CN106883675A - A kind of water-based ink and preparation method thereof - Google Patents
A kind of water-based ink and preparation method thereof Download PDFInfo
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- CN106883675A CN106883675A CN201510936360.7A CN201510936360A CN106883675A CN 106883675 A CN106883675 A CN 106883675A CN 201510936360 A CN201510936360 A CN 201510936360A CN 106883675 A CN106883675 A CN 106883675A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/03—Printing inks characterised by features other than the chemical nature of the binder
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D11/00—Inks
- C09D11/02—Printing inks
- C09D11/10—Printing inks based on artificial resins
- C09D11/106—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- C09D11/107—Printing inks based on artificial resins containing macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds from unsaturated acids or derivatives thereof
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- Inks, Pencil-Leads, Or Crayons (AREA)
Abstract
The invention discloses a kind of water-based ink, including following component：Polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin, pigment, polyurethane, ethanol, magnesium silicate, auxiliary agent and deionized water.A kind of preparation method of water-based ink, comprises the following steps：（1）, equipment prepare；（2）, material prepare；（3）, preliminary working；（4）, secondary operation.Water-based ink disclosed by the invention, environmentally friendly, low production cost, production efficiency is high, product quality stabilization, strong adaptability, and instantaneous drying can be realized, without dusting, product stabilization, it is uniformly dispersed, using effect is good, by the addition of citric acid or peppermint oil or lavender oil, so that with lasting faint scent during product use, heat resistance is good, during high temperature is killed virus, does not result in and drops, decolourizes or discharge the phenomenons such as harmful material.
Description
Technical field
The present invention relates to printing-ink field, and in particular to a kind of preparation method of water-based ink.
Background technology
Ink is a kind of important materials for being widely used in printing industry, and it is made up of pigment, binder, auxiliary agent etc., and at present, ink is used for the various printings such as books and periodicals, packing and decorating, building decoration.As social demand increases, ink kind and yield also respective extension and growth.Ink before bimillennium as one of the material base for printing just has been occurred in that, the international generally acknowledged Chinese country to use ink in ancient civilization at first, begin to use ink early in Western Han Dynastry's period (B.C. 200 years), this ink can write transmission information on ancient books, and its some function can be with analogy with contemporary ink.In 1000 or so Christian era, the Bi Sheng of Northern Song Dynasty has invented clay type printing, substantially increases printing efficiency.For further improve production efficiency and reduces cost, shorten the cycle at quarter, some places begin to use cork to cut blocks for printing, this being cut blocks for printing easily make, and is published books fast, low cost.In addition to having big development in Anhui Jiangxi, Fujian also turns into Printing Development area with Zhejiang to Yuan Dynasty's printing technology.The Ming Dynasty is the epoch of the flourishing culture in feudal society of China later stage, is also the period of art of printing development.The development of the Ming Dynasty has following features from from the point of view of printing technology:1 has been developed polychrome set platemaking technology;The black technology of 2 systems has great progress again;3 printing technologies are further expanded using scope, and books and periodicals, newspaper, advertisement, letter paper are all the famous printed matters of the Ming Dynasty;4 letterprint books also grow a lot;5 thread-bound book extensive uses.The paddy of the 15th century Germany steps on fort and has invented metal type printing, and ink has improvement, and with lampblack as pigment, linseed oil is link stuff, and it is uniformly mixed but has been made ink at that time by hand.But until in the middle of the 19th century, the especially chemical progress of science so that the development of coal-tar colours and color science, ink manufacturer could according to user need for user make with different form and aspect, lightness, degree of unsaturation shades of colour come.Printing ink producing enters new developing stage.The species of ink is a lot, and physical property is different, and what is had is very thick, very glutinous, and what is had is but quite dilute.Its composition can be divided into three parts:Wherein liquid component is referred to as link stuff:Solid constituent is colorant (pigment or dyestuff) and various auxiliary agents.Its drying mode of different ink is also different;The ink that different printing process is used is different;The ink of different stock materials'uses is also different.Ink is classified according to the drying mode of ink, different printing process and stock material below.So that ink meets the printability of various printing process.Ink should have certain mobility, and meet the property required by various printing process, can rapidly be dried in printing, dried ink film should have resistance, colorant (pigment or dyestuff) and the various auxiliary agents such as corresponding various water-fast, acidproof, alkaline-resisting, fast light, anti-scratch, wear-resisting.For ink, color, body bone (rheological equationm of state of the ink such as dilute denseness, mobility generally is referred to as into the body bone of ink) and drying property are three most important properties of ink, ink is the important materials for packaging material printing, pattern, word are shown that stock curing ink includes that main component and auxiliary element, the formulation ratio of pigment etc. are constituted by it by printing, it is critical that, somewhat change, larger difference will be produced, but it is most sensitive to color with pigment.
