CN106880507A - Washing-free antibacterial hand sanitizer and preparation method thereof - Google Patents
Washing-free antibacterial hand sanitizer and preparation method thereof Download PDFInfo
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- CN106880507A CN106880507A CN201710087655.0A CN201710087655A CN106880507A CN 106880507 A CN106880507 A CN 106880507A CN 201710087655 A CN201710087655 A CN 201710087655A CN 106880507 A CN106880507 A CN 106880507A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/19—Cosmetics or similar toiletry preparations characterised by the composition containing inorganic ingredients
- A61K8/27—Zinc; Compounds thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
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- A—HUMAN NECESSITIES
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- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N37/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a carbon atom having three bonds to hetero atoms with at the most two bonds to halogen, e.g. carboxylic acids
- A01N37/02—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof
- A01N37/04—Saturated carboxylic acids or thio analogues thereof; Derivatives thereof polybasic
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N41/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom
- A01N41/02—Biocides, pest repellants or attractants, or plant growth regulators containing organic compounds containing a sulfur atom bound to a hetero atom containing a sulfur-to-oxygen double bond
- A01N41/04—Sulfonic acids; Derivatives thereof
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N59/00—Biocides, pest repellants or attractants, or plant growth regulators containing elements or inorganic compounds
- A01N59/16—Heavy metals; Compounds thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/362—Polycarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/46—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur
- A61K8/466—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing sulfur containing sulfonic acid derivatives; Salts
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q17/00—Barrier preparations; Preparations brought into direct contact with the skin for affording protection against external influences, e.g. sunlight, X-rays or other harmful rays, corrosive materials, bacteria or insect stings
- A61Q17/005—Antimicrobial preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/10—Washing or bathing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/40—Chemical, physico-chemical or functional or structural properties of particular ingredients
- A61K2800/41—Particular ingredients further characterized by their size
- A61K2800/413—Nanosized, i.e. having sizes below 100 nm
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Abstract
The present invention relates to include washing-free antibacterial hand sanitizer of Nano-Zinc antiseptic and preparation method thereof.Washing-free antibacterial hand sanitizer of the invention has outstanding bactericidal effect and low-down skin irritation, can be widely applied to the antibacterial of skin and body surface in daily life, antibacterial, sterilization.
Description
Technical field
The invention belongs to sterile products technical field, and in particular to a kind of washing-free antibacterial hand sanitizer, and preparation method thereof.
Background technology
Antibacterial includes antibacterial, sterilizing, sterilized, mould proof, anti-corrosion.Bacterium is killed using chemically or physically method or is prevented thin
The process of bacteria growing breeding is the general name of antibacterial.Antiseptic is can to make certain micro-organisms within a certain period of time（Bacterium, fungi,
Saccharomycete, algae and virus etc.）Growth or breeding be maintained at necessary chemical substance below horizontal.
Antiseptic is broadly divided into organic antibacterial agent, inorganic antiseptic and natural antibacterial agent.Organic antibacterial agent anti-microbial property is high,
Sterilization speed is fast, but to environment and human body is harmful and working life is short, poor heat resistance；Natural antibacterial agent antimicrobial efficiency is high, peace
Atoxic, but processing difficulties, poor heat resistance.Inorganic antiseptic is because its effective antibacterial phase is long, the good, has a broad antifungal spectrum of heat resistance etc.
Feature turns into the class antiseptic being most widely used.
In inorganic antiseptic, at most, purposes is most for the inorganic salts of metal ion or the inorganic antiseptic kind of complex compound
Extensively, at most, wherein antibiotic property size is ordered as yield：Hg>Ag>Cd>Cu>Zn>Fe>Ni etc., but be with antibiotic property only
Inadequate, also requiring that it can not be damaged to human body, the metal such as Hg, Cd, Pb also has antibacterial ability, but harmful.
The security of metal ion is ordered as：Ag>Co>Ni>Al>Zn>Cu=Fe>Mn>Sn>Ba>Mg>Ca, so with regard to security and antibacterial
Property the common result for considering, next to that Cu systems and Zn systems, therefore these three with inorganic compound as carrier with Ag ions preferably
Inorganic antiseptic is obtained a wide range of applications.But, Cu ions carry color because of itself, can influence the expressive force of product；Silver
Because its easy oxidation discoloration, it is expensive, easily reunite the problems such as, be restricted using scope.
