CN106861890B - A kind of cassiterite process mineralogy ore-dressing technique - Google Patents
A kind of cassiterite process mineralogy ore-dressing technique Download PDFInfo
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- CN106861890B CN106861890B CN201710037697.3A CN201710037697A CN106861890B CN 106861890 B CN106861890 B CN 106861890B CN 201710037697 A CN201710037697 A CN 201710037697A CN 106861890 B CN106861890 B CN 106861890B
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- cassiterite
- ore
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03B—SEPARATING SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS
- B03B7/00—Combinations of wet processes or apparatus with other processes or apparatus, e.g. for dressing ores or garbage
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B02—CRUSHING, PULVERISING, OR DISINTEGRATING; PREPARATORY TREATMENT OF GRAIN FOR MILLING
- B02C—CRUSHING, PULVERISING, OR DISINTEGRATING IN GENERAL; MILLING GRAIN
- B02C21/00—Disintegrating plant with or without drying of the material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D1/00—Flotation
- B03D1/001—Flotation agents
- B03D1/018—Mixtures of inorganic and organic compounds
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D3/00—Differential sedimentation
- B03D3/06—Flocculation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B03—SEPARATION OF SOLID MATERIALS USING LIQUIDS OR USING PNEUMATIC TABLES OR JIGS; MAGNETIC OR ELECTROSTATIC SEPARATION OF SOLID MATERIALS FROM SOLID MATERIALS OR FLUIDS; SEPARATION BY HIGH-VOLTAGE ELECTRIC FIELDS
- B03D—FLOTATION; DIFFERENTIAL SEDIMENTATION
- B03D2201/00—Specified effects produced by the flotation agents
- B03D2201/02—Collectors
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- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Food Science & Technology (AREA)
- Manufacture And Refinement Of Metals (AREA)
Abstract
The invention discloses a kind of cassiterite ore-dressing techniques, include the following steps: the broken screening of cassiterite, and grading vibration screening after being crushed is collected respectively;Preconcentration puts together the thin mud of multipass sort;Graded desliming, the thin mud that partial size after sorting is put together are sieved by filter mud and carry out separating and filtering, and crude separation screening cassiterite is obtained;Crude separation screening cassiterite is incorporated in collectors for cassiterite, is stood after strong mixing, carried out classified filtering after standing and obtain by-pass filtration liquid and secondary filtration liquid by cassiterite collecting;Tin-lead soldering injects air into by-pass filtration liquid, collects cassiterite dross, and secondary filtration liquid is carried out high temperature concentration;Cassiterite dross is dried and obtains cassiterite product by drying forming;Improving accumulation rate reduces the flow time of process during carrying out collecting, improves the service efficiency of actual production, improves the thick recovery utilization rate of drug, reduces production cost.
Description
Technical field
The present invention relates to mineralogy technology fields, and in particular to a kind of cassiterite process mineralogy ore-dressing technique.
Background technique
Tin-lead soldering is primarily referred to as the flotation of Fine cassiterite.Cassiterite is the crisp mineral of property, and cleavage, crack, cause to grind in addition
Mine process easily crushes argillization, and always there is floatation recycling Fine cassiterite is necessary cassiterite argillization to some extent.State
Inside and outside expert has done a large amount of work with regard to the Oxidized copper ores of micro fine particle, but really realize industrialized production and it is few.Tin
The progress of stone flotation technology is largely shown in the process of pretreatment early period, the research of collecting agent and collecting technique.
Tin-lead soldering common problem is, since fine-particle minerals surface area is big, quality is small, to cause conventional floating at present
Mechanical entrainment is serious when method being selected to recycle, and medicament specificity is poor and dosage is big, causes concentrate grade and the rate of recovery not high, and for
The usage amount of medicament requires greatly, especially collecting agent, and again since medicament can not be recycled slightly, wastage
More, and do that secondary further purified treatment cost is big, the economic cost of flotation further increases, it is difficult to meet market at
This demand.
Summary of the invention
In view of the above problems, the present invention is directly with cassiterite the present invention provides a kind of cassiterite process mineralogy ore-dressing technique
The mistake of cassiterite should be avoided to crush as far as possible in ore grinding in order to guarantee effective recycling of cassiterite for raw material and carry out two multiple fractions
From and screening, substantially increase the accumulation rate of same particle size cassiterite, improve pretreated first enrichment, and carrying out collecting
In the process, using stirring, standing and air flotation, the flow time of process is greatly reduced, improves making for actual production
With efficiency, and classification processing can also be carried out after carrying out secondary sorting and respectively obtains cassiterite and recovered liquid, improve the thick of drug
Recovery utilization rate reduces production cost, can effectively solve the problems in background technique.