Water-based ink generally also has colouring agent, link stuff, adjuvant etc. into being grouped into.Colouring agent is the present-color material of water-based ink, gives the particular color of ink one.To make trace beautiful in colour in flexo, its colouring agent is typically good from chemical stability, tinting strength, tinting power pigment high;Link stuff is made up of water, resin, aminated compounds and other organic solvents.Resin is most important composition in water-based ink, usually using water soluble acrylic resin, link stuff composition directly affects the attached function of ink, rate of drying, preventing stick dirty performance etc., while also influenceing ink and ink transfer, aminated compounds mainly maintains the alkaline ph values of water-based ink, acrylic resin is provided more preferable printing effect, water or other organic solvents are mainly dissolving resin, adjust the viscosity and rate of drying of ink;Adjuvant is mainly included:Defoamer, retarding agent, stabilizer, diluent etc. are several.Because water-based ink is a kind of soap composition, bubble is also easy to produce in use, therefore to add silicone oil and suppressed as defoamer and eliminate bubble, while improving the transfer performance of ink.Retarding agent is used to suppress the rate of drying of water-based ink, prevents ink solid in anilox roll, reduces scumming.Stabilizer can adjust ink pH, and the viscosity of ink can be also reduced as diluent.Diluent is the color for subtracting light water-based ink, as a kind of polishes, can also improve the brightness of water-based ink.Some waxs are also added to increase its wearability in other water-based ink.
The content of the invention
In view of the shortcomings of the prior art, it is an object of the invention to provide a kind of preparation method of water-based ink.
Present invention solves the technical problem that can be realized using following technical scheme：A kind of preparation method of water-based ink, including following component：20~40 parts of polyamide, 15~30 parts of methyl acrylate, 20~25 parts of butyl acrylate, 2~4 parts of organic-silicon-modified PEF wax, 5~10 parts of rosin, 15~35 parts of pigment, 1~2 part of polyurethane, 10~15 parts of 5~15 parts of ethanol, 5~8 parts of magnesium silicate, 1~3 part of auxiliary agent and deionized water.
Preferably, the pigment is aqueous pigment.
Preferably, the rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；
（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape；
（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing, sealed beaker and insufflation gas heated on alcolhol burner, be incubated 5~8 minutes；
（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85~120 degree, and stirring at low speed 10~15 minutes, be heated to 260~320 degree, and high-speed stirred 1 hour, you can be obtained.
Preferably, the step（2）In be ground to material fineness be 5.0 microns ~ 6.0 microns.
Preferably, the step（3）In gas be nitrogen or inert gas.
Preferably, the step（4）In stirring at low speed speed be 50~100 rpms, the speed of high-speed stirred is 180~250 rpms.
Preferably, the step（4）The mixed liquor of one or more in 0~1 part of citric acid, 0~2 part of peppermint oil, 0~2.5 part of lavender oil can be added afterwards.
Beneficial effect is：Water-based ink disclosed by the invention, environmentally friendly, low production cost, production efficiency is high, product quality stabilization, strong adaptability, and instantaneous drying can be realized, without dusting, product stabilization, it is uniformly dispersed, using effect is good, by the addition of citric acid or peppermint oil or lavender oil, so that with lasting faint scent during product use, heat resistance is good, during high temperature is killed virus, does not result in and drops, decolourizes or discharge the phenomenons such as harmful material.
Specific embodiment
Embodiment
1
The following detailed description of the preferred embodiment of the present invention.
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, is heated to 260 degree, and high-speed stirred 1 hour, and the speed of high-speed stirred is 180 rpms, you can be obtained.
Embodiment
2
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, is heated to 260 degree, and high-speed stirred 1 hour, the speed of high-speed stirred is 180 rpms, adds 1 part of citric acid, you can be obtained.
Embodiment
3
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, is heated to 260 degree, and high-speed stirred 1 hour, the speed of high-speed stirred is 180 rpms, adds 2 parts of peppermint oil, you can be obtained.
Embodiment
4
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, is heated to 260 degree, and high-speed stirred 1 hour, the speed of high-speed stirred is 180 rpms, adds 2.5 parts of lavender oil, you can be obtained.
Embodiment
5
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, it is heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, it is heated to 260 degree, and high-speed stirred 1 hour, the speed of high-speed stirred is 180 rpms, add 1 part of citric acid, 2 parts of peppermint oil, the mixed liquor of 2.5 parts of lavender oil, you can be obtained.
