CN106913484A - A kind of production method of perfume stick - Google Patents
A kind of production method of perfume stick Download PDFInfo
- Publication number
- CN106913484A CN106913484A CN201710205326.1A CN201710205326A CN106913484A CN 106913484 A CN106913484 A CN 106913484A CN 201710205326 A CN201710205326 A CN 201710205326A CN 106913484 A CN106913484 A CN 106913484A
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- Prior art keywords
- leaf
- stick
- perfume
- production method
- mixed
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Classifications
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/02—Cosmetics or similar toiletry preparations characterised by special physical form
- A61K8/0216—Solid or semisolid forms
- A61K8/0229—Sticks
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q13/00—Formulations or additives for perfume preparations
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/805—Corresponding aspects not provided for by any of codes A61K2800/81 - A61K2800/95
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/84—Products or compounds obtained by lyophilisation, freeze-drying
Abstract
The invention discloses a kind of production method of perfume stick, fresh Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are put into decoyl hydroximic acid solution and are soaked by Bu Zhou ﹕ under Bao includes Yi；Freeze-drying；Crush, mix；Second distillation；First distillate, after-fractionating liquid, deodorizing alcohol, eucalyptus oil, bergamot oil, osmanthus essential oil are mixed, mixed liquor is obtained, it is standby；Sponge stick is put into and contains immersion in parahydroxyacet-ophenone, the mixed solution of chitin；Mixed liquor, sponge stick carry out vacuum infiltration in being put into vacuum infiltration tank；Sponge stick carries out microporous barrier cladding, both obtains perfume stick.Perfume aromatic flavour of the present invention, persistently, and for inspirator, the effect with preventing cough, asthma, wind wheat simultaneously, also with treatment is dizzy, headache health care auxiliaring effect.
Description
Technical field
The present invention relates to a kind of production method of perfume stick, belong to perfume area.
Background technology
Perfume is a kind of liquid for being mixed with essential oil, fixative and alcohol or ethyl acetate, for allowing object（Typically
Human body）Possess the smell of lasting and happy people.Perfume is had changed into just as having a meal, sleep, wear the clothes, make up, as you
Life, work, study, even leisure, love, an essential part, increase the color of people, lift the grade of people！
Existing perfume is mostly that the form of liquid is present, and has chemical stimulation in its composition of the perfume of sale described in the market
Material, long-term sprinkling, harm people are healthy.It is understood that now, when crossing safety check, the control to liquid is particularly severe,
Often because the capacity problem of perfume, in safety check, there is problem.
The content of the invention
To overcome above-mentioned deficiency, it is an object of the present invention to provide a kind of perfume stick, with solid as carrier, the work(of perfume is realized
Can, can have lasting, effective fragrant.
The solution of the present invention for example Xias a kind of production methods of perfume stick of ﹕, and Bao includes Bu Zhou ﹕ under Yi
A, by fresh Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa is put into the decoyl hydroximic acid solution that concentration is 12%
Row immersion, soak time was controlled at 4-5 hours；
B, taking-up Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa carry out freeze-drying in being put into freeze drier；Temperature control
At -26 DEG C, vacuum is 0.23 millibar, is kept for 15-18 hours；Then it is vacuum dried under 6-10 handkerchief vacuum states.
C, the powder that dried Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are ground into 200-300 mesh, then mix
Close；
D, mixed powder and water are passed through in distillation still by the mass ratio of 1 ﹕ 8-11 and are distilled；Temperature control at 95-98 DEG C, when
Between be 30-40min, obtain the first distillate；Extraction raffinate after distillation is carried out into second distillation, temperature control is in 116-118 DEG C, time
It is 40-50min, obtains after-fractionating liquid；
E, the first distillate, after-fractionating liquid, deodorizing alcohol, eucalyptus oil, bergamot oil, osmanthus essential oil are mixed, obtained
Mixed liquor, it is standby；
F, sponge stick is put into containing in parahydroxyacet-ophenone, the mixed solution of chitin, soaked 5-6 hours；
G, the treated sponge stick of the mixed liquor in step e, step f is put into vacuum infiltration tank carries out vacuum infiltration, time
It is 1-2 hours；
H, by step g treat sponge stick carry out microporous barrier cladding, both perfume stick.
Further, in described step a, Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa mass ratio are 0.7 ﹕ 0.2-
0.3 ﹕ 0.14-0.16 ﹕ 0.45-0.49.
Further, in described step e, the first distillate, after-fractionating liquid, deodorizing alcohol, eucalyptus oil, bergamot
Oil, osmanthus essential oil mass ratio are the ﹕ 1-1.5 ﹕ 0.12-0.14 ﹕ 0.16-0.19 ﹕ 0.25-0.29 of 0.1 ﹕ 0.08.
