21, the top of stretching tube 22
Provided with circular cover 23, cover plate 23 is in same level with the top of discharge nozzle 19, and the bottom of stretching tube 22 is additionally provided with circle along girth
Circular orientation ring 24, locating ring 24 is located at the top of stop valve 20, cover plate 23 and the diameter of locating ring 24 with the internal diameter phase of discharge nozzle 19
Adaptation.
The height of annular fastener 21 is 15~20cm, the distance at the top of annular fastener 21 to the top of discharge nozzle 19 with
The height of cover plate 23 is equal, and the first half side of discharge nozzle 19, which is provided with, to be vertically arranged and through discharge nozzle 19 and annular fastener 21
Strip groove 25, the height of groove 25 is 10~15cm, and the two ends of groove 25 and the distance at the corresponding two ends of annular fastener 21 are homogeneous
Pull bar 26 is provided with Deng, the bottom of groove 25, the one end of pull bar 26 is fixedly connected with the outer wall of stretching tube 22, and the other end extends to discharge nozzle
19 outsides, stretching tube 22 is located at the through hole 27 for being uniformly provided with that aperture is 1~2cm on the cylinder at the top of pull bar 26, the stretching tube 22
Side is provided with the seal area 28 of correspondence groove 25, and the distance between pull bar 26 and the top of locating ring 24 are more than pull bar 26 and cover plate 23
The distance between bottom.
Temperature sensor, pressure sensor are additionally provided with the kettle 1, also including a controller, universal joint 7, temperature are passed
Sensor, pressure sensor are connected with controller.
The better embodiment to this patent is explained in detail above, but this patent is not limited to above-mentioned embodiment party
, can also be on the premise of this patent objective not be departed from formula, the knowledge that one skilled in the relevant art possesses
Make a variety of changes.
Claims (5)
1. a kind of Western medicine production and processing processes stirring reaction equipment, including kettle with decoction, the kettle is provided with upper lid, upper lid
Top is provided with motor, and the rotating shaft end of motor is connected with agitating shaft, and agitating shaft is located in kettle, it is characterised in that agitating shaft
Axle envelope is installed with the junction of kettle, the lower end of agitating shaft is threaded with milling cutter, agitating shaft by driving power apparatus
Universal joint is provided with arc puddler, and kettle is wrapped with cooling jacket, and the left side top of cooling jacket offers condensing agent and entered
Mouthful, right side top offered and be connected at refrigerant outlet, refrigerant outlet with spiral plate condenser by pipeline, spiral plate condensation
Device is connected with pipe bundle condenser by pipeline, and pipe bundle condenser, which is connected with measuring tank, measuring tank, is provided with the 3rd condenser, metering
Tank opposite side is also connected with vavuum pump；The upper lid is provided with charging aperture, and the top of kettle is provided with discharge nozzle, discharge nozzle bottom
Provided with stop valve, the discharging inside pipe wall first half, which is also fixed with annular fastener, annular fastener, is provided with size and annular
The stretching tube that fastener internal diameter is adapted and can moved up and down in annular fastener, stretching tube top is provided with circular cover, cover plate
Same level is in discharge nozzle top, stretching tube bottom is additionally provided with annular locating ring along girth, and locating ring is located at cut-off
Valve top, cover plate is adapted with positioning ring diameter with discharging bore.
2. Western medicine production and processing according to claim 1 processes stirring reaction equipment with decoction, it is characterised in that described the
Three condensers are half coiled tube condenser.
3. Western medicine production and processing according to claim 1 or 2 processes stirring reaction equipment with decoction, it is characterised in that institute
It is highly 15~20cm to state annular fastener, and annular fastener top is equal with the height of cover plate to the distance at the top of discharge nozzle,
Discharge nozzle first half side, which is provided with, to be vertically arranged and through the strip groove of discharge nozzle and annular fastener, and groove is highly 10
~15cm, groove two ends are equal with the distance at corresponding annular fastener two ends, groove bottom be provided with pull bar, pull bar one end with
Stretching drum outer wall is fixedly connected, and the other end is extended on the outside of discharge nozzle.
4. Western medicine production and processing according to claim 3 processes stirring reaction equipment with decoction, it is characterised in that the drawing
Stretch cylinder and the through hole that aperture is 1~2cm is uniformly provided with the cylinder at the top of pull bar, stretching tube side is provided with the close of correspondence groove
Seal area.
