CN106917096A - 一种银制品清洗剂及其制备方法 - Google Patents

一种银制品清洗剂及其制备方法 Download PDF

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CN106917096A
CN106917096A CN201710215892.0A CN201710215892A CN106917096A CN 106917096 A CN106917096 A CN 106917096A CN 201710215892 A CN201710215892 A CN 201710215892A CN 106917096 A CN106917096 A CN 106917096A
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parts
water
cleaning agent
silverware
preparation
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银柳香
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LIUZHOU LIJIE TECHNOLOGY Co Ltd
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LIUZHOU LIJIE TECHNOLOGY Co Ltd
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Priority to CN201710215892.0A priority Critical patent/CN106917096A/zh
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    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23G—CLEANING OR DE-GREASING OF METALLIC MATERIAL BY CHEMICAL METHODS OTHER THAN ELECTROLYSIS
    • C23G1/00—Cleaning or pickling metallic material with solutions or molten salts
    • C23G1/02—Cleaning or pickling metallic material with solutions or molten salts with acid solutions
    • C23G1/10—Other heavy metals
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/1229—Composition of the substrate
    • C23C18/1241—Metallic substrates
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C—CHEMISTRY; METALLURGY
    • C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
    • C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
    • C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
    • C23C18/02—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition
    • C23C18/12—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating by thermal decomposition characterised by the deposition of inorganic material other than metallic material
    • C23C18/125—Process of deposition of the inorganic material
    • C23C18/1279—Process of deposition of the inorganic material performed under reactive atmosphere, e.g. oxidising or reducing atmospheres

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • General Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • Organic Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Cosmetics (AREA)

Abstract

本发明公开了一种银制品清洗剂，是由按照重量份计的以下原料制备得到的：硫酸65‑75份、磷酸4‑6份、氟硅酸14‑16份、硫酸汞3‑6份、硫酸银8‑10份、硫酸钠12‑14份、1,4‑丁炔二醇6‑8份、水20‑24份；并提供了其制备方法。本发明的有益效果为：本发明提供的一种银制品清洗剂及其制备方法，能够快速清洗银制品，使其恢复原有光泽，不会损伤表面的光滑程度，同时，本清洗剂清洗后，可减缓银制品的发黑发乌现象。

Description

一种银制品清洗剂及其制备方法
技术领域
本发明涉及化学制剂领域，具体涉及一种银制品清洗剂及其制备方法。
背景技术
银制品，是一种以金属银打造的制品，质地光滑，富有光泽。银是一种比较活泼的贵重金属，在空气中极易与硫或硫化氢反应而生成黑色的硫化银，长期使用的银首饰由于表面很少受到磨擦，放置后这种发黑变乌现象更严重。现有市售的专业银制品清洗剂大多清洗速度慢，无法满足市场需求。
发明内容
本发明的目的就是针对上述现有技术中的缺陷，提供了一种银制品清洗剂及其制备方法。
为了实现上述目的，本发明提供的技术方案为：一种银制品清洗剂，是由按照重量份计的以下原料制备得到的：
硫酸65-75份、磷酸4-6份、氟硅酸14-16份、硫酸汞3-6份、硫酸银8-10份、硫酸钠12-14份、1,4-丁炔二醇6-8份、水20-24份。
进一步的，上述的一种银制品清洗剂，是由按照重量份计的以下原料制备得到的：
硫酸70份、磷酸5份、氟硅酸14份、硫酸汞5份、硫酸银10份、硫酸钠14份、1,4-丁炔二醇7份、水24份。
进一步的，上述的一种银制品清洗剂，所述清洗剂是将除水以外的各组分置于水浴70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
本发明的第二个目的是提供了上述一种银制品清洗剂的制备方法，将除水以外的各组分置于水浴70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
本发明的有益效果为：本发明提供的一种银制品清洗剂及其制备方法，能够快速清洗银制品，使其恢复原有光泽，不会损伤表面的光滑程度，同时，本清洗剂清洗后，可减缓银制品的发黑发乌现象。
具体实施方式
实施例1：
一种银制品清洗剂，是由以下原料制备得到的：
硫酸65-75kg、磷酸4-6kg、氟硅酸14-16kg、硫酸汞3-6kg、硫酸银8-10kg、硫酸钠12-14kg、1,4-丁炔二醇6-8kg、水20-24kg。
其制备方法为：是将除水以外的各组分置于水浴70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
实施例2：
一种银制品清洗剂，是由以下原料制备得到的：
硫酸70g、磷酸5g、氟硅酸14g、硫酸汞5g、硫酸银10g、硫酸钠14g、1,4-丁炔二醇7g、水24g。
其制备方法为：是将除水以外的各组分置于水浴70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
最后应说明的是：以上所述仅为本发明的优选实施例而已，并不用于限制本发明，尽管参照前述实施例对本发明进行了详细的说明，对于本领域的技术人员来说，其依然可以对前述各实施例所记载的技术方案进行修改，或者对其中部分技术特征进行等同替换。凡在本发明的精神和原则之内，所作的任何修改、等同替换、改进等，均应包含在本发明的保护范围之内。

