CN106904995A - One kind can damping ceramic tile and preparation method thereof - Google Patents
One kind can damping ceramic tile and preparation method thereof Download PDFInfo
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Abstract
The invention discloses one kind can damping ceramic tile and preparation method thereof, be related to ceramic field；It is described can the making raw material of damping ceramic tile be：Diatomite, kaolin, clay, zeolite, quartz sand, vermiculite, guar bean flour, sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide；The present invention optimizes improvement by raw material and preparation method, obtained ceramic tile is had preferable moisture absorption and desorption property and rupture strength, and after testing, ceramic tile wet volume capacity of the present invention is up to 750.33 768.15g/m2, moisture releasing amount is 489.21 504.13g/m2, rupture strength is 40.19 42.01MPa, and the porosity is 40.97 46.87%.
Description
【Technical field】
The present invention relates to ceramic field, and in particular to one kind can damping ceramic tile and preparation method thereof.
【Background technology】
Indoor air humidity has a great impact to person health, article preservation and device longevity etc., in regulation room
Air humidity is significant, therefore damping ceramic tile arises at the historic moment.Damping ceramic tile species on current market is various, mainly with diatom
The materials such as soil, zeolite, activated carbon, activated alumina are reached as main absorbent using the moisture absorption and desorption property of natural mineral matter
The purpose of moisture in regulation room, there is certain effect, but most of damping capacity is small, and hygroscopicity is poor, and part hygroscopicity is preferable, but
Only focus on the porosity in ceramic tile and ignore rupture strength, cause obtained ceramic tile rupture strength poor.
【The content of the invention】
Regarding to the issue above, the technical problem to be solved in the present invention be to provide one kind can damping ceramic tile and preparation method thereof,
Obtained ceramic tile of the invention has the features such as porosity is high, wet volume capacity is big, moisture releasing amount performance is good, rupture strength is big.
In order to solve the above technical problems, the technical solution adopted by the present invention is as follows：
One kind can damping ceramic tile, be prepared from the following raw materials in parts by weight：Diatomite 30-40 parts, kaolin 20-25 parts,
Clay 19-23 parts, zeolite 15-19 parts, quartz sand 10-14 parts, vermiculite 11-16 parts, guar bean flour 8-14 parts, carboxymethylcellulose calcium
Sodium 5-9 parts, calcium chloride 1-4 parts, ammonium hydrogen carbonate 5-8 parts, magnesia 0.8-1.5 parts and aluminum oxide 0.3-0.7 parts.
Preferably, one kind can damping ceramic tile, be prepared from the following raw materials in parts by weight：35 parts of diatomite, 22 parts of kaolin,
21 parts of clay, 17 parts of zeolite, 12 parts of quartz sand, 14 parts of vermiculite, 11 parts of guar bean flour, 7 parts of sodium carboxymethylcellulose, calcium chloride 3
Part, 6 parts of ammonium hydrogen carbonate, 1 part of magnesia and 0.5 part of aluminum oxide.
Further, the loss on ignition of the kaolin and clay is 9-15wt%.
According to above-mentioned formula, the present invention also provide it is above-mentioned it is a kind of can damping ceramic tile preparation method, comprise the following steps：
(1) each raw material is weighed by above-mentioned weight portion；
(2) diatomite, kaolin, clay, zeolite, quartz sand and vermiculite are crushed, crosses 80-90 mesh sieves, obtain powder；
(3) sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide are mixed with above-mentioned powder, is obtained
Compound, by compound and the water of the 65-68% of the compound weight, the ethanol solution one of the compound weight 5-9%
In with addition wet ball mill, ground 35-40 minutes in the case where rotating speed is 10-12r/min, slurry is obtained, by slurry in 150-180
After being dried 30-60 minutes at DEG C, 90-110 mesh sieves are crossed in crushing, obtain fine powder raw material；
(4) base is mixed and made into the water that guar bean flour, above-mentioned fine powder raw material are added the fine powder raw material weight 40-60%
Material, base substrate is pressed into by blank, and pressing pressure is 4500-4800kN, by base substrate after drying 50-60 minutes at 180-200 DEG C,
Fired 50-70 minutes at being 1100-1300 DEG C in temperature, and be incubated 30-40 minutes, you can obtain the ceramic tile.
