CN106916476A - A kind of concave convex rod surface lacquer and preparation method - Google Patents
A kind of concave convex rod surface lacquer and preparation method Download PDFInfo
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- CN106916476A CN106916476A CN201710231012.9A CN201710231012A CN106916476A CN 106916476 A CN106916476 A CN 106916476A CN 201710231012 A CN201710231012 A CN 201710231012A CN 106916476 A CN106916476 A CN 106916476A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D5/00—Coating compositions, e.g. paints, varnishes or lacquers, characterised by their physical nature or the effects produced; Filling pastes
- C09D5/08—Anti-corrosive paints
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/02—Elements
- C08K3/04—Carbon
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- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K3/00—Use of inorganic substances as compounding ingredients
- C08K3/34—Silicon-containing compounds
- C08K3/346—Clay
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K9/00—Use of pretreated ingredients
- C08K9/02—Ingredients treated with inorganic substances
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
- C09D7/62—Additives non-macromolecular inorganic modified by treatment with other compounds
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Abstract
The invention discloses a kind of concave convex rod surface lacquer and preparation method, belong to paint technology field.The preparation method of the surface lacquer is：Natural attapulgite clay is purified first is pre-processed, then respectively through alkalization, acidified modified treatment, then 500 DEG C ~ 800 DEG C of Muffle 3 ~ 5h of kiln roasting will be placed in after the Concave-convex clay rod drying after treatment again, be ground after cooling, obtain modified Concave-convex clay rod；Finally, in parts by weight, 20 ~ 30 parts of modified Concave-convex clay rod, 1 ~ 5 part of Graphene, 60 ~ 80 parts of mixing of surface lacquer are weighed respectively, is stirred, obtain final product the attapulgite's surface paint.The concave convex rod surface lacquer not only has preferable water-tight corrosion-proof effect, additionally it is possible to the harmful substance for effectively going paint-removing itself to give out so that the characteristics of surface lacquer is using having green non-pollution.Additionally, the preparation method is simple and easy to apply, with preferable application value.
Description
Technical field
The present invention relates to paint technology field, and in particular to a kind of concave convex rod surface lacquer and preparation method.
Background technology
It is known, with the progress and development of society, although people significantly improve to the consciousness of health and environmental protection, but
It is, as the affaires such as substantial amounts of construction material, ornament materials and Wood-based Panel Furniture enter in family or working entertainment place,
And the density of building is continuously increased in urban construction, indoor environmental quality of today also become be not it is so optimistic, its
In a major reason be exactly：For smooth good-looking, the water-fast, acid and alkali-resistance in the surface for ensureing these affaires, while also to make
There is moistureproof, corrosion-resistant to act on for it, and the surface of these affaires will spray one layer of table containing chemical industry toxic substance substantially
Finish paint, and ever-increasing site coverage is highly detrimental to air circulation, i.e., current indoor environment is highly detrimental to discharge
The toxic substance that the enamelled coating on affaires surface is volatilized；On the other hand, according to incompletely statistics, the people in city are one
The time that 80% is will be about within it tides over indoors, therefore, how effectively to remove or suppress indoor and build
The chemical industry toxin for building material, ornament materials or Wood-based Panel Furniture and other items volatilization generation has become indoor environment scientific research
One of important topic.
The Chinese invention patent of Patent No. CN103468046A is disclosed and a kind of is related to the activated carbon surface in paint field
Paint, described activated carbon surface paint is uniformly mixed by surface lacquer with the activated carbon for accounting for its gross weight 3~10%；Described work
Property charcoal should reach following requirement：Methylenum careuleum adsorption rate（0.15%）>=10ml, iodine sorption value >=900mg/g, benzene adsorption rate >=
40%, total ash≤3%, the mesh of fineness 300 passes through 80%；Although described activated carbon surface paint be able to can be sent out surface lacquer itself
Toxic substance has certain suction-operated, but the adsorption effect of activated carbon is limited, and to the antiseptic effect of surface lacquer not
It is preferable.
Therefore, researching and developing one kind both has preferable water-tight corrosion-proof effect, and the surface with green non-pollution is painted
It is the emphasis of current research, it may have preferable application prospect and use value.