5. the Western medicine production and processing according to claim 1 or 2 or 4 processes stirring reaction equipment with decoction, it is characterised in that
The distance between the pull bar and locating ring top are more than the distance between pull bar and cover plate bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710290545.4A CN106955657A (en) | 2017-04-17 | 2017-04-17 | A kind of Western medicine production and processing processes stirring reaction equipment with decoction |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710290545.4A CN106955657A (en) | 2017-04-17 | 2017-04-17 | A kind of Western medicine production and processing processes stirring reaction equipment with decoction |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN106955657A true CN106955657A (en) | 2017-07-18 |
Family
ID=59484500
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710290545.4A Pending CN106955657A (en) | 2017-04-17 | 2017-04-17 | A kind of Western medicine production and processing processes stirring reaction equipment with decoction |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106955657A (en) |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN202366704U (en) * | 2011-11-30 | 2012-08-08 | 安徽省兴宙医药食品有限公司 | Heat exchange type stirring reaction kettle for processing calcium gluconate |
| US20130236368A1 (en) * | 2010-10-05 | 2013-09-12 | Korea Institute Of Industrial Technology | Double helix type gas hydrate reactor |
| CN204973857U (en) * | 2015-04-13 | 2016-01-20 | 天津八通化工有限公司 | Porcelain enamel reaction kettle |
| CN204996440U (en) * | 2015-08-18 | 2016-01-27 | 赣县鑫亿化工有限公司 | Ammonium chloride neutralization reaction equipment |
| CN205127949U (en) * | 2015-10-28 | 2016-04-06 | 王燕程 | Reation kettle with condensing agent recovery unit |
-
2017
- 2017-04-17 CN CN201710290545.4A patent/CN106955657A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20130236368A1 (en) * | 2010-10-05 | 2013-09-12 | Korea Institute Of Industrial Technology | Double helix type gas hydrate reactor |
| CN202366704U (en) * | 2011-11-30 | 2012-08-08 | 安徽省兴宙医药食品有限公司 | Heat exchange type stirring reaction kettle for processing calcium gluconate |
| CN204973857U (en) * | 2015-04-13 | 2016-01-20 | 天津八通化工有限公司 | Porcelain enamel reaction kettle |
| CN204996440U (en) * | 2015-08-18 | 2016-01-27 | 赣县鑫亿化工有限公司 | Ammonium chloride neutralization reaction equipment |
| CN205127949U (en) * | 2015-10-28 | 2016-04-06 | 王燕程 | Reation kettle with condensing agent recovery unit |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN206276381U (en) | A kind of reactor of quick blend feedstock | |
| CN104974219A (en) | Convenient ossotide alcohol precipitation tank and application method thereof | |
| CN207446220U (en) | A kind of Western medicine production and processing liquid processing is stirred to react equipment | |
| CN206881530U (en) | A kind of medicine company Agitation Tank | |
| CN106955657A (en) | A kind of Western medicine production and processing processes stirring reaction equipment with decoction | |
| CN209423594U (en) | It is a kind of for synthesizing the reaction kettle of Du Lutewei intermediate | |
| CN206980678U (en) | A kind of chemical industry tail gas foam removal condenses gas operated device | |
| CN106190811A (en) | A kind of diphasic anaerobic fermentation is from stirring reaction unit | |
| CN109277050A (en) | Method and device is added dropwise in acetaldehyde negative pressure in a kind of production of metronidazole | |
| CN205759863U (en) | A kind of Chinese medicine extraction liquid efficiently cracks automaton | |
| CN208711104U (en) | A kind of new type of continuous extraction equipment | |
| CN208678412U (en) | A kind of low-temperature reduced-pressure distilling apparatus | |
| CN208356171U (en) | A kind of tetrandrine extraction system | |
| CN210302451U (en) | Double-effect concentration device for traditional Chinese medicine | |
| CN207493683U (en) | A kind of reaction kettle for being evenly heated or cooling down | |
| CN207253803U (en) | A kind of vacuum concentration reaction kettle for rose extraction | |
| CN205392436U (en) | Reation kettle with storage device | |
| CN206474142U (en) | A kind of tetrahydrofuran derivatives medicine intermediate reactor | |
| CN205549635U (en) | Multi -functional flashing device is used in anticorrosive type bio -pharmaceuticals | |
| CN206167959U (en) | Distillation condensation device | |
| CN205392438U (en) | Reation kettle structure with storage device | |
| CN207708565U (en) | Solid water mixture bosh | |
| CN205313567U (en) | Novel fermenting case | |
| CN208562243U (en) | A kind of coal tar atmospheric and vacuum distillation system | |
| CN206081747U (en) | Multi -functional mellow wine precipitates recovery unit |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| WD01 | Invention patent application deemed withdrawn after publication | ||
| WD01 | Invention patent application deemed withdrawn after publication |
Application publication date: 20170718 |