CN106923324B - Selenium-rich polygonatum sibiricum whole powder and preparation method thereof - Google Patents

Selenium-rich polygonatum sibiricum whole powder and preparation method thereof Download PDF

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CN106923324B
CN106923324B CN201611153000.0A CN201611153000A CN106923324B CN 106923324 B CN106923324 B CN 106923324B CN 201611153000 A CN201611153000 A CN 201611153000A CN 106923324 B CN106923324 B CN 106923324B
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rhizoma polygonati
selenium
rich
whole powder
sealwort
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CN106923324A (en
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杨德
李露
薛淑静
陈晓春
郭鹏
高虹
史德芳
叶丽秀
周明
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Enshi Source Technology Development Co ltd
Farm Product Processing and Nuclear Agricultural Technology Institute of Hubei Academy of Agricultural Sciences
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Enshi Source Technology Development Co ltd
Farm Product Processing and Nuclear Agricultural Technology Institute of Hubei Academy of Agricultural Sciences
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    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23LFOODS, FOODSTUFFS, OR NON-ALCOHOLIC BEVERAGES, NOT COVERED BY SUBCLASSES A21D OR A23B-A23J; THEIR PREPARATION OR TREATMENT, e.g. COOKING, MODIFICATION OF NUTRITIVE QUALITIES, PHYSICAL TREATMENT; PRESERVATION OF FOODS OR FOODSTUFFS, IN GENERAL
    • A23L2/00Non-alcoholic beverages; Dry compositions or concentrates therefor; Their preparation
    • A23L2/385Concentrates of non-alcoholic beverages
    • A23L2/39Dry compositions
    • AHUMAN NECESSITIES
    • A23FOODS OR FOODSTUFFS; TREATMENT THEREOF, NOT COVERED BY OTHER CLASSES
    • A23VINDEXING SCHEME RELATING TO FOODS, FOODSTUFFS OR NON-ALCOHOLIC BEVERAGES AND LACTIC OR PROPIONIC ACID BACTERIA USED IN FOODSTUFFS OR FOOD PREPARATION
    • A23V2002/00Food compositions, function of food ingredients or processes for food or foodstuffs

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  • Health & Medical Sciences (AREA)
  • Nutrition Science (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Food Science & Technology (AREA)
  • Polymers & Plastics (AREA)
  • Preparation Of Fruits And Vegetables (AREA)
  • Coloring Foods And Improving Nutritive Qualities (AREA)

Abstract

The invention relates to a selenium-rich rhizoma polygonati whole powder and a preparation method thereof, wherein the selenium-rich rhizoma polygonati whole powder contains 60-80% of rhizoma polygonati; 20-40% of maltodextrin. The processing method comprises cleaning selenium-rich rhizoma Polygonati of selenium-rich production field, removing impurities, soaking in rhizoma Polygonati peeling agent, and peeling with nylon roller brush; cleaning with citric acid solution after peeling to neutralize residual alkali liquor on the surface; treating the peeled selenium-rich rhizoma Polygonati tubers for 90-180min at the high temperature and high pressure of 105-; pulping the processed selenium-rich rhizoma Polygonati tubers, and then performing enzymolysis by using high-temperature saccharifying enzyme; adding a certain amount of drying assistant (maltodextrin) into the selenium-rich rhizoma Polygonati homogenate obtained after enzymolysis, and homogenizing by a colloid mill; and spray drying the homogenized rhizoma polygonati homogenate to obtain selenium-rich rhizoma polygonati whole powder. The product obtained by the invention is light yellow powdery solid, has certain water solubility, contains functional components such as organic selenium and polygonatum polysaccharide, and has the characteristics of simple eating, high content of the functional components and the like; the invention has simple process, convenient operation and lower cost.