The content of the invention
For defect of the prior art, it is an object of the invention to provide a kind of concave convex rod surface lacquer and preparation method, institute
Stating concave convex rod surface lacquer not only has preferable water-tight corrosion-proof effect, additionally it is possible to the nuisance for effectively going paint-removing itself to give out
Matter so that the characteristics of surface lacquer is using having green non-pollution, for the healthy living of people provides guarantee.And the present invention
The surface lacquer has preferable mechanical property, can greatly prolong the service life of surface lacquer, additionally, the preparation method is simple
It is easy, with preferable application value.
The present invention solves technical problem and adopts the following technical scheme that：
The present invention relates to a kind of preparation method of concave convex rod surface lacquer, comprise the following steps：
（1）Taking natural attapulgite clay carries out being crushed to 100 ~ 200 mesh, adds water, and stirring forms mud in suspension, then by ultrasound
After fully dispersed, upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；
Filter cake is placed in beaker, methyl alcohol is added, in 10 ~ 20min of ultrasound, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain
Concave-convex clay rod pretreatment product；
（2）Concave-convex clay rod pretreatment product is placed in sodium bicarbonate solution, 2 ~ 5h is soaked, vacuum filtration simultaneously washs filter
Cake；
（3）By step（2）In the Concave-convex clay rod that obtains be placed in flask, the watery hydrochloric acid of 2moL/L is added, in ultrasonic wave bar
20 ~ 30min, vacuum filtration after standing are mixed under part, and washs filter cake；
（4）By step（3）In be placed in 500 DEG C ~ 800 DEG C of Muffle 3 ~ 5h of kiln roasting after the Concave-convex clay rod drying that obtains,
Particle diameter is ground to after cooling for 100 ~ 200 mesh, modified Concave-convex clay rod is obtained；
（5）In parts by weight, weigh respectively 20 ~ 30 parts of modified Concave-convex clay rod, 1 ~ 5 part of Graphene, surface lacquer 60 ~
80 parts of mixing, stir, and obtain final product the attapulgite's surface paint.
Preferably, the step（1）In the weight that adds water be 3 ~ 8 times of Concave-convex clay rod weight.
Preferably, the step（1）The addition volume of middle methyl alcohol is 50mL with Concave-convex clay rod mass ratio：10~15g.
Preferably, the step（2）The addition quality of middle sodium acid carbonate is 0.1 ~ 0.5 times of Concave-convex clay rod quality.
Preferably, the step（3）The volume that middle watery hydrochloric acid is added is 1mL with concave convex rod mass ratio：2g~10g.
Preferably, the step（2）And step（3）The washing step of middle filter cake includes being placed in filter cake in distilled water, in
5 ~ 10min of ultrasound, suction filtration, are repeated twice operation under ultrasound condition, you can.
Preferably, the step（4）The addition sequence of middle raw material is first to mix Concave-convex clay rod, Graphene and suitable quantity of water
Conjunction stirs, then is placed in 10 ~ 20min of ultrasound under Ultrasonic Conditions, then again to adding surface lacquer in mixture, you can.
The invention further relates to a kind of concave convex rod surface lacquer, the concave convex rod surface lacquer is by the concave convex rod surface lacquer
Preparation method is prepared.
Compared with prior art, the present invention has following beneficial effect：
（1）Concave convex rod surface lacquer of the present invention, due to the presence of Concave-convex clay rod so that the surface lacquer not only has
Preferable water-tight corrosion-proof effect, additionally it is possible to the harmful substance for effectively going paint-removing itself to give out so that the surface lacquer is used
The characteristics of with green non-pollution, additionally, the Concave-convex clay rod added in surface lacquer can also to surrounding enviroment in poisonous have
Evil and bad smell play certain absorption, removal effect, for the healthy living of people provides guarantee.Additionally, the preparation
Method is simple and easy to apply, easy to operate, is adapted to industrial applications, with preferable application value.
（2）The modified Concave-convex clay rod added in surface lacquer of the present invention, not only increases attapulgite
The porosity of clay, also effectively eliminates that acid therein is molten and alkali soluble impurity, can greatly increase Concave-convex clay rod on surface
Dispersing uniformity in paint, and absorption of the Concave-convex clay rod to pernicious gas can be effectively improved.
（3）Grapheme material is added with coating of the present invention, because Graphene has unique laminar structured, layer
Stacking plus the fine and close physical isolation layer of formation so that there is the surface lacquer after addition Graphene preferable physical isolation waterproof to make
With along with Graphene has excellent mechanical property, for the mechanical strength of surface lacquer provides guarantee, enhancing surface lacquer
Service life, and then reduce use cost.