To achieve the goals above, The technical solution adopted by the invention is as follows: a kind of cassiterite process mineralogy ore-dressing technique,
Include the following steps:
The cassiterite for needing ore dressing concentration coarse grain is crushed, by shaking after carrying out coarse grain and being crushed by the broken screening of S1, cassiterite
Bed carries out grading vibration screening, and collecting respectively by size fractionated range;
Collected cassiterite is crushed by S2, preconcentration again, and the particle size range of cassiterite is 0.5- after being crushed
1mm;Then again by next stage separation by shaking table, and the tailing on shaking tables at different levels is abandoned, the thin mud of sortings at different levels is concentrated
Get up;
The thin mud put together after sorting is sieved by filter mud and carries out separating and filtering by S3, graded desliming, obtains crude separation sieve
Select cassiterite;
Crude separation screening cassiterite is incorporated in collectors for cassiterite, and is added and lives in collectors for cassiterite by S4, cassiterite collecting
Property agent and stabilizer, strong mixing is carried out after adding reagent, is stood after strong mixing, carries out classified filtering after standing
By-pass filtration liquid and secondary filtration liquid are obtained, the filter screen mesh number of secondary filtration is higher than primary filter mesh number.
S5, tin-lead soldering inject air into by-pass filtration liquid, and flocculant are added while injecting air, collect
Secondary filtration liquid is carried out high temperature concentration, puts into step S4 and be recycled after concentration by the cassiterite dross that surface floats;
Cassiterite dross is dried and obtains cassiterite product by S6, drying forming.
In the step S1 and S2, cassiterite is broken to avoid the excessively broken of cassiterite as far as possible, and tricresyl phosphate fourth is added in cassiterite
Ester,
According to the above technical scheme, in the step S3, hot-air seasoning is first carried out before carrying out filter mud, it is aqueous after drying
Amount is lower than 20%.
According to the above technical scheme, in the step S4, the collectors for cassiterite is fatty acid collecting agent or and alkyl
One of hydroximic acid, alkyl sulfosuccinate acids, phosphonic acids and organic sequestering agent or a variety of mixtures.
In the step S4, the activating agent is lead chloride, and the stabilizer is iron chloride.
In the step S4, the stirring rate of strong mixing is 3600-4000r/min;Time of repose is 2-4h, preferably 2-
3 hours.
In the step S5, the speed of gas injection is 40-50L/min.
Beneficial effects of the present invention:
The present invention, in order to guarantee effective recycling of cassiterite, should avoid cassiterite in ore grinding directly using cassiterite as raw material as far as possible
It crosses and crushes and carry out multiple the second-order separation and screening, substantially increase the accumulation rate of same particle size cassiterite, improve pretreatment
First enrichment using stirring, standing and air flotation, greatly reduce the stream of process and during carrying out collecting
The water time improves the service efficiency of actual production, and can also carry out classification processing after carrying out secondary sorting and respectively obtain
Cassiterite and recovered liquid improve the thick recovery utilization rate of drug, reduce production cost.
Detailed description of the invention
Fig. 1 is the graph of relation of mixing speed of the present invention and flotation efficiency.
Fig. 2 is the graph of relation of time of repose of the present invention and flotation efficiency.
Fig. 3 is the graph of relation of gas injection speed of the present invention and flotation efficiency.
Specific embodiment
In order to make the objectives, technical solutions, and advantages of the present invention clearer, with reference to embodiments, to the present invention
It is further elaborated.It should be appreciated that the specific embodiments described herein are merely illustrative of the present invention, it is not used to
Limit the present invention.