Description

Selenium-rich polygonatum sibiricum whole powder and preparation method thereof
Technical Field
The invention belongs to the field of food processing, and relates to selenium-rich polygonatum sibiricum whole powder and a preparation method thereof.
Background
Rhizoma Polygonati (Rhizoma Polygonatum) is dried rhizome of Polygonatum sibiricum of Polygonatum of Liliaceae (Liliaaeea), is a traditional medicinal and edible plant material with homology, and is also a plant resource special in Wuling mountain area. Rhizoma Polygonati contains starch, protein, vitamins, amino acids, microelements, and multiple physiologically active substances such as steroid saponin, polysaccharides, anthraquinone, lignanoid, and alkaloid. According to records of ancient books of famous physicians and others, polygonatum sibiricum can remove rheumatism, calm five internal organs, lighten body after long-term taking, prolong life and avoid hunger, and is one of the commonly used traditional Chinese medicines for resisting aging and preserving health. The selenium resource of Enshi is abundant, and the selenium content of the produced crops, traditional Chinese medicinal materials and the like is generally higher. Through determination, the selenium content in wild rhizoma polygonati tubers in Enshi Bifeng, Xuan En and the like reaches 0.4-0.8mg/kg, is 8-20 times of the selenium content in rhizoma polygonati tubers in other areas, and reaches the standard of selenium enrichment.
The traditional rhizoma polygonati processing method is nine times of steaming and nine times of drying in the sun, namely, the rhizoma polygonati and yellow wine are steamed together, then the rhizoma polygonati and the yellow wine are dried in the sun until the epidermis becomes dry, then the rhizoma polygonati and the yellow wine are soaked and then steamed, the steps are repeated for 9 times, and the consumed time is as long as about 1 month; and extracting rhizoma Polygonati functional components with water, concentrating into paste, and packaging to obtain rhizoma Polygonati paste, with high loss of functional components and high concentration cost. Because rhizoma polygonati is rich in polysaccharide, starch, dietary cellulose and other water-absorbing components, the traditional grinding process, the powdering process and the like can not prepare the rhizoma polygonati powder.
CN103931861A discloses a processing technology of selenium-rich polygonatum sibiricum preserved fruit, which sequentially comprises the steps of selecting materials, cleaning, rehydrating, dicing, soaking, blanching, sugar soaking, drying and packaging, wherein the sugar soaking treatment comprises the steps of adding clear water into mannitol to be placed in a boiling pot, preparing sweet solution, adding citric acid, heating until the mannitol is completely dissolved, adding the blanched polygonatum sibiricum dices, boiling until the polygonatum sibiricum dices are uniform, and taking out when the polygonatum sibiricum dices are sweet and sour, and putting the polygonatum sibiricum dices into a heat-preservation barrel for heat preservation. CN 105349356A discloses a method for preparing a fresh bamboo wine containing selenium-rich rhizoma Polygonati, which comprises soaking fresh selenium-rich rhizoma Polygonati in a white spirit jar of 52 degree in proportion for one year to obtain selenium-rich rhizoma Polygonati wine; selecting more than 2 years old moso bamboos without scabs and green mottles 10 days after the Qingming festival, selecting a bamboo joint section 1-2 m away from the ground, injecting selenium-rich yellow wine, allowing the bamboo joint section to grow, and taking out the moso bamboos after one year.
Disclosure of Invention
The invention aims to provide the selenium-rich polygonatum sibiricum whole powder which is beneficial to human health, is instant, easy to store and convenient to eat and the preparation method thereof.
The selenium-rich polygonatum sibiricum whole powder comprises the following components in percentage by mass: 60-80% of rhizoma polygonati; 20-40% of maltodextrin.
The preparation method of the selenium-rich polygonatum sibiricum whole powder comprises the following specific steps:
1) selecting and peeling, cleaning rhizoma Polygonati tuber of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati dehulling agent at 60 deg.C for 10-15min, and peeling off rhizoma Polygonati epidermis;
2) soaking the peeled rhizoma polygonati tubers obtained in the step 1) in a 0.2% citric acid solution, neutralizing residual alkali liquor on the surface, and then washing with clear water;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 90-180min at the central temperature of 105-;
4) pulping the sealwort processed in the step 3) by using a pulping machine until no obvious lumps can be seen by naked eyes, and then adding water to adjust the solid content to 10-20%;