Metallic zinc is the 1/1000 of argent due to the antibacterial ability of itself, causes most of research institutions and manufacturer
All energy is concentrated in the modified research and development of Ag and Nano Silver to improve it as the performance of antiseptic, so as to have ignored zinc conduct
The plurality of advantages of antiseptic, studies seldom it.In fact, Nano-Zinc antiseptic can overcome nano silver antimicrobials actually should
Many defects in, such as easily oxidation, blackening, expensive, difficult dispersion, and possess significant antibacterial effect, significantly
Extend antibacterial ageing, especially can relatively easily be scattered in corresponding product, such as plastics, textile fabric, slurry,
Waterborne liquid, oil soluble liquid, greatly extend range of application.Therefore, research and development Nano-Zinc antiseptic can be greatly
Meet social desirability.
Within past a very long time, sanitary washing is used as commonly using soap, perfumed soap in people's daily life
Articles for use.Though soap, perfumed soap easily slide when in use with good dirt-removing power, meeting water and high temperature can soften and nature
Consumption, soap, perfumed soap can make dry skin in alkalescence after cleaning, lack gloss, and soap, perfumed soap are sterilized in cleaning process
Effect is limited, and is bound to be infected with dirt on hand and bacterium after use, produces secondary pollution, and washing-free antibacterial hand sanitizer
With antibacterial, skin care, using and effect easy to clean etc..Recently as growth in the living standard, people's consumption idea
Change therewith, demand higher is it is also proposed to hygiene, so that washing-free antibacterial hand sanitizer substitutes conventional soap, perfumed soap,
As widely used hand-washing article, work, family and public arena are applied to.
The major antibacterial composition of current anti-bacterial hand lotion on the market is with parachlorometaxylenol, gluconic acid chlorhexidine, iodine
Based on class, alcohols, quaternary ammonium salt and its complex antimicrobials, these antiseptics are all easily caused the resistance to the action of a drug and mistake to varying degrees
The generation of quick reaction, and there is the defects such as action time is short, bactericidal range is narrow.
The content of the invention
To solve above-mentioned the problems of washing-free antibacterial hand sanitizer in the prior art, the present invention proposes a kind of including receiving
Washing-free antibacterial hand sanitizer of rice zinc antiseptic and preparation method thereof, washing-free antibacterial hand sanitizer of the invention has outstanding sterilized effect
Fruit and low-down skin irritation, can be widely applied to the antibacterial of skin and body surface in daily life, antibacterial, sterilization.
In an aspect, the present invention relates to a kind of washing-free antibacterial hand sanitizer, it is grouped into by each group of following mass fraction：
The mass parts of Nano-Zinc antiseptic 0.5 ~ 3, the mass parts of ethanol 20 ~ 65, the mass parts of isopropanol 0.5 ~ 10, the mass parts of propane diols 0.1 ~ 5,
The mass parts of deionized water 10 ~ 90, the mass parts of essence 0 ~ 0.5.
In a preferred embodiment, the content of the essence is not zero.
In a preferred embodiment, described washing-free antibacterial hand sanitizer is grouped into by each group of following mass fraction：Receive
The mass parts of rice zinc antiseptic 1, the mass parts of ethanol 60, the mass parts of isopropanol 5, the mass parts of propane diols 0.3, the mass of deionized water 33
Part, the mass parts of essence 0.01.
In another aspect, the present invention relates to the preparation method of the washing-free antibacterial hand sanitizer, comprise the following steps：
（1）The Nano-Zinc antiseptic of formula rate amount is added in reactor, the deionized water for being subsequently added 1/3 formula ratio is stirred
Mix 3-10min；Preferably 4-6min；More preferably 5min；
（2）The ethanol of formula ratio is added while stirring, it is extremely well mixed；
（3）Isopropanol, the propane diols of formula ratio are sequentially added under stirring, it is extremely well mixed；
（4）Add the deionized water of surplus while stirring, stirring 5-15min is to well mixed；Preferably 7-12min；It is more excellent
Elect 10min as；
（5）It is added dropwise to essence under stirring, and continues stirring to well mixed.
In various embodiments, isopropanol can be replaced normal propyl alcohol or polyethylene glycol.
In various embodiments, propane diols can be replaced glycerine, hyaluronic acid, amino acid or water-soluble Jojoba
Oil.
Wherein, ethanol has the disposable effect of volatilization concurrently as primary solvent, and isopropanol, propane diols play the work of volatilization hydrotropy
With, and smell is thin.Can be reduced in the case where disposable performance is not changed using three kinds of components as described above and be given out
Smell.