Embodiment 1:
A kind of cassiterite process mineralogy ore-dressing technique, includes the following steps:
The cassiterite for needing ore dressing concentration coarse grain is crushed, by shaking after carrying out coarse grain and being crushed by the broken screening of S1, cassiterite
Bed carries out grading vibration screening, and collecting respectively by size fractionated range;
The cassiterite of size fractionated range is being crushed by S2, preconcentration, the broken mistake for avoiding cassiterite as far as possible of cassiterite
It is broken, tributyl phosphate is added in cassiterite, broken particle size range is 0.5-1mm, and again by next stage shaking table point
Choosing, and the tailing on shaking tables at different levels is abandoned, the thin mud of multipass sort is put together;
S3, graded desliming are first dried before filter mud, hot-air seasoning are first carried out before carrying out filter mud, after drying
Water content is lower than 20%, and the thin mud that partial size after sorting is put together is sieved by filter mud and carries out separating and filtering, obtains crude separation sieve
Select cassiterite;
Crude separation screening cassiterite is incorporated in collectors for cassiterite, and is added and lives in collectors for cassiterite by S4, cassiterite collecting
Property agent and stabilizer, the collectors for cassiterite is fatty acid collecting agent, alkyl hydroximic acid, alkyl sulfosuccinate acids, phosphonic acids
With one of organic sequestering agent or a variety of mixtures, the activating agent is chlorination dithizone, and the stabilizer is that iron chloride tries
Agent carries out strong mixing after adding reagent, is stood after strong mixing, carries out classified filtering after standing and obtains level-one mistake
Filtrate and secondary filtration liquid, the stirring rate of strong mixing are 3600r/min, time of repose 2h;
S5, tin-lead soldering inject air into by-pass filtration liquid, and the speed of gas injection is 40L/min, and in injection air
Flocculant is added simultaneously, collects the cassiterite dross that surface floats, secondary filtration liquid is subjected to high temperature concentration, step is put into after concentration
It is recycled in rapid S4;
Cassiterite dross is dried and obtains cassiterite product by S6, drying forming.
Embodiment 2:
A kind of cassiterite process mineralogy ore-dressing technique, includes the following steps:
The cassiterite for needing ore dressing concentration coarse grain is crushed, by shaking after carrying out coarse grain and being crushed by the broken screening of S1, cassiterite
Bed carries out grading vibration screening, and collecting respectively by size fractionated range;
The cassiterite of size fractionated range is being crushed by S2, preconcentration, the broken mistake for avoiding cassiterite as far as possible of cassiterite
It is broken, tributyl phosphate is added in cassiterite, broken particle size range is 0.5-1mm, and again by next stage shaking table point
Choosing, and the tailing on shaking tables at different levels is abandoned, the thin mud of multipass sort is put together;
S3, graded desliming are first dried before filter mud, hot-air seasoning are first carried out before carrying out filter mud, after drying
Water content is lower than 20%, and the thin mud that partial size after sorting is put together is sieved by filter mud and carries out separating and filtering, obtains crude separation sieve
Select cassiterite;
Crude separation screening cassiterite is incorporated in collectors for cassiterite, and is added and lives in collectors for cassiterite by S4, cassiterite collecting
Property agent and stabilizer, the collectors for cassiterite is fatty acid collecting agent, alkyl hydroximic acid, alkyl sulfosuccinate acids, phosphonic acids
With one of organic sequestering agent or a variety of mixtures, the activating agent is chlorination dithizone, and the stabilizer is that iron chloride tries
Agent carries out strong mixing after adding reagent, is stood after strong mixing, carries out classified filtering after standing and obtains level-one mistake
Filtrate and secondary filtration liquid, the stirring rate of strong mixing are 3800r/min, time of repose 3h;
S5, tin-lead soldering inject air into by-pass filtration liquid, and the speed of gas injection is 45L/min, and in injection air
Flocculant is added simultaneously, collects the cassiterite dross that surface floats, secondary filtration liquid is subjected to high temperature concentration, step is put into after concentration
It is recycled in rapid S4;
Cassiterite dross is dried and obtains cassiterite product by S6, drying forming.
