CN106908708B - A kind of gallium nitride based light emitting diode analysis method for reliability based on electroluminescent focus statistics - Google Patents

A kind of gallium nitride based light emitting diode analysis method for reliability based on electroluminescent focus statistics Download PDF

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CN106908708B
CN106908708B CN201710130645.0A CN201710130645A CN106908708B CN 106908708 B CN106908708 B CN 106908708B CN 201710130645 A CN201710130645 A CN 201710130645A CN 106908708 B CN106908708 B CN 106908708B
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light emitting
emitting diode
electroluminescent
gallium nitride
component
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CN106908708A (en
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赵琳娜
闫大为
顾晓峰
陈雷雷
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Jiangnan University
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Jiangnan University
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R31/00Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
    • G01R31/26Testing of individual semiconductor devices
    • G01R31/2601Apparatus or methods therefor
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01RMEASURING ELECTRIC VARIABLES; MEASURING MAGNETIC VARIABLES
    • G01R31/00Arrangements for testing electric properties; Arrangements for locating electric faults; Arrangements for electrical testing characterised by what is being tested not provided for elsewhere
    • G01R31/26Testing of individual semiconductor devices
    • G01R31/2642Testing semiconductor operation lifetime or reliability, e.g. by accelerated life tests

Abstract

The invention discloses a kind of gallium nitride based light emitting diode analysis method for reliability based on electroluminescent focus statistics.This method passes through stepstress test or reverse scan current -voltage curve first, the reverse leakage current degenerative process at any time for analyzing gallium nitride based light emitting diode, choose reverse leakage current is in the voltage of apparent ascendant trend as fixed-bias transistor circuit when acquiring component electroluminescent hot spot at any time;Then by low-light microscopic system, the image of an electroluminescent hot spot is acquired at regular intervals;Finally by electroluminescent hot spot number is accumulated in statistics light emitting diode component degenerative process, the Weibull distribution curve of hot spot generation time is drawn, to analyze reliability and the service life of light emitting diode component.The present invention realizes the fail-safe analysis to gallium nitride based light emitting diode component, than existing methods compared to advantages such as quick, low costs using a kind of simple operable method.