Further, in described step f, hydroxy acetophenone, the mixed solution of chitin, its concentration are 25%, hydroxy benzenes second
Ketone, chitin mass ratio are 1.2 ﹕ 0.7.
Further, in described step h, the perfume stick for obtaining is vacuum-packed or is fitted into closed container.
The fragrance effective ingredient of perfume of the present invention be mainly Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa, eucalyptus oil,
Bergamot oil, osmanthus essential oil, wherein again based on osmanthus essential oil.Osmanthus essential oil is calm, promote the sexual maturity, antibacterial, and to toothache, cough to be had
Curative effect, beautifying whitening skin mediates the effects such as vivotoxin and defaecation.Woman can allow skin delicate using osmanthus essential oil, delay
Aging, can also send light fragrance in vivo.Bergamot oil has happy, nice and cool, fragrant fragrance, and the sweet fruity of blue or green perfumed ribbon has clear
The fresh sense of spirit；Eucalyptus oil has the property and pleasant fragrance of quick volatilization.Essential oil obtained by the distillation of Blumea balsamifera leaf contains a left side
Revolve the composition of borneol.L-Borneol, has no toxic side effect to body, the sterilized dynamics of enhancing product, mildew resistant moistureproof, long shelf-life,
Can be used for treatment and close card coma, red eye, swell pain, larynx numbness aphtha, sore swell and ache curative are not held back after bursting, tune the five internal organs and six internal organs, dredging the channel,
Thoroughly eliminate the focus effect on channels and collaterals, and beauty or the effect for the treatment of disease.Murraya jasminorage leaf gives off a strong fragrance, and dream flower has
Nourishing the liver and kidney, improving eyesight disappears the effect of screen, and boenninghausenia sessilicarpa has clearing heat and eliminating phlegm, relieving cough and asthma effect.
Perfume aromatic flavour of the present invention, persistently, and for inspirator, the effect with preventing cough, asthma, wind wheat is same
When, the health care auxiliaring effect also with treatment dizziness, headache.
In the production method of perfume of the present invention, decoyl hydroxyl oxime is first carried out to Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa
Soaked in acid solution, its effect is to pin fragrance and effective ingredient.Then the lyophilization treatment for carrying out, it is relatively conventional
Simple drying, air-dry, can with the fragrance in significantly more efficient reservation Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa and effectively
Composition；Meanwhile, by freeze drying technology, distillation time can be substantially reduced；Distill twice, can be with more efficient, rational utilization
Raw material, it is ensured that effect is maximized.
Sponge stick of the present invention is made from the microporous sponge material of perforate, first carries out the solution of hydroxy acetophenone, chitin
Immersion, by hydroxy acetophenone, the rational proportion of chitin, after sponge stick immersion, sea is retained in by hydroxy acetophenone, chitin
In the micropore of continuous rod, coordinate vacuum infiltration, fragrance effective ingredient is more rapidly and effectively drawn on sponge stick.Invention sponge
Rod also carries out microporous barrier cladding, and volatilization is slow, and moisture-locking is persistently fragrant by micropore.
Specific embodiment
With reference to embodiment, the present invention will be further described.
The mixed solution of hydroxy acetophenone, chitin in the present invention, is by hydroxy benzenes second that mass ratio is 1.2 ﹕ 0.7
Ketone, chitin with go from water mix gained, its concentration be 25%.
Embodiment 1
A kind of production method of perfume stick, it is characterised in that Bao includes Bu Zhou ﹕ under Yi
A, fresh Blumea balsamifera leaf 2100g, Murraya jasminorage leaf 720g, dream flower 450g, boenninghausenia sessilicarpa 1380g are put into concentration is 12%
Soaked in decoyl hydroximic acid solution, soak time was controlled at 4.3 hours；
B, taking-up Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa carry out freeze-drying in being put into freeze drier；Temperature control
At -26 DEG C, vacuum is 0.23 millibar, is kept for 16 hours；Then it is vacuum dried under 8 handkerchief vacuum states.
C, the powder that dried Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are ground into 200-300 mesh, then mix
Close；
D, mixed powder and water are passed through in distillation still by the mass ratio of 1 ﹕ 9 and are distilled；At 96 DEG C, the time is temperature control
33min, obtains the first distillate；Extraction raffinate after distillation is carried out into second distillation, at 117 DEG C, the time is 42min to temperature control, is obtained
After-fractionating liquid；
E, by the first distillate 3000g, after-fractionating liquid 2400g, deodorizing alcohol 39000g, eucalyptus oil 3900g, bergamot oil
5100g, osmanthus essential oil 6600g are mixed, and obtain mixed liquor, standby；
F, sponge stick is put into the mixed solution that the concentration containing parahydroxyacet-ophenone, chitin is 25%, soaked 6 hours；Hydroxyl
Benzoylformaldoxime, chitin mass ratio are 1.2 ﹕ 0.7；
G, the treated sponge stick of the mixed liquor in step e, step f is put into vacuum infiltration tank carries out vacuum infiltration, time
It is 1.5 hours.