Nano-Zinc antiseptic of the invention and preparation method thereof for example may refer to Chinese patent application CN
201510532442.5, entire contents are incorporated herein here by reference.
Specific embodiment
Embodiments of the invention will hereafter be conducted further description, wherein, each embodiment is only the exemplary present invention
Implementation method, it is not intended to constitute limiting the scope of the invention.Those skilled in the art can according to explanation above with
And following description of the embodiments makes various different improvement and deformation, it is without departing from spirit and substance of the present invention.
Accordingly, the scope of the present invention is intended merely to be defined by every claim scope required for protection.
Embodiment 1
0.5g Nano-Zinc antiseptics are added in reactor, 30g deionized waters stirring 5min is subsequently added；Add while stirring
The ethanol of 30g, it is extremely well mixed；5g isopropanols and 1g propane diols are sequentially added under stirring, it is extremely well mixed；Stir on side
Side adds 60g deionized waters, and stirring 10min is to well mixed；0.02g essence is added dropwise under stirring, and continues stirring extremely
It is well mixed；Obtain washing-free antibacterial hand sanitizer of the invention.
Embodiment 2
1g Nano-Zinc antiseptics are added in reactor, 11g deionized waters stirring 5min is subsequently added；Add while stirring
The ethanol of 60g, it is extremely well mixed；5g isopropanols and 0.3g propane diols are sequentially added under stirring, it is extremely well mixed；While stirring
Mix side and add 22g deionized waters, stirring 10min is to well mixed；0.01g essence is added dropwise under stirring, and continues stirring
It is extremely well mixed；Obtain washing-free antibacterial hand sanitizer of the invention.
Embodiment 3
2g Nano-Zinc antiseptics are added in reactor, 15g deionized waters stirring 5min is subsequently added；Add while stirring
The ethanol of 45g, it is extremely well mixed；2g isopropanols and 4g propane diols are sequentially added under stirring, it is extremely well mixed；Stir on side
Side adds 30g deionized waters, and stirring 10min is to well mixed；It is added dropwise 0.1g essence under stirring, and continues stirring to mixed
Close uniform；Obtain washing-free antibacterial hand sanitizer of the invention.
Embodiment 4
3g Nano-Zinc antiseptics are added in reactor, 25g deionized waters stirring 5min is subsequently added；Add while stirring
The ethanol of 36g, it is extremely well mixed；2g isopropanols and 1.2g glycerine are sequentially added under stirring, it is extremely well mixed；While stirring
Mix side and add 50g deionized waters, stirring 10min is to well mixed；0.15g essence is added dropwise under stirring, and continues stirring
It is extremely well mixed；Obtain washing-free antibacterial hand sanitizer of the invention.
Embodiment 5
0.5g Nano-Zinc antiseptics are added in reactor, 4g deionized waters stirring 3min is subsequently added；Add while stirring
The ethanol of 65g, it is extremely well mixed；9g isopropanols and 0.1g glycerine are sequentially added under stirring, it is extremely well mixed；While stirring
Mix side and add 8g deionized waters, stirring 15min is to well mixed；0.01g essence is added dropwise under stirring, and continues stirring extremely
It is well mixed；Obtain washing-free antibacterial hand sanitizer of the invention.
Embodiment 6
3g Nano-Zinc antiseptics are added in reactor, 25g deionized waters stirring 5min is subsequently added；Add while stirring
The ethanol of 20g, it is extremely well mixed；10g isopropanols and 5g glycerine are sequentially added under stirring, it is extremely well mixed；While stirring
Mix side and add 50g deionized waters, stirring 14min is to well mixed；0.5g essence is added dropwise under stirring, and continues stirring extremely
It is well mixed；Obtain washing-free antibacterial hand sanitizer of the invention.
Claims (8)
1. a kind of washing-free antibacterial hand sanitizer, it is characterised in that be grouped into by each group of following mass fraction：Nano-Zinc antiseptic 0.5
~ 3 mass parts, the mass parts of ethanol 20 ~ 65, the mass parts of isopropanol 0.5 ~ 10, the mass parts of propane diols 0.1 ~ 5, the matter of deionized water 10 ~ 90
Amount part, the mass parts of essence 0 ~ 0.5.
2. washing-free antibacterial hand sanitizer according to claim 1, it is characterised in that：The content of the essence is not zero.