Description

A kind of gallium nitride based light emitting diode reliability based on electroluminescent focus statistics point Analysis method
Technical field
The present invention relates to gallium nitride based light emitting diode reliability analysis technology fields, more particularly to one kind to be based on electroluminescent hair The gallium nitride based light emitting diode analysis method for reliability of light focus statistics.
Background technique
Recently as the continuous maturation of iii-v based luminescent material technology, light emitting diode is widely used in colored aobvious Show, the storage of indicator light, data, medical treatment and the fields such as traffic lights, especially because the fast development of gallium nitride based light emitting diode, Global semiconductor has been developed into true color that gallium nitride is basic light emitting diode and white light emitting diode product Illuminate the hot spot of development & production.
The most important advantage of light emitting diode is the longer life expectancy relative to other light sources such as incandescent lamp bulb, and reliability is more It is high.But this characteristic depends on many manufacture factors.With regard to currently used using sapphire as the gallium nitride serial emission two of substrate Pole pipe product, Sapphire Substrate and epitaxial layer of gallium nitride lattice mismatch are 13%, thermal mismatching 34%, therefore there are serious such as position The problems such as dislocation density is big, defect is more, crystal quality is poor.The stability of long-time service to light emitting diode all is caused to cause by these The influence of life.Currently, light emitting diode component reliability analysis method is the mistake based on a large amount of light emitting diode component Effect statistics, this method have two: 1. at high cost, it is contemplated that the accuracy of failure statistics model is needed using a large amount of Light emitting diode component carry out failure analysis;2. the time is long, failure analysis is based on component in forward bias or reversed The research of soft breakdown characteristic under bias condition generally requires hundreds of to differ to tens of thousands of a hours.
The purpose of the present invention is to the deficiencies in the prior art, provide a kind of new quick, inexpensive luminous two The analysis method for reliability of pole pipe component.
Summary of the invention
In view of the shortcomings of the prior art, the purpose of the present invention is intended to provide a kind of new quick, inexpensive shine Diode component reliability analysis method.This method carries out applying fixed reverse bias to the light emitting diode component of preparation The electricity degradation testing of voltage counts the number of electroluminescent hot spot in degenerative process by electroluminescent imaging system, draws The distribution curve of hot spot generation time.Pass through the initial failure of Weibull distribution model analysis light emitting diode component, accidentally mistake The reliability of effect and loss failure three phases.
The present invention is achieved through the following technical solutions:
1. analyzing the degenerative process of the reverse leakage current of gallium nitride based light emitting diode at any time.To light emitting diode member device Part carries out stepstress test, and at normal temperature, test voltage is stepped up since lesser reverse bias voltage, Mei Ge electricity Compression continues for some time, until there is soft breakdown phenomenon.
2. capturing the image of electroluminescent hot spot in light emitting diode component degenerative process by low-light microscopic system.Tool Body method is, in gallium nitride based light emitting diode degenerative process, chooses leakage current with stress time in the trend that rises appreciably Fixed-bias transistor circuit when bias voltage is as acquisition electroluminescent hot spot image.Light emitting diode component to be measured is placed on probe On platform, fixed reverse biased is applied to the component by source table.One is captured at regular intervals by low-light microscopic system The picture of electroluminescent hot spot in light emitting diode component degenerative process.
3. counting electroluminescent hot spot number.By a gallium nitride based light emitting diode component be equivalent to multiple areas compared with The parallel connection of small component, the lesser component of the area of each corresponding failure of the electroluminescent hotspot location, The number for confirming the electroluminescent hotspot location is the number of electroluminescent hot spot.Light emitting diode component is applying fixation Reverse biased during, the cumulative amount of leakage current and the electroluminescent hot spot during stress approximately linearly increases.Cause This, the electroluminescent hot spot number that the failure likelihood dependent on the time of the component can continuously occur by number replaces Out-of-service time by recording a large amount of sample carries out fail-safe analysis.This method is advantageous in that without considering differences between samples pair Analyze the influence of result.
4. analyzed by the Weibull distribution of the hot spot generation time initial failure of light emitting diode component, accidentally The reliability of failure and loss failure three phases.Accident analysis for component reliability, weber (Weibull) distributed mode Type is the most commonly used.Corresponding cumulative distribution function is F (t)=1-exp [- (τ B/ η) β], and wherein η represents out-of-service time characteristic Scale parameter, β are a weber slope (or form parameters), indicate that failure rate changes with time.It is applied by counting with reversal of stress The electroluminescent hot spot number occurred is accumulated between added-time, the Weibull distribution curve of the component is drawn, to analyze component Reliability.
Detailed description of the invention
Fig. 1 is the gallium nitride based light emitting diode analysis method for reliability flow chart based on electroluminescent focus statistics;
Fig. 2 is reverse leakage current evolution process figure of gallium nitride based light emitting diode during stepstress;
Fig. 3 is low-light microscopic system;Respectively label respectively represents in figure: the highly sensitive camera lens Charged Couple component of 1-, 2- microscope, 3- are tested gallium nitride based light emitting diode, the source 4- table
Fig. 4 is the spatial distribution map of electroluminescent hot spot in degenerative process;
Fig. 5 is when backward voltage is -28V, and electroluminescent hot spot accumulates the relation curve of number and pull-down current;
Fig. 6 is the Weibull distribution curve of gallium nitride based light emitting diode.
Specific embodiment
Further description of the technical solution of the present invention with reference to the accompanying drawings and examples.
To make the objectives, technical solutions, and advantages of the present invention clearer, below in conjunction with specific embodiment, and reference Attached drawing, the present invention is described in more detail.