Specific embodiment
With reference to specific embodiment, the present invention is expanded on further.These embodiments be merely to illustrate the present invention and without
In limitation the scope of the present invention.The experimental technique of unreceipted actual conditions in the following example, generally according to normal condition, for example
Sambrook equimoleculars are cloned：Laboratory manual（New York:Cold Spring Harbor Laboratory Press,
1989）Described in condition, or according to the condition proposed by manufacturer.
Embodiment 1：
A kind of concave convex rod surface lacquer and preparation method of the preferred embodiment of the present invention；
The preparation method of the concave convex rod surface lacquer, comprises the following steps：
（1）Taking natural attapulgite clay carries out being crushed to 200 mesh, adds 5 times of water of amount of Concave-convex clay rod weight, stirring
Formed mud in suspension, then by ultrasound it is fully dispersed after, take upper suspension centrifugal treating in the centrifuge of 3000 turns/min
10 min, vacuum filtration after standing；Filter cake is placed in beaker, methyl alcohol is added, in ultrasonic 15 min under Ultrasonic Conditions, stood
Vacuum filtration, is dried to obtain Concave-convex clay rod pretreatment product afterwards, wherein, addition volume and the Concave-convex clay rod matter of methyl alcohol
Amount is than being 50mL：12 g；
（2）Concave-convex clay rod pretreatment product is placed in sodium bicarbonate solution, 3 h are soaked, vacuum filtration simultaneously washs filter cake,
Wherein, the addition quality of sodium acid carbonate is 0.3 times of Concave-convex clay rod quality；
（3）By step（2）In the Concave-convex clay rod that obtains be placed in flask, the watery hydrochloric acid of 2moL/L is added, in ultrasonic wave bar
20 min are mixed under part, vacuum filtration after standing, and filter cake is washed, wherein, volume and concave convex rod that watery hydrochloric acid is added
Mass ratio is 1mL：8 g；
（4）By step（3）In be placed in 600 DEG C of the h of Muffle kiln roasting 5 after the Concave-convex clay rod drying that obtains, ground after cooling
Particle diameter is milled to for 200 mesh, modified Concave-convex clay rod is obtained；
（5）In parts by weight, 25 parts of modified Concave-convex clay rod, 3 parts of Graphene, 70 parts of surface lacquer are weighed respectively to mix
Close, stir, obtain final product the attapulgite's surface paint.
Step（2）And step（3）The washing step of middle filter cake includes being placed in filter cake in distilled water, in super under ultrasound condition
The min of sound 10, suction filtration is repeated twice operation, you can.
Step（4）The addition sequence of middle raw material be first by Concave-convex clay rod, Graphene and suitable quantity of water mixing and stirring,
Ultrasonic 15 min under Ultrasonic Conditions is placed in again, then can effectively improve attapulgite to surface lacquer is added in mixture again
Dispersing uniformity with Graphene in surface lacquer.
The concave convex rod surface lacquer is to be prepared by the preparation method of the concave convex rod surface lacquer.
Embodiment 2：
A kind of concave convex rod surface lacquer and preparation method of the preferred embodiment of the present invention；
The preparation method of the concave convex rod surface lacquer, comprises the following steps：
（1）Taking natural attapulgite clay carries out being crushed to 100 mesh, adds 3 times of water of amount of Concave-convex clay rod weight, stirring
Formed mud in suspension, then by ultrasound it is fully dispersed after, take upper suspension centrifugal treating 5 in the centrifuge of 3000 turns/min
Min, vacuum filtration after standing；Filter cake is placed in beaker, methyl alcohol is added, in ultrasonic 10 min under Ultrasonic Conditions, after standing
Vacuum filtration, is dried to obtain Concave-convex clay rod pretreatment product, wherein, addition volume and the Concave-convex clay rod quality of methyl alcohol
Than being 50mL：10 g；
（2）Concave-convex clay rod pretreatment product is placed in sodium bicarbonate solution, 2 h are soaked, vacuum filtration simultaneously washs filter cake,
Wherein, the addition quality of sodium acid carbonate is 0.1 times of Concave-convex clay rod quality；
（3）By step（2）In the Concave-convex clay rod that obtains be placed in flask, the watery hydrochloric acid of 2moL/L is added, in ultrasonic wave bar
2 min are mixed under part, vacuum filtration after standing, and filter cake is washed, wherein, volume and concave convex rod matter that watery hydrochloric acid is added
The ratio between amount is 1mL：2g；
（4）By step（3）In be placed in 800 DEG C of the h of Muffle kiln roasting 3 after the Concave-convex clay rod drying that obtains, ground after cooling
Particle diameter is milled to for 100 mesh, modified Concave-convex clay rod is obtained；
（5）In parts by weight, 20 parts of modified Concave-convex clay rod, 1 part of Graphene, 60 parts of surface lacquer are weighed respectively to mix
Close, stir, obtain final product the attapulgite's surface paint.