Enter a ground, the volume fraction of ethanol solution described in step (3) is 50-70%.
Enter a ground, the temperature of water described in step (3) is 65-70 DEG C.
Diatomite and zeolite are natural porous material in the present invention；Vermiculite can expand under high temperature action；Quartz sand is hard,
Wear-resisting, stable chemical performance；Kaolin and clay plasticity are good, easy-formation；These materials are the base stocks of ceramic tile of the present invention,
The moisture pick-up properties itself having.
Sodium carboxymethylcellulose can effectively improve the plasticity of ceramic tile raw material as the incorporation of additive in the present invention, reduce
Slurry viscosity, increases the dry tenacity of base substrate, reduces the process time of base substrate, while, moreover it is possible to increase the water absorption rate of firing sample
And the porosity, increase hygroscopicity.
The addition of calcium chloride can be evenly dispersed into brick body surface, in the present invention for improving ceramic tile moisture releasing performance.
Ammonium hydrogen carbonate is pore creating material, and being heated can release carbon dioxide and ammonia, and gas overflows generation hole knot from material
Structure, in the present invention for increasing pore quantity, further improves moisture pick-up properties.
Magnesia and aluminum oxide are respectively provided with the thermal coefficient of expansion higher than other glass phases of the invention, for improving the anti-of ceramic tile
Folding intensity.
Guar bean flour has preferably water-soluble and very high viscosity, in the present invention both as binding agent, and as pore-forming
Agent, certain space is occupied after guar bean flour and other raw material mixed-formings, is burned off after burning till, and forms more spaces, is entered
One step increased the porosity of prepared ceramic tile.
Compared with prior art, the present invention has the advantages that：
The present invention optimizes improvement by raw material and preparation method, obtained ceramic tile is had preferable absorb-discharge humid
Energy and rupture strength, after testing, ceramic tile wet volume capacity of the present invention reaches 750.33-768.15g/m2, moisture releasing amount is 489.21-
504.13g/m2, rupture strength is 40.19-42.01MPa, and the porosity is 40.97-46.87%.Wherein, diatomite, zeolite, leech
Stone and ammonium hydrogen carbonate are together calcined, and increased the quantity of stomata, occupy certain after guar bean flour and other raw material mixed-formings
Space, is burned off after burning till, and forms more spaces, and the porosity of prepared ceramic tile is further increased；Quartz sand, magnesia
Together being calcined with aluminum oxide can effectively improve the rupture strength of ceramic tile, make obtained ceramic tile good toughness, wear-resisting, chemical property steady
It is fixed, it is to avoid the problem of rupture strength difference caused by the porosity is high；The addition of calcium chloride can be evenly dispersed into brick body surface, enter one
Step improves ceramic tile moisture releasing performance；Kaolin, clay, sodium carboxymethylcellulose and guar bean flour are used cooperatively and strengthen ceramic tile slurry
Viscosity, plastotype is good, and dry tenacity is big, and rate of drying is fast, reduces the process time of base substrate, improves blank strength, reduces base substrate
Damage amount, further increases the quality of base substrate；Additionally, when making when also strict control Ball-milling Time, firing temperature and insulation
Between wait technological parameter, make sintering effect more preferably.
【Specific embodiment】
Specific embodiment of the invention is described further with reference to embodiments.
Embodiment 1
The present embodiment one kind can damping ceramic tile, be prepared from the following raw materials in parts by weight：30 parts of diatomite, kaolin 20
Part, 19 parts of clay, 15 parts of zeolite, 10 parts of quartz sand, 11 parts of vermiculite, 8 parts of guar bean flour, 5 parts of sodium carboxymethylcellulose, calcium chloride
0.3 part of 1 part, 5 parts of ammonium hydrogen carbonate, 0.8 part of magnesia and aluminum oxide.The loss on ignition of above-mentioned kaolin and clay is 9wt%.