Claims (4)

1.一种银制品清洗剂，其特征在于，是由按照重量份计的以下原料制备得到的：
硫酸65-75份、磷酸4-6份、氟硅酸14-16份、硫酸汞3-6份、硫酸银8-10份、硫酸钠12-14份、1,4-丁炔二醇6-8份、水20-24份。
2.根据权利要求1所述的一种银制品清洗剂，其特征在于，是由按照重量份计的以下原料制备得到的：
硫酸70份、磷酸5份、氟硅酸14份、硫酸汞5份、硫酸银10份、硫酸钠14份、1,4-丁炔二醇7份、水24份。
3.根据权利要求1或2所述的一种银制品清洗剂，其特征在于，所述清洗剂是将除水以外的各组分置于水浴60-70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
4.根据权利要求1或2所述的一种银制品清洗剂的制备方法，其特征在于，是将除水以外的各组分置于水浴60-70℃环境下，边搅拌边加入水，待其完全搅拌均匀后，再保持水浴加热2h后，制备得到的。
CN201710215892.0A 2017-03-31 2017-03-31 一种银制品清洗剂及其制备方法 Pending CN106917096A (zh)

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Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3468804A (en) * 1964-03-13 1969-09-23 Winfield Brooks Co Inc Silver cleaning composition
US5669978A (en) * 1995-07-03 1997-09-23 Brown; Mattie L. Method for removing scale from silver articles using an aqueous oxalic acid solution
JPH1046375A (ja) * 1996-07-31 1998-02-17 Sumitomo Metal Mining Co Ltd 銀の硫化被膜洗浄剤
CN1198783A (zh) * 1996-06-08 1998-11-11 雷克特和科尔曼产品有限公司 清洗银或铜的组合物
CN102660747A (zh) * 2012-04-13 2012-09-12 中国文化遗产研究院 用于银器与鎏金银器保护的硫脲类复配除锈剂和除锈膏

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3468804A (en) * 1964-03-13 1969-09-23 Winfield Brooks Co Inc Silver cleaning composition
US5669978A (en) * 1995-07-03 1997-09-23 Brown; Mattie L. Method for removing scale from silver articles using an aqueous oxalic acid solution
CN1198783A (zh) * 1996-06-08 1998-11-11 雷克特和科尔曼产品有限公司 清洗银或铜的组合物
JPH1046375A (ja) * 1996-07-31 1998-02-17 Sumitomo Metal Mining Co Ltd 銀の硫化被膜洗浄剤
CN102660747A (zh) * 2012-04-13 2012-09-12 中国文化遗产研究院 用于银器与鎏金银器保护的硫脲类复配除锈剂和除锈膏

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Application publication date: 20170704