Embodiment 2
A, fresh Blumea balsamifera leaf 1750g, Murraya jasminorage leaf 550g, dream flower 350g, boenninghausenia sessilicarpa 1200g are put into concentration is 12%
Soaked in decoyl hydroximic acid solution, soak time was controlled at 4.6 hours；
B, taking-up Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa carry out freeze-drying in being put into freeze drier；Temperature control
At -26 DEG C, vacuum is 0.23 millibar, is kept for 17 hours；Then it is vacuum dried under 9 handkerchief vacuum states.
C, the powder that dried Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are ground into 200-300 mesh, then mix
Close；
D, mixed powder and water are passed through in distillation still by the mass ratio of 1 ﹕ 10 and are distilled；At 97 DEG C, the time is temperature control
33min, obtains the first distillate；Extraction raffinate after distillation is carried out into second distillation, at 117 DEG C, the time is 42min to temperature control, is obtained
After-fractionating liquid；
E, by the first distillate 2600g, after-fractionating liquid 2080g, deodorizing alcohol 286000g, eucalyptus oil 3120g, bergamot
Oily 4680g, osmanthus essential oil 6240g are mixed, and obtain mixed liquor, standby；
F, sponge stick is put into the mixed solution that the concentration containing parahydroxyacet-ophenone, chitin is 25%, soaked 5-6 hours；
Hydroxy acetophenone, chitin mass ratio are 1.2 ﹕ 0.7；
G, the treated sponge stick of the mixed liquor in step e, step f is put into vacuum infiltration tank carries out vacuum infiltration, time
It is 1.5 hours.
Embodiment 3
A, fresh Blumea balsamifera leaf 1960g, Murraya jasminorage leaf 728g, dream flower 448g, boenninghausenia sessilicarpa 1316g are put into concentration is 12%
Soaked in decoyl hydroximic acid solution, soak time was controlled at 4.3 hours；
B, taking-up Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa carry out freeze-drying in being put into freeze drier；Temperature control
At -26 DEG C, vacuum is 0.23 millibar, is kept for 15 hours；Then it is vacuum dried under 9 handkerchief vacuum states.
C, the powder that dried Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are ground into 200-300 mesh, then mix
Close；
D, mixed powder and water are passed through in distillation still by the mass ratio of 1 ﹕ 10 and are distilled；At 98 DEG C, the time is temperature control
34min, obtains the first distillate；Extraction raffinate after distillation is carried out into second distillation, at 116 DEG C, the time is 42min to temperature control, is obtained
After-fractionating liquid；
E, by the first distillate 2800g, after-fractionating liquid 2240g, deodorizing alcohol 39200g, eucalyptus oil 3920g, bergamot oil
4480g, osmanthus essential oil 5320g are mixed, and obtain mixed liquor, standby；；
F, sponge stick is put into containing in parahydroxyacet-ophenone, the mixed solution of chitin, soaked 5.7 hours；
G, the treated sponge stick of the mixed liquor in step e, step f is put into vacuum infiltration tank carries out vacuum infiltration, time
It is 1.8 hours.
Although detailed description being given to specific embodiment of the invention above and being illustrated, it should be noted that
We can carry out various equivalent changes and modification to above-mentioned implementation method according to conception of the invention, and the function produced by it is made
With still without departing from specification covered it is spiritual when, all should be within protection scope of the present invention.
Claims (5)
1. a kind of production method of perfume stick, it is characterised in that Bao includes Bu Zhou ﹕ under Yi
A, by fresh Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa is put into the decoyl hydroximic acid solution that concentration is 12%
Row immersion, soak time was controlled at 4-5 hours；
B, taking-up Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa carry out freeze-drying in being put into freeze drier；Temperature control
At -26 DEG C, vacuum is 0.23 millibar, is kept for 15-18 hours；Then it is vacuum dried under 6-10 handkerchief vacuum states；
C, the powder that dried Blumea balsamifera leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa are ground into 200-300 mesh, then mix；
D, mixed powder and water are passed through in distillation still by the mass ratio of 1 ﹕ 8-11 and are distilled；Temperature control at 95-98 DEG C, when
Between be 30-40min, obtain the first distillate；Extraction raffinate after distillation is carried out into second distillation, temperature control is in 116-118 DEG C, time
It is 40-50min, obtains after-fractionating liquid；
E, the first distillate, after-fractionating liquid, deodorizing alcohol, eucalyptus oil, bergamot oil, osmanthus essential oil are mixed, obtained
Mixed liquor, it is standby；
F, sponge stick is put into containing in parahydroxyacet-ophenone, the mixed solution of chitin, soaked 5-6 hours；
G, the treated sponge stick of the mixed liquor in step e, step f is put into vacuum infiltration tank carries out vacuum infiltration, time
It is 1-2 hours；
H, by step g treat sponge stick carry out microporous barrier cladding, both perfume stick.