The present invention provides one kind by electroluminescent imaging system, counts in gallium nitride based light emitting diode degenerative process The accumulation number of electroluminescent hot spot draws the distribution curve of hot spot generation time, and is shone by Weibull distribution model analysis The method of the reliability of the initial failure of diode component, random failure and loss failure three phases.It specifically includes following Step, as shown in Figure 1:
Step 1: analyzing the degenerative process of the reverse leakage current of gallium nitride based light emitting diode at any time.At normal temperature, right The gallium nitride based light emitting diode component of preparation carries out stepstress test.
Specific test method is to apply reverse biased to component using source table, and since -5V, step-length is -5V, until There is soft breakdown phenomenon in component.From figure 2 it can be seen that reverse leakage current is at any time when reverse biased is more than -25V Apparent ascendant trend, the breakdown voltage of component are -40V.Therefore, when acquiring the image of electroluminescent hot spot, selection Reversed fixed-bias transistor circuit range should be between -25V to -40V.The present embodiment is using -28V voltage.
Step 2: the figure of electroluminescent hot spot in light emitting diode component degenerative process is captured by low-light microscopic system Picture.
The low-light microscopic system is a kind of analysis system that defect and failure are positioned using semiconductor light emitting phenomenon, such as Shown in Fig. 3, including the highly sensitive camera lens Charged Couple component of 1-, 2- microscope, 3- are tested gallium nitride based light emitting diode, the source 4- Table.Fixed reverse biased is applied to tested gallium nitride based light emitting diode component by source table, is existed when in tested component When electric leakage and hot carrier's effect, photon transmitting is had from failpoint.It can get tested first device by traditional optical microscopy The reflected image of part, in addition, photon will enter image intensifier from tested component.Image intensifier can amplify faint light Signal, then vision signal is converted the signal into Charged Couple component (CCD), illuminated diagram is obtained by Computer Image Processing Picture.Luminescent image is overlapped with reflected image, realizes the positioning to defect or failpoint.
Specific test method is by gallium nitride based light emitting diode component application -28V reverse biased.It is micro- using low-light System, when the every increase -0.05mA of reverse leakage current acquires the image of an electroluminescent hot spot.Fig. 4, which is shown, works as reverse leakage Stream is respectively -1.05mA, -1.75mA, -2.5mA, and when stress application time is respectively 800s, 3500s, 10620s acquires The image of electroluminescent hot spot.In Fig. 4, the area of light emitting diode component is 300um × 300um, the lower left corner of component It is respectively positive and negative electrode with the upper right corner, centre is transparent electrode, and white point is the electroluminescent of low-light microscopic system acquisition Hot spot.As can be seen that as time increases, electroluminescent hot spot quantity also gradually increases under fixed reverse biased.
Step 3: statistics electroluminescent hot spot number.
Specific method is to analyze the electroluminescent hair acquired in light emitting diode component degenerative process by low-light microscopic system Photo-thermal point image.One gallium nitride based light emitting diode component is equivalent to the parallel connection of the lesser component of multiple areas, often The lesser component of the area of a corresponding failure of the electroluminescent hotspot location, confirms the electroluminescent hot spot The number of position is the number of electroluminescent hot spot.It is found by statistics, light emitting diode component is applying the reversed of fixation In bias voltages, the cumulative amount of reverse leakage current and the electroluminescent hot spot during stress approximately linearly increases, statistics knot Fruit is as shown in Figure 5.Therefore, the electroluminescent that the failure likelihood dependent on the time of the component can continuously occur by number Hot spot number, so that the out-of-service time by recording a large amount of sample be replaced to carry out fail-safe analysis.
Step 4: the analysis of light emitting diode component reliability.
Weber (Weibull) distribution is the most frequently used theoretical model of fail-safe analysis and longevity test.From probability theory and system From the perspective of meter is learned, Weibull distribution is successional probability distribution, and cumulative distribution function is F (t)=1-exp [- (τ B/ η) β], wherein η is the scale parameter for representing out-of-service time characteristic, and β is a weber slope (or form parameter).β < 1 indicate failure rate with Time reduces, that is, deposits type failure in the early stage, or is infancy failure;β=1 indicate failure rate be at any time it is constant, this Show that random external event is causing to fail, referred to as accidental type failure;β > 1 indicates failure rate increase with time, often has During " aging ", referred to as loss-type failure.
The present embodiment delineates the generation of component hot spot by counting the relationship of out-of-service time and hot spot cumulative amount The distribution curve of time, as shown in Figure 6.From fig. 6, it can be seen that the out-of-service time of electroluminescent hot spot obeys Weibull distribution.It is logical It crosses and data is fitted, the β value of extraction is about 0.67 and 4.09, as infancy and loss-type failure.Infancy failure is lost Effect is related with external factor, such as manufacturing defect;And in the loss phase, generation of failing derives from internal factor, pre- such as active layer The defect pre-existed.The service life of light emitting diode component can be estimated by Weibull distribution curve.
The present invention counts electroluminescent heat in gallium nitride based light emitting diode degenerative process by electroluminescent imaging system The accumulation number of point analyzes the reliable and expected life of component by Weibull distribution.It was degenerating due to only counting component The accumulation number of electroluminescent hot spot in journey, component without breakdown, therefore compare with existing method required annealing time compared with It is short;In addition, compared to it is existing by record a large amount of sample out-of-service time carry out reliability analysis method, this method it is good Be in it is low in testing cost, and without consider differences between samples to analysis result influence.
Finally, it is stated that the above examples are only used to illustrate the technical scheme of the present invention and are not limiting, although referring to compared with Good embodiment describes the invention in detail, those skilled in the art should understand that, it can be to skill of the invention Art scheme is modified or replaced equivalently, and without departing from the objective and range of technical solution of the present invention, should all be covered at this In the scope of the claims of invention.