The present embodiment it is a kind of can damping ceramic tile preparation method, comprise the following steps：
(1) each raw material is weighed by above-mentioned weight portion；
(2) diatomite, kaolin, clay, zeolite, quartz sand and vermiculite are crushed, crosses 80 mesh sieves, obtain powder；
(3) sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide are mixed with above-mentioned powder, is obtained
Compound, water, the volume fraction of the compound weight 5% by compound with 65 DEG C of the 65% of the compound weight are
50% ethanol solution is together added in wet ball mill, is ground 35 minutes in the case where rotating speed is 10r/min, obtains slurry, will be starched
Expect that after being dried 60 minutes at 150 DEG C 90 mesh sieves are crossed in crushing, obtain fine powder raw material；
(4) blank is mixed and made into the water that guar bean flour, above-mentioned fine powder raw material are added the fine powder raw material weight 40%,
Blank is pressed into base substrate, pressing pressure is 4500kN, is 1100 DEG C in temperature by base substrate after being dried 60 minutes at 180 DEG C
It is lower to fire 70 minutes, and it is incubated 30 minutes, you can obtain the ceramic tile.
Embodiment 2
The present embodiment one kind can damping ceramic tile, be prepared from the following raw materials in parts by weight：40 parts of diatomite, kaolin 25
Part, 23 parts of clay, 19 parts of zeolite, 14 parts of quartz sand, 16 parts of vermiculite, 14 parts of guar bean flour, 9 parts of sodium carboxymethylcellulose, chlorination
0.7 part of 4 parts of calcium, 8 parts of ammonium hydrogen carbonate, 1.5 parts of magnesia and aluminum oxide.The loss on ignition of above-mentioned kaolin and clay is
15wt%.
The present embodiment it is a kind of can damping ceramic tile preparation method, comprise the following steps：
(1) each raw material is weighed by above-mentioned weight portion；
(2) diatomite, kaolin, clay, zeolite, quartz sand and vermiculite are crushed, crosses 90 mesh sieves, obtain powder；
(3) sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide are mixed with above-mentioned powder, is obtained
Compound, water, the volume fraction of the compound weight 9% by compound with 70 DEG C of the 68% of the compound weight are
70% ethanol solution is together added in wet ball mill, is ground 40 minutes in the case where rotating speed is 12r/min, obtains slurry, will be starched
Expect that after being dried 30 minutes at 180 DEG C 110 mesh sieves are crossed in crushing, obtain fine powder raw material；
(4) blank is mixed and made into the water that guar bean flour, above-mentioned fine powder raw material are added the fine powder raw material weight 60%,
Blank is pressed into base substrate, pressing pressure is 4800kN, is 1300 DEG C in temperature by base substrate after being dried 50 minutes at 200 DEG C
It is lower to fire 50 minutes, and it is incubated 40 minutes, you can obtain the ceramic tile.
Embodiment 3
The present embodiment one kind can damping ceramic tile, be prepared from the following raw materials in parts by weight：35 parts of diatomite, kaolin 22
Part, 21 parts of clay, 17 parts of zeolite, 12 parts of quartz sand, 14 parts of vermiculite, 11 parts of guar bean flour, 7 parts of sodium carboxymethylcellulose, chlorination
0.5 part of 3 parts of calcium, 6 parts of ammonium hydrogen carbonate, 1 part of magnesia and aluminum oxide.The loss on ignition of above-mentioned kaolin and clay is 12wt%.
The present embodiment it is a kind of can damping ceramic tile preparation method, comprise the following steps：
(1) each raw material is weighed by above-mentioned weight portion；
(2) diatomite, kaolin, clay, zeolite, quartz sand and vermiculite are crushed, crosses 85 mesh sieves, obtain powder；
(3) sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide are mixed with above-mentioned powder, is obtained
Compound, water, the volume fraction of the compound weight 7% by compound with 68 DEG C of the 66% of the compound weight are
59% ethanol solution is together added in wet ball mill, is ground 38 minutes in the case where rotating speed is 11r/min, obtains slurry, will be starched
Expect that after being dried 45 minutes at 160 DEG C 100 mesh sieves are crossed in crushing, obtain fine powder raw material；
(4) blank is mixed and made into the water that guar bean flour, above-mentioned fine powder raw material are added the fine powder raw material weight 50%,
Blank is pressed into base substrate, pressing pressure is 4600kN, is 1200 DEG C in temperature by base substrate after being dried 55 minutes at 190 DEG C
It is lower to fire 60 minutes, and it is incubated 35 minutes, you can obtain the ceramic tile.