5) adding high-temperature saccharifying enzyme with the mass of 0.5% of the rhizoma polygonati pulp obtained in the step 4), and treating at 50 ℃ for 3h, wherein stirring is carried out once every 20min in the treatment process;
6) adding 5% of maltodextrin drying aid into the rhizoma polygonati homogenate obtained in the step 5), homogenizing and homogenizing by a colloid mill for 15-25 cycles;
7) heating the homogenized rhizoma polygonati homogenate obtained in the step 6) to 60 ℃ by using a jacketed kettle, and then carrying out spray drying to obtain selenium-rich rhizoma polygonati whole powder;
the spray drying conditions are as follows: the air inlet temperature is 180 ℃, the air outlet temperature is 90 ℃, the feeding speed is 900ml/min, and the air inlet quantity is set to be 5.0m3/min。
The invention combines a rhizoma polygonati peeling process, a high-temperature high-pressure processing process, an enzymolysis process, a homogenization process and a spray drying process, and the obtained product furthest retains the functional components of rhizoma polygonati polysaccharide, rhizoma polygonati saponin, organic selenium and the like in the rhizoma polygonati; the process is simple, the operation is convenient, the cost is lower, and the practicability is high; the prepared product is easy to store, has the characteristic of instant dissolution and is convenient to eat; the product has low water content and good water solubility, can be compounded with other food raw materials to prepare different products such as tablets, granular beverages, instant powder and the like, and has wide technical applicability; .
Detailed Description
The selenium-rich polygonatum sibiricum whole powder contains 60-80% of polygonatum sibiricum; 20-40% of maltodextrin. The processing method comprises cleaning selenium-rich rhizoma Polygonati of selenium-rich production field, removing impurities, soaking in rhizoma Polygonati dehulling agent until the rhizoma Polygonati dehulling is clean; cleaning with citric acid solution after peeling to neutralize residual alkali liquor on the surface; treating the peeled selenium-rich rhizoma Polygonati tubers for 90-180min at the high temperature and high pressure of 105-; pulping the processed selenium-rich rhizoma Polygonati tubers, and then performing enzymolysis by using high-temperature saccharifying enzyme; adding a certain amount of maltodextrin drying aid into the selenium-rich rhizoma polygonati homogenate obtained after enzymolysis, and homogenizing by a colloid mill; and spray drying the homogenized rhizoma polygonati homogenate to obtain the selenium-rich rhizoma polygonati whole powder.
The technical solution of the present invention will be described with reference to the following examples.
The sealwort dehulling agent used in the step 1) is an aqueous solution of 5% of sodium hydroxide, 1% of trisodium phosphate and 0.1% of cinnamic acid. Washing with nylon roller brush and pressurized water until the epidermis of rhizoma Polygonati completely falls off.
The spray drying conditions are as follows: the air inlet temperature is 180 ℃, the air outlet temperature is 90 ℃, the feeding speed is 900ml/min, and the air inlet quantity is set to be 5.0m3And/min. Under the condition, the materials in the drying chamber are slightly adhered to the wall, the yield of the fine powder reaches 75-90%, and the polygonatum is rich in flavor and good in water solubility.
Example 1:
1) selecting and peeling, cleaning rhizoma Polygonati tubers of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati peeling agent at 60 deg.C for 10min, and washing with nylon roller brush and pressurized water until rhizoma Polygonati epidermis is peeled off completely;
the sealwort dehulling agent is an aqueous solution of 5 percent of sodium hydroxide, 1 percent of trisodium phosphate and 0.1 percent of cinnamic acid.
2) Soaking the peeled rhizoma polygonati tubers obtained in the step 1) in a 0.2% citric acid solution, neutralizing residual alkali liquor on the surface, and then washing with clear water;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 180min at the central temperature of 105 ℃ for processing;
4) pulping the sealwort processed in the step 3) by using a pulping machine until no obvious lumps can be seen by naked eyes, and then adding water to adjust the solid content to 10%;
5) adding high-temperature saccharifying enzyme with the mass of 0.5% of the rhizoma polygonati pulp obtained in the step 4), and treating at 50 ℃ for 3h, wherein stirring is carried out once every 20min in the treatment process;
6) adding 5% of maltodextrin drying aid into the rhizoma polygonati homogenate obtained in the step 5), homogenizing and homogenizing by a colloid mill for 15 cycles;
7) heating the homogenized rhizoma polygonati homogenate obtained in the step 6) to 60 ℃ by using a jacketed kettle, and then carrying out spray drying to obtain selenium-rich rhizoma polygonati whole powder;
the spray drying conditions are as follows: the air inlet temperature is 180 ℃, the air outlet temperature is 90 ℃, the feeding speed is 900ml/min, and the air inlet quantity is set to be 5.0m3/min。