Claims (3)

1. a kind of gallium nitride based light emitting diode analysis method for reliability based on electroluminescent focus statistics, it is characterised in that: This method comprises:
Analyze the degenerative process of the reverse leakage current of gallium nitride based light emitting diode at any time;
By low-light microscopic system, a light emitting diode component is captured in the degenerative process every preset time The picture of electroluminescent hot spot analyzes the picture of the electroluminescent hot spot, by a gallium nitride based light emitting diode component It is equivalent to the parallel connection of the lesser component of multiple areas, the face of each corresponding failure of the electroluminescent hotspot location The lesser component of product confirms that the number of the electroluminescent hotspot location is the number of electroluminescent hot spot;
According to the number of the electroluminescent hot spot, it is based on Weibull distribution model, draws out-of-service time and hot spot cumulative amount Relation curve determines scale parameter and shape parameter values in Weibull distribution, and according to parameter value analysis described luminous two The reliability of pole pipe component and service life.
2. the gallium nitride based light emitting diode fail-safe analysis side according to claim 1 based on electroluminescent focus statistics Method, which is characterized in that analyze the degenerative process of the reverse leakage current of gallium nitride based light emitting diode at any time, comprising:
Choose reverse leakage current is in the bias voltage that rises appreciably as fixation when acquiring electroluminescent hot picture at any time Bias.
3. the gallium nitride based light emitting diode fail-safe analysis side according to claim 1 based on electroluminescent focus statistics Method, which is characterized in that stepstress test is carried out to the gallium nitride based light emitting diode component, comprising:
Component is biased, since lesser reverse biased, reasonable step-length is set, until soft breakdown occurs in component Phenomenon.
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CN107576895B (en) * 2017-08-29 2020-02-21 上海华力微电子有限公司 In-situ hot spot detection method suitable for TDDB
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CN113203929B (en) * 2021-04-23 2022-11-11 香港科技大学深圳研究院 Method for testing reliability of back bias voltage of gallium nitride power device
CN113406484B (en) * 2021-08-19 2021-11-09 华芯半导体研究院(北京)有限公司 Device and method for failure analysis of chip
CN117269712B (en) * 2023-11-22 2024-01-30 墨研计算科学(南京)有限公司 Method, device, equipment and medium for predicting hot carrier injection life of transistor

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