Ceramic tile performance evaluation of the present invention：
In order to illustrate moisture absorption and the compressive property of ceramic tile of the present invention, applicant has done comparative testing below：Experiment is divided into
Be divided into the 1st group, the 2nd group, the 3rd group, control group 1, control group 2, totally 6 groups of control group 3, wherein, the 1st group uses embodiment 1
Formula and preparation method make ceramic tile；The 2nd group of formula and preparation method using embodiment 2 makes ceramic tile；3rd group using real
The formula and preparation method for applying example 3 make ceramic tile；Control group 1 is made using the preparation method of embodiment 3, but is not contained in formula
The material composition of guar bean flour；Control group 2 is made using the preparation method of embodiment 3, but the original of calcium chloride is not contained in formula
Material composition；Control group 3 is made using the preparation method of embodiment 3, but do not contained in formula the raw material of magnesia and aluminum oxide into
Point.Ceramic tile obtained in each group is carried out into the performance detections such as wet volume capacity, moisture releasing amount, the porosity and rupture strength after sintering, detection is equal
Carried out under identical environmental condition, wherein, rupture strength is measured by the electronic anti-folding instrument of KZY-300-1 types；The porosity
Using Archimedes method, measured by medium of kerosene；Wet volume capacity and moisture releasing amount in strict accordance with《Construction material absorb-discharge humid
Can method of testing》Professional standard is measured.Testing result is as shown in table 1：
The ceramic tile properties testing result of table 1
By 1 group, the 2nd group, the 3rd group of data, ceramic tile wet volume capacity of the present invention reaches 750.33-768.15g/m2, puts
Moisture is 489.21-504.13g/m2, and rupture strength is 40.19-42.01MPa, and the porosity is 40.97-46.87%；By
The contrast of 3 groups and control group 1 understands that guar bean flour can further increase the porosity of prepared ceramic tile in raw material of the present invention；It is logical
Cross the 3rd group and control group 2 contrast understand raw material of the present invention in calcium chloride can further improve ceramic tile moisture releasing performance；By the 3rd
The contrast of group and control group 3 understand magnesia and aluminum oxide in raw material of the present invention together calcine can effectively improve ceramic tile anti-folding it is strong
Degree.
Described above is directed to the detailed description of preferably possible embodiments of the invention, but embodiment is not limited to this hair
Bright patent claim, the equal change completed under the technical spirit suggested by all present invention or modification change, all should belong to
Cover the scope of the claims in the present invention.
Claims (6)
1. one kind can damping ceramic tile, it is characterised in that：It is prepared from the following raw materials in parts by weight：Diatomite 30-40 parts, kaolin
20-25 parts, clay 19-23 parts, zeolite 15-19 parts, quartz sand 10-14 parts, vermiculite 11-16 parts, guar bean flour 8-14 parts, carboxylic first
5-9 parts, calcium chloride 1-4 parts, ammonium hydrogen carbonate 5-8 parts, magnesia 0.8-1.5 parts and aluminum oxide 0.3-0.7 parts of base sodium cellulosate.
2. one kind according to claim 1 can damping ceramic tile, it is characterised in that：It is prepared from the following raw materials in parts by weight：
35 parts of diatomite, 22 parts of kaolin, 21 parts of clay, 17 parts of zeolite, 12 parts of quartz sand, 14 parts of vermiculite, 11 parts of guar bean flour, carboxylic first
0.5 part of 7 parts of base sodium cellulosate, 3 parts of calcium chloride, 6 parts of ammonium hydrogen carbonate, 1 part of magnesia and aluminum oxide.
3. one kind according to claim 1 and 2 can damping ceramic tile, it is characterised in that：The burning of the kaolin and clay is lost
Amount is 9-15wt%.