example, the selenium-rich polygonatum sibiricum whole powder obtained in the drying chamber slightly sticks to the wall, the polygonatum sibiricum powder amount of the obtained selenium-rich polygonatum sibiricum whole powder can reach 90% of the dry matter content in the raw materials, and the polygonatum sibiricum is rich in flavor and good in water solubility.
Example 2, like example 1, except that,
1) selecting and peeling, cleaning rhizoma Polygonati tubers of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati peeling agent at 60 deg.C for 13min, and washing with nylon roller brush and pressurized water until rhizoma Polygonati epidermis is peeled off completely;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 120min at the central temperature of 110 ℃ to process;
4) pulping the sealwort processed in the step 3) by using a pulping machine until no obvious lumps can be seen by naked eyes, and then adding water to adjust the solid content to 15%;
6) adding 5% of maltodextrin drying aid into the rhizoma polygonati homogenate obtained in the step 5), homogenizing and homogenizing by a colloid mill for 20 cycles.
example, the selenium-rich polygonatum sibiricum whole powder obtained in the drying chamber slightly sticks to the wall, the polygonatum sibiricum powder amount of the obtained selenium-rich polygonatum sibiricum whole powder can reach 85% of the dry matter content in the raw materials, and the polygonatum sibiricum is rich in flavor and good in water solubility.
Example 3, like example 1, except that,
1) selecting and peeling, cleaning rhizoma Polygonati tubers of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati dehulling agent at 60 deg.C for 12min, and washing with nylon roller brush and pressurized water until the rhizoma Polygonati epidermis is completely peeled off;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 90min at the central temperature of 115 ℃ to process;
4) pulping the sealwort processed in the step 3) by using a pulping machine until no obvious lumps can be seen by naked eyes, and then adding water to adjust the solid content to 20%;
6) adding 5% of maltodextrin drying aid into the rhizoma polygonati homogenate obtained in the step 5), homogenizing and homogenizing by a colloid mill for 25 cycles.
example, the selenium-rich polygonatum sibiricum whole powder obtained in the drying chamber slightly sticks to the wall, the polygonatum sibiricum powder amount of the obtained selenium-rich polygonatum sibiricum whole powder can reach 75% of the dry matter content in the raw materials, and the polygonatum sibiricum is rich in flavor and good in water solubility.
Example 4, like example 1, except that,
1) selecting and peeling, cleaning rhizoma Polygonati tubers of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati peeling agent at 60 deg.C for 10min, and washing with nylon roller brush and pressurized water until rhizoma Polygonati epidermis is peeled off completely;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 90min at the central temperature of 115 ℃ to process;
4) pulping the pulped rhizoma polygonati by using a pulping machine, preferably, no obvious lumps can be seen by naked eyes, and then adjusting the solid content to 15%;
6) adding 5% drying assistant (maltodextrin) into the homogenized rhizoma Polygonati slurry, homogenizing with colloid mill, and homogenizing for 20 cycles;
example, the selenium-rich polygonatum sibiricum whole powder obtained in the drying chamber slightly sticks to the wall, the polygonatum sibiricum powder amount of the obtained selenium-rich polygonatum sibiricum whole powder can reach 80% of the dry matter content in the raw materials, and the polygonatum sibiricum is rich in flavor and good in water solubility.
Example 5, like example 1, except that,
1) selecting and peeling, cleaning rhizoma Polygonati tubers of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati peeling agent at 60 deg.C for 10min, and washing with nylon roller brush and pressurized water until rhizoma Polygonati epidermis is peeled off completely;
3) transferring the sealwort obtained in the step 2) into an autoclave, processing for 150min at the central temperature of 110 ℃, and processing;
4) pulping the pulped rhizoma polygonati by using a pulping machine, preferably, no obvious lumps can be seen by naked eyes, and then adjusting the solid content to 15%;
6) adding 5% drying assistant (maltodextrin) into the homogenized rhizoma Polygonati slurry, homogenizing with colloid mill, and homogenizing for 20 cycles;
in this embodiment, the selenium-rich polygonatum sibiricum whole powder obtained in the drying chamber slightly adheres to the wall, the polygonatum sibiricum powder amount of the obtained selenium-rich polygonatum sibiricum whole powder can reach 85% of the dry matter content in the raw materials, and the polygonatum sibiricum is rich in flavor and good in water solubility.