Step（2）And step（3）The washing step of middle filter cake includes being placed in filter cake in distilled water, in super under ultrasound condition
The min of sound 5, suction filtration is repeated twice operation, you can.
Step（4）The addition sequence of middle raw material be first by Concave-convex clay rod, Graphene and suitable quantity of water mixing and stirring,
Ultrasonic 10 min under Ultrasonic Conditions is placed in again, then can effectively improve attapulgite to surface lacquer is added in mixture again
Dispersing uniformity with Graphene in surface lacquer.
The concave convex rod surface lacquer is to be prepared by the preparation method of the concave convex rod surface lacquer.
Embodiment 3：
A kind of concave convex rod surface lacquer and preparation method of the preferred embodiment of the present invention；
The preparation method of the concave convex rod surface lacquer, comprises the following steps：
（1）Taking natural attapulgite clay carries out being crushed to 200 mesh, adds 8 times of water of amount of Concave-convex clay rod weight, stirring
Formed mud in suspension, then by ultrasound it is fully dispersed after, take upper suspension centrifugal treating in the centrifuge of 3000 turns/min
10min, vacuum filtration after standing；Filter cake is placed in beaker, methyl alcohol is added, in ultrasound 20min under Ultrasonic Conditions, after standing
Vacuum filtration, is dried to obtain Concave-convex clay rod pretreatment product, wherein, addition volume and the Concave-convex clay rod quality of methyl alcohol
Than being 50mL：15g；
（2）Concave-convex clay rod pretreatment product is placed in sodium bicarbonate solution, 5 h are soaked, vacuum filtration simultaneously washs filter cake,
Wherein, the addition quality of sodium acid carbonate is 0.5 times of Concave-convex clay rod quality；
（3）By step（2）In the Concave-convex clay rod that obtains be placed in flask, the watery hydrochloric acid of 2moL/L is added, in ultrasonic wave bar
30 min are mixed under part, vacuum filtration after standing, and filter cake is washed, wherein, volume and concave convex rod that watery hydrochloric acid is added
Mass ratio is 1mL：10 g；
（4）By step（3）In be placed in 500 DEG C of the h of Muffle kiln roasting 5 after the Concave-convex clay rod drying that obtains, ground after cooling
Particle diameter is milled to for 200 mesh, modified Concave-convex clay rod is obtained；
（5）In parts by weight, 30 parts of modified Concave-convex clay rod, 5 parts of Graphene, 80 parts of surface lacquer are weighed respectively to mix
Close, stir, obtain final product the attapulgite's surface paint.
Step（2）And step（3）The washing step of middle filter cake includes being placed in filter cake in distilled water, in super under ultrasound condition
The min of sound 10, suction filtration is repeated twice operation, you can.
Step（4）The addition sequence of middle raw material be first by Concave-convex clay rod, Graphene and suitable quantity of water mixing and stirring,
Ultrasonic 20 min under Ultrasonic Conditions is placed in again, then can effectively improve attapulgite to surface lacquer is added in mixture again
Dispersing uniformity with Graphene in surface lacquer.
The concave convex rod surface lacquer is to be prepared by the preparation method of the concave convex rod surface lacquer.
In sum, concave convex rod surface lacquer of the present invention, due to the presence of attapulgite, can effectively remove paint-removing
The harmful substance for itself giving out so that the characteristics of surface lacquer is using having green non-pollution, is the healthy living of people
There is provided guarantee.The presence of Graphene also enhances the mechanics of surface lacquer while greatly strengthen surface lacquer water-tight corrosion-proof effect
Intensity, extends the service life of surface lacquer.Additionally, the preparation method is simple and easy to apply, easy to operate, being adapted to industrialization should
With with preferable application value.