Embodiment
5
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：10 parts of 20 parts of polyamide, 15 parts of methyl acrylate, 20 parts of butyl acrylate, 2 parts of organic-silicon-modified PEF wax, 5 parts of rosin, 15 parts of pigment, 1 part of polyurethane, 5 parts of ethanol, 5 parts of magnesium silicate, 1 part of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 6.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 8 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 120 degree, and stirring at low speed 15 minutes, stirring at low speed speed is 100 rpms, is heated to 320 degree, and high-speed stirred 1 hour, and the speed of high-speed stirred is 250 rpms, you can be obtained.
Embodiment
6
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：15 parts of 40 parts of polyamide, 30 parts of methyl acrylate, 25 parts of butyl acrylate, 4 parts of organic-silicon-modified PEF wax, 10 parts of rosin, 35 parts of pigment, 2 parts of polyurethane, 15 parts of ethanol, 8 parts of magnesium silicate, 3 parts of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 5.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 5 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85 degree, and stirring at low speed 10 minutes, stirring at low speed speed is 50 rpms, is heated to 260 degree, and high-speed stirred 1 hour, and the speed of high-speed stirred is 180 rpms, you can be obtained.
Embodiment
7
A kind of specific embodiment of the preparation method of water-based ink of the present invention：A kind of preparation method of water-based ink, including following component：15 parts of 40 parts of polyamide, 30 parts of methyl acrylate, 25 parts of butyl acrylate, 4 parts of organic-silicon-modified PEF wax, 10 parts of rosin, 35 parts of pigment, 2 parts of polyurethane, 15 parts of ethanol, 8 parts of magnesium silicate, 3 parts of auxiliary agent and deionized water.Pigment is aqueous pigment.Rosin is fumaric acid modified rosin resin.
A kind of preparation method of water-based ink, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape, the fineness for being ground to material is 6.0 microns；（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing heated on alcolhol burner, sealed beaker is simultaneously filled with nitrogen or inert gas, is incubated 8 minutes；（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 120 degree, and stirring at low speed 15 minutes, stirring at low speed speed is 100 rpms, is heated to 320 degree, and high-speed stirred 1 hour, and the speed of high-speed stirred is 250 rpms, you can be obtained.
By after above-mentioned processing step, obtaining a kind of water-based ink, its product quality stabilization, strong adaptability, and instantaneous drying can be realized, and it is uniformly dispersed, using effect is good.
The foregoing is only embodiments of the invention; not thereby the scope of the claims of the invention is limited; equivalent structure or equivalent flow conversion that every utilization description of the invention is made, or other related technical fields are directly or indirectly used in, it is included within the scope of the present invention.
Claims (8)
1. a kind of water-based ink, it is characterised in that including following component：20~40 parts of polyamide, 15~30 parts of methyl acrylate, 20~25 parts of butyl acrylate, 2~4 parts of organic-silicon-modified PEF wax, 5~10 parts of rosin, 15~35 parts of pigment, 1~2 part of polyurethane, 10~15 parts of 5~15 parts of ethanol, 5~8 parts of magnesium silicate, 1~3 part of auxiliary agent and deionized water.
2. a kind of water-based ink according to claim 1, it is characterised in that：The pigment is aqueous pigment.
3. a kind of water-based ink according to claim 1, it is characterised in that：The rosin is fumaric acid modified rosin resin.
4. a kind of preparation method of water-based ink any according to claim 1-3, it is characterised in that comprise the following steps：（1）, equipment prepare：Prepare mill, mixer alcolhol burner and beaker etc.；
（2）, material prepare：By above-mentioned material on deck, polyamide, methyl acrylate, butyl acrylate, organic-silicon-modified PEF wax, rosin are clayed into power shape；
（3）, preliminary working：By step（2）In the dusty material worn into inserted in beaker in addition to rosin, be placed on after adding water and fusing, sealed beaker and insufflation gas heated on alcolhol burner, be incubated 5~8 minutes；
（4）, secondary operation：By step（3）In remaining material be all added in beaker, be heated to 85~120 degree, and stirring at low speed 10~15 minutes, be heated to 260~320 degree, and high-speed stirred 1 hour, you can be obtained.
5. a kind of preparation method of water-based ink according to claim 4, it is characterised in that：The step（2）In be ground to material fineness be 5.0 microns ~ 6.0 microns.
6. a kind of preparation method of water-based ink according to claim 4, it is characterised in that：The step（3）In gas be nitrogen or inert gas.
7. a kind of preparation method of water-based ink according to claim 4, it is characterised in that：The step（4）In stirring at low speed speed be 50~100 rpms, the speed of high-speed stirred is 180~250 rpms.
8. a kind of preparation method of water-based ink according to claim 4, it is characterised in that：The step（4）The mixed liquor of one or more in 0~1 part of citric acid, 0~2 part of peppermint oil, 0~2.5 part of lavender oil can be added afterwards.
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Application publication date: 20170623 |