Claims (2)

1. The preparation method of the selenium-rich polygonatum sibiricum whole powder is characterized by comprising the following steps: the preparation method comprises the following specific steps:
1) selecting and peeling, cleaning rhizoma Polygonati tuber of selenium-rich production place, removing impurities, soaking in water solution containing rhizoma Polygonati dehulling agent at 60 deg.C for 10-15min, and peeling off rhizoma Polygonati epidermis;
the sealwort dehulling agent is an aqueous solution of 5 percent of sodium hydroxide, 1 percent of trisodium phosphate and 0.1 percent of cinnamic acid;
2) soaking the peeled rhizoma polygonati tubers obtained in the step 1) in a 0.2% citric acid solution, neutralizing residual alkali liquor on the surface, and then washing with clear water;
3) transferring the sealwort obtained in the step 2) into an autoclave, and processing for 90-180min at the central temperature of 105-;
4) pulping the sealwort processed in the step 3) by using a pulping machine until no obvious lumps can be seen by naked eyes, and then adding water to adjust the solid content to 10-20%;
5) adding high-temperature saccharifying enzyme with the mass of 0.5% of the rhizoma polygonati pulp obtained in the step 4), and treating at 50 ℃ for 3h, wherein stirring is carried out once every 20min in the treatment process;
6) adding 5% of maltodextrin drying aid into the rhizoma polygonati homogenate obtained in the step 5), homogenizing and homogenizing by a colloid mill for 15-25 cycles;
7) heating the rhizoma polygonati homogenate homogenized in the step 6) to 60 ℃ by using a jacketed kettle, and then performing spray drying to obtain the following components in percentage by mass: 60-80% of sealwort; maltodextrin 20-40% of selenium-rich rhizoma Polygonati powder;
the spray drying conditions are as follows: the air inlet temperature is 180 ℃, the air outlet temperature is 90 ℃, the feeding speed is 900ml/min, and the air inlet quantity is set to be 5.0m3Min; under the condition, the materials in the drying chamber are slightly adhered to the wall, the yield of the fine powder reaches 75-90%, and the polygonatum is rich in flavor and good in water solubility.
2. The method for preparing the selenium-rich polygonatum sibiricum whole powder of claim 1, which is characterized by comprising the following steps: washing with a nylon rolling brush and pressurized water in the step 1) until the surfaces of the sealwort are peeled off completely.
CN201611153000.0A 2016-12-14 2016-12-14 Selenium-rich polygonatum sibiricum whole powder and preparation method thereof Active CN106923324B (en)

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CN109527317A (en) * 2018-10-16 2019-03-29 恩施徕福硒业有限公司 A kind of Selenium in Plants solid beverage and preparation method thereof
CN109486630A (en) * 2018-12-19 2019-03-19 成都青衣美人科技有限公司 A kind of sealwort wine and preparation method thereof
CN115990226A (en) * 2022-11-04 2023-04-21 中国农业科学院农产品加工研究所 Polygonatum sibiricum powder for improving active ingredients in rhizoma polygonati, and processing method and application thereof
CN116035153A (en) * 2023-03-06 2023-05-02 安徽中志科技有限公司 Selenium-enriched collagen dietary fiber protein powder solid beverage

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CN103783517B (en) * 2013-12-31 2016-01-20 陈慧珊 A kind of Rhizoma Dioscoreae Rhizoma Polygonati dispersible tablet and preparation method
CN105285559A (en) * 2014-06-30 2016-02-03 河南省淼雨饮品股份有限公司 Processing method of instant Chinese yam rhizome powder
CN105029154B (en) * 2015-06-19 2018-08-14 恩施州源惠科技开发有限公司 A kind of Siberian solomonseal rhizome polysaccharide rapidly dissolving tablet and processing method
CN105341942A (en) * 2015-11-10 2016-02-24 胡志荣 Preparation method for polygonatum sibiricum composite nutrition powder

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