3. washing-free antibacterial hand sanitizer according to claim 1 and 2, it is characterised in that be grouped by each group of following mass fraction
Into：The mass parts of Nano-Zinc antiseptic 1, the mass parts of ethanol 60, the mass parts of isopropanol 5, the mass parts of propane diols 0.3, deionized water 33
Mass parts, the mass parts of essence 0.01.
4. the washing-free antibacterial hand sanitizer according to any one of claims 1 to 3, it is characterised in that：Isopropanol replaces with positive third
Alcohol or polyethylene glycol.
5. the washing-free antibacterial hand sanitizer according to any one of Claims 1-4, it is characterised in that：Propane diols replaces with the third three
Alcohol, hyaluronic acid, amino acid or water-soluble jojoba oil.
6. the preparation method of the washing-free antibacterial hand sanitizer according to any one of claim 1 to 5, it is characterised in that including following
Step：
（1）The Nano-Zinc antiseptic of formula rate amount is added in reactor, the deionized water for being subsequently added 1/3 formula ratio is stirred
Mix 3-10min；
（2）The ethanol of formula ratio is added while stirring, it is extremely well mixed；
（3）Isopropanol, the propane diols of formula ratio are sequentially added under stirring, it is extremely well mixed；
（4）Add the deionized water of surplus while stirring, stirring 5-15min is to well mixed；
（5）It is added dropwise to essence under stirring, and continues stirring to well mixed.
7. preparation method according to claim 6, it is characterised in that：Step（1）Mixing time be 4-6min；Preferably
5min。
8. the preparation method according to claim 6 or 7, it is characterised in that：Step（4）Mixing time be 7-12min；It is excellent
Elect 10min as.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710087655.0A CN106880507A (en) | 2017-02-17 | 2017-02-17 | Washing-free antibacterial hand sanitizer and preparation method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710087655.0A CN106880507A (en) | 2017-02-17 | 2017-02-17 | Washing-free antibacterial hand sanitizer and preparation method thereof |
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| Publication Number | Publication Date |
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| CN106880507A true CN106880507A (en) | 2017-06-23 |
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| CN201710087655.0A Pending CN106880507A (en) | 2017-02-17 | 2017-02-17 | Washing-free antibacterial hand sanitizer and preparation method thereof |
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Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108271807A (en) * | 2018-02-05 | 2018-07-13 | 南京凯创协同纳米技术有限公司 | Travelling antimicrobial spray |
| CN111249220A (en) * | 2020-02-17 | 2020-06-09 | 李立和 | Formula of hand-washing-free efficient disinfection gel |
| CN111944617A (en) * | 2020-08-19 | 2020-11-17 | 河南昇阳生物科技有限公司 | Composite water-free hand sanitizer containing amino acid |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101658469A (en) * | 2009-09-10 | 2010-03-03 | 上海泛亚生命科技有限公司 | Cleaning-free hand sanitizer and preparation thereof |
| CN105708718A (en) * | 2016-04-13 | 2016-06-29 | 广州丹奇日用化工厂有限公司 | Acne-removal cosmetic composition containing nano-zinc |
| CN106265449A (en) * | 2016-09-19 | 2017-01-04 | 江苏田亮日用品有限公司 | A kind of composite bactericidal handwashing liquid and preparation method thereof |
-
2017
- 2017-02-17 CN CN201710087655.0A patent/CN106880507A/en active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101658469A (en) * | 2009-09-10 | 2010-03-03 | 上海泛亚生命科技有限公司 | Cleaning-free hand sanitizer and preparation thereof |
| CN105708718A (en) * | 2016-04-13 | 2016-06-29 | 广州丹奇日用化工厂有限公司 | Acne-removal cosmetic composition containing nano-zinc |
| CN106265449A (en) * | 2016-09-19 | 2017-01-04 | 江苏田亮日用品有限公司 | A kind of composite bactericidal handwashing liquid and preparation method thereof |
Cited By (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108271807A (en) * | 2018-02-05 | 2018-07-13 | 南京凯创协同纳米技术有限公司 | Travelling antimicrobial spray |
| CN111249220A (en) * | 2020-02-17 | 2020-06-09 | 李立和 | Formula of hand-washing-free efficient disinfection gel |
| CN111944617A (en) * | 2020-08-19 | 2020-11-17 | 河南昇阳生物科技有限公司 | Composite water-free hand sanitizer containing amino acid |
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Application publication date: 20170623 |