4. it is a kind of it is according to claim 1 and 2 can damping ceramic tile preparation method, it is characterised in that：Comprise the following steps：
(1) each raw material is weighed by above-mentioned weight portion；
(2) diatomite, kaolin, clay, zeolite, quartz sand and vermiculite are crushed, crosses 80-90 mesh sieves, obtain powder；
(3) sodium carboxymethylcellulose, calcium chloride, ammonium hydrogen carbonate, magnesia and aluminum oxide are mixed with above-mentioned powder, is mixed
Material, compound is together added with the water of the 65-68% of the compound weight, the ethanol solution of the compound weight 5-9%
Enter in wet ball mill, ground 35-40 minutes in the case where rotating speed is 10-12r/min, slurry is obtained, by slurry at 150-180 DEG C
After drying 30-60 minutes, 90-110 mesh sieves are crossed in crushing, obtain fine powder raw material；
(4) blank is mixed and made into the water that guar bean flour, above-mentioned fine powder raw material are added the fine powder raw material weight 40-60%,
Blank is pressed into base substrate, pressing pressure is 4500-4800kN, by base substrate after drying 50-60 minutes at 180-200 DEG C,
Temperature is incubated 30-40 minutes to be fired 50-70 minutes at 1100-1300 DEG C, you can obtain the ceramic tile.
5. it is according to claim 4 it is a kind of can damping ceramic tile preparation method, it is characterised in that：Second described in step (3)
The volume fraction of alcoholic solution is 50-70%.
6. it is according to claim 4 it is a kind of can damping ceramic tile preparation method, it is characterised in that：Water described in step (3)
Temperature be 65-70 DEG C.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109956676A (en) * | 2017-12-26 | 2019-07-02 | 淡江大学 | To incinerate the damping ceramics and its manufacturing method that react ash manufacture |
| CN110028334A (en) * | 2019-03-20 | 2019-07-19 | 广西大学 | A kind of ecology damping brick and preparation method thereof |
| CN111995362A (en) * | 2020-08-13 | 2020-11-27 | 福建省德化县零度创意有限公司 | Water-permeable and air-permeable microporous ceramic flowerpot and preparation process thereof |
| CN112521017A (en) * | 2021-01-13 | 2021-03-19 | 常州市武进人民医院 | Bioactive porous material and preparation method thereof |
| CN112830765A (en) * | 2021-03-03 | 2021-05-25 | 德化县嘉祥陶瓷有限公司 | Red pottery moisturizing device for brown sugar storage and manufacturing method thereof |
| CN109437845B (en) * | 2018-12-25 | 2021-06-01 | 佛山科学技术学院 | Antiskid wear-resistant ceramic and preparation method thereof |
| CN113563050A (en) * | 2021-07-29 | 2021-10-29 | 陕西华达陶瓷有限公司 | Ceramic tile and preparation process thereof |
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN109956676A (en) * | 2017-12-26 | 2019-07-02 | 淡江大学 | To incinerate the damping ceramics and its manufacturing method that react ash manufacture |
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| CN109437845B (en) * | 2018-12-25 | 2021-06-01 | 佛山科学技术学院 | Antiskid wear-resistant ceramic and preparation method thereof |
| CN110028334A (en) * | 2019-03-20 | 2019-07-19 | 广西大学 | A kind of ecology damping brick and preparation method thereof |
| CN111995362A (en) * | 2020-08-13 | 2020-11-27 | 福建省德化县零度创意有限公司 | Water-permeable and air-permeable microporous ceramic flowerpot and preparation process thereof |
| CN112521017A (en) * | 2021-01-13 | 2021-03-19 | 常州市武进人民医院 | Bioactive porous material and preparation method thereof |
| CN112830765A (en) * | 2021-03-03 | 2021-05-25 | 德化县嘉祥陶瓷有限公司 | Red pottery moisturizing device for brown sugar storage and manufacturing method thereof |
| CN113563050A (en) * | 2021-07-29 | 2021-10-29 | 陕西华达陶瓷有限公司 | Ceramic tile and preparation process thereof |
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