Specific embodiment of the invention is described above.It is to be appreciated that the invention is not limited in above-mentioned
Particular implementation, those skilled in the art can within the scope of the claims make various deformations or amendments, this not shadow
Sound substance of the invention.
Claims (8)
1. a kind of preparation method of concave convex rod surface lacquer, it is characterised in that comprise the following steps：
（1）Taking natural attapulgite clay carries out being crushed to 100 ~ 200 mesh, adds water, and stirring forms mud in suspension, then by ultrasound
After fully dispersed, upper suspension 5 ~ 10min of centrifugal treating in the centrifuge of 3000 turns/min, vacuum filtration after standing are taken；
Filter cake is placed in beaker, methyl alcohol is added, in 10 ~ 20min of ultrasound, vacuum filtration after standing under Ultrasonic Conditions, is dried to obtain
Concave-convex clay rod pretreatment product；
（2）Concave-convex clay rod pretreatment product is placed in sodium bicarbonate solution, 2 ~ 5h is soaked, vacuum filtration simultaneously washs filter
Cake；
（3）By step（2）In the Concave-convex clay rod that obtains be placed in flask, the watery hydrochloric acid of 2moL/L is added, in ultrasonic wave bar
20 ~ 30min, vacuum filtration after standing are mixed under part, and washs filter cake；
（4）By step（3）In be placed in 500 DEG C ~ 800 DEG C of Muffle 3 ~ 5h of kiln roasting after the Concave-convex clay rod drying that obtains,
Particle diameter is ground to after cooling for 100 ~ 200 mesh, modified Concave-convex clay rod is obtained；
（5）In parts by weight, weigh respectively 20 ~ 30 parts of modified Concave-convex clay rod, 1 ~ 5 part of Graphene, surface lacquer 60 ~
80 parts of mixing, stir, and obtain final product the attapulgite's surface paint.
2. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（1）In add water
Weight be 3 ~ 8 times of Concave-convex clay rod weight.
3. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（1）Middle methyl alcohol
Addition volume and Concave-convex clay rod mass ratio be 50mL：10~15g.
4. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（2）Middle carbonic acid
The addition quality of hydrogen sodium is 0.1 ~ 0.5 times of Concave-convex clay rod quality.
5. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（3）In dilute salt
The volume that acid is added is 1mL with concave convex rod mass ratio：2g~10g.
6. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（2）And step
（3）The washing step of middle filter cake includes being placed in filter cake in distilled water, and in 5 ~ 10min of ultrasound under ultrasound condition, suction filtration repeats two
Secondary operation, you can.
7. the preparation method of concave convex rod surface lacquer according to claim 1, it is characterised in that：The step（4）Middle raw material
Addition sequence be, first by Concave-convex clay rod, Graphene and suitable quantity of water mixing and stirring, then to be placed under Ultrasonic Conditions and surpass
10 ~ 20min of sound, then again to adding surface lacquer in mixture, you can.
8. a kind of concave convex rod surface lacquer, it is characterised in that：The concave convex rod surface lacquer is by described in any one of claim 1 ~ 7
Method be prepared.
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| CN107189619A (en) * | 2017-07-05 | 2017-09-22 | 合肥市片叶装饰工程有限公司 | Porcelain-like decorative material and preparation method thereof |
| CN107298937A (en) * | 2017-08-08 | 2017-10-27 | 合肥安力电力工程有限公司 | A kind of capacitor electrically-conducting paint and preparation method |
| CN108219564A (en) * | 2018-04-09 | 2018-06-29 | 合肥博之泰电子科技有限公司 | A kind of environmental-protection decoration type putty being modified based on concave convex rod and preparation method thereof |
| CN115403941A (en) * | 2022-09-28 | 2022-11-29 | 江苏清源新材料科技有限公司 | Modified attapulgite clay and preparation method and application thereof |
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| CN107189619A (en) * | 2017-07-05 | 2017-09-22 | 合肥市片叶装饰工程有限公司 | Porcelain-like decorative material and preparation method thereof |
| CN107298937A (en) * | 2017-08-08 | 2017-10-27 | 合肥安力电力工程有限公司 | A kind of capacitor electrically-conducting paint and preparation method |
| CN108219564A (en) * | 2018-04-09 | 2018-06-29 | 合肥博之泰电子科技有限公司 | A kind of environmental-protection decoration type putty being modified based on concave convex rod and preparation method thereof |
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