2. the production method of a kind of perfume stick according to claim 1, it is characterised in that in described step a, Blumea balsamifera
Leaf, Murraya jasminorage leaf, dream flower, boenninghausenia sessilicarpa mass ratio are 0.7 ﹕ 0.2-0.3 ﹕ 0.14-0.16 ﹕ 0.45-0.49.
3. the production method of a kind of perfume stick according to claim 1, it is characterised in that in described step e, first steams
Distillate, after-fractionating liquid, deodorizing alcohol, eucalyptus oil, bergamot oil, osmanthus essential oil mass ratio are the ﹕ 1-1.5 ﹕ of 0.1 ﹕ 0.08
0.12-0.14 ﹕ 0.16-0.19 ﹕ 0.25-0.29.
4. the production method of a kind of perfume stick according to claim 1, it is characterised in that in described step f, hydroxy benzenes
The mixed solution of ethyl ketone, chitin, its concentration is 25%, and hydroxy acetophenone, chitin mass ratio are 1.2 ﹕ 0.7.
5. the production method of a kind of perfume stick according to claim 1, it is characterised in that in described step h, obtain
Perfume stick is vacuum-packed or is fitted into closed container.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710205326.1A CN106913484A (en) | 2017-03-31 | 2017-03-31 | A kind of production method of perfume stick |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710205326.1A CN106913484A (en) | 2017-03-31 | 2017-03-31 | A kind of production method of perfume stick |
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| Publication Number | Publication Date |
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| CN106913484A true CN106913484A (en) | 2017-07-04 |
Family
ID=59460766
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| Application Number | Title | Priority Date | Filing Date |
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| CN201710205326.1A Withdrawn CN106913484A (en) | 2017-03-31 | 2017-03-31 | A kind of production method of perfume stick |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108432830A (en) * | 2018-05-10 | 2018-08-24 | 福建然晟生物科技有限公司 | A kind of production method of super long effective mosquito repellent fly pellet |
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|---|---|---|---|---|
| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN102028646A (en) * | 2010-11-23 | 2011-04-27 | 陕西师范大学 | Thyme perfume |
| CN102232918A (en) * | 2011-04-22 | 2011-11-09 | 珠海尚尔生物科技有限公司 | Antibiotic perfume |
| CN202113481U (en) * | 2011-04-07 | 2012-01-18 | 梁秀奎 | Double-functional portable using device for essential oil |
| CN102406575A (en) * | 2011-11-21 | 2012-04-11 | 江西金乔园林有限公司 | Sweet osmanthus perfume |
| CN103830151A (en) * | 2014-03-25 | 2014-06-04 | 贵州利生香中药科技有限公司 | Application of blumea balsamifera oil in daily chemical product |
| CN104638442A (en) * | 2013-11-11 | 2015-05-20 | 陕西恒发电子科技有限公司 | Socket type power surge protector with aromatherapy function and cleaning brush |
| CN106074221A (en) * | 2016-06-24 | 2016-11-09 | 广西华香道生物科技有限公司 | One takes care of health fragrance liquid |
-
2017
- 2017-03-31 CN CN201710205326.1A patent/CN106913484A/en not_active Withdrawn
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| CN101961300A (en) * | 2010-09-29 | 2011-02-02 | 重庆市超临界精细化工生产力促进中心有限公司 | Perfume composition containing pepper aroma essential oil and preparation method thereof |
| CN102028646A (en) * | 2010-11-23 | 2011-04-27 | 陕西师范大学 | Thyme perfume |
| CN202113481U (en) * | 2011-04-07 | 2012-01-18 | 梁秀奎 | Double-functional portable using device for essential oil |
| CN102232918A (en) * | 2011-04-22 | 2011-11-09 | 珠海尚尔生物科技有限公司 | Antibiotic perfume |
| CN102406575A (en) * | 2011-11-21 | 2012-04-11 | 江西金乔园林有限公司 | Sweet osmanthus perfume |
| CN104638442A (en) * | 2013-11-11 | 2015-05-20 | 陕西恒发电子科技有限公司 | Socket type power surge protector with aromatherapy function and cleaning brush |
| CN103830151A (en) * | 2014-03-25 | 2014-06-04 | 贵州利生香中药科技有限公司 | Application of blumea balsamifera oil in daily chemical product |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108432830A (en) * | 2018-05-10 | 2018-08-24 | 福建然晟生物科技有限公司 | A kind of production method of super long effective mosquito repellent fly pellet |
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