Embodiment 3:
A kind of cassiterite process mineralogy ore-dressing technique, includes the following steps:
The cassiterite for needing ore dressing concentration coarse grain is crushed, by shaking after carrying out coarse grain and being crushed by the broken screening of S1, cassiterite
Bed carries out grading vibration screening, and collecting respectively by size fractionated range;
The cassiterite of size fractionated range is being crushed by S2, preconcentration, the broken mistake for avoiding cassiterite as far as possible of cassiterite
It is broken, tributyl phosphate is added in cassiterite, broken particle size range is 0.5-1mm, and again by next stage shaking table point
Choosing, and the tailing on shaking tables at different levels is abandoned, the thin mud of multipass sort is put together;
S3, graded desliming are first dried before filter mud, hot-air seasoning are first carried out before carrying out filter mud, after drying
Water content is lower than 20%, and the thin mud that partial size after sorting is put together is sieved by filter mud and carries out separating and filtering, obtains crude separation sieve
Select cassiterite;
Crude separation screening cassiterite is incorporated in collectors for cassiterite, and is added and lives in collectors for cassiterite by S4, cassiterite collecting
Property agent and stabilizer, the collectors for cassiterite is fatty acid collecting agent, alkyl hydroximic acid, alkyl sulfosuccinate acids, phosphonic acids
With one of organic sequestering agent or a variety of mixtures, the activating agent is chlorination dithizone, and the stabilizer is that iron chloride tries
Agent carries out strong mixing after adding reagent, is stood after strong mixing, carries out classified filtering after standing and obtains level-one mistake
Filtrate and secondary filtration liquid, the stirring rate of strong mixing are 4000r/min, time of repose 4h;
S5, tin-lead soldering inject air into by-pass filtration liquid, and the speed of gas injection is 50L/min, and in injection air
Flocculant is added simultaneously, collects the cassiterite dross that surface floats, secondary filtration liquid is subjected to high temperature concentration, step is put into after concentration
It is recycled in rapid S4;
Cassiterite dross is dried and obtains cassiterite product by S6, drying forming.
Mixing speed, time of repose and gas injection speed etc. are had studied to the shadow of tin-lead soldering performance by following test method
It rings.
(1) mixing speed (as shown in Figure 1)
In the case where other conditions are consistent, the speed of rotation has apparent influence to the tin-lead soldering effect of product, with
The continuous quickening of the speed of rotation, product flotation efficiency is presented first increase after reduction trend, and with the later period speed of rotation
Quickening, the reduction trend of product suspending efficiency is getting faster.Wherein, when rotation speed is lower than 3500r/min, product is floated
Efficiency is selected to gradually increase with the quickening fiber number of the speed of rotation, and when revolving speed reaches 3550r/min, flotation efficiency highest,
When the speed of rotation is in 3600-3800r/min, the flotation efficiency of product is being gradually decreased with the quickening fiber number of heating rate,
It is reduced to 85% by 98%, when the speed of rotation is greater than 3600r/min, the flotation efficiency of product is fine with the quickening of the speed of rotation
Degree is being reduced rapidly.
(2) time of repose (as shown in Figure 2)
Time of repose refer to by completely stir after product again at a certain temperature carry out constant temperature standing, be in order to
Impurity in textile raw material is further discharged by standing.As seen from Figure 2, flotation efficiency is with time of repose
Extension and reduce.When being lower than 3 hours between upon standing, flotation efficiency, average flotation efficiency is 96%, therefore is had good
Flotation efficiency, upon standing between when extending to 3.5 hours, flotation efficiency is substantially reduced, and average flotation efficiency is 85%, works as standing
When time is greater than 4 hours, flotation efficiency is extremely low, average pore 80%, this is for tin-lead soldering, and flotation efficiency is
It is extremely low.
This is because cassiterite is also gradually precipitating with the extension of time of repose, the content of cassiterite is caused also gradually to drop
It is low.
(3) gas injection speed (as shown in Figure 3)
As seen from Figure 3, the flotation efficiency of product is reduced with the extension of gas injection speed.When gas injection speed is lower than
When 50L/min, the flotation efficiency of product is higher, average pore 96%, therefore has good flotation efficiency, when gas injection speed
When degree extends to 55L/min, flotation efficiency is substantially reduced, and average flotation efficiency is 85%, when gas injection speed is greater than 60 hours,
The flotation efficiency of product is extremely low, average pore 80%, and for tin-lead soldering, porosity has been extremely low for this.
Based on above-mentioned, it is an advantage of the current invention that the present invention is directly using cassiterite as raw material, in order to guarantee effectively returning for cassiterite
It receives, the mistake of cassiterite should be avoided to crush as far as possible in ore grinding and carries out multiple the second-order separation and screening, substantially increase same particle size
The accumulation rate of cassiterite improves pretreated first enrichment, and during carrying out collecting, utilizes stirring, standing and sky
Air bearing choosing, greatly reduces the flow time of process, improves the service efficiency of actual production, and can also carry out secondary point
Classification processing is carried out after choosing and respectively obtains cassiterite and recovered liquid, is improved the thick recovery utilization rate of drug, is reduced production cost.
The foregoing is merely illustrative of the preferred embodiments of the present invention, is not intended to limit the invention, all in essence of the invention
Made any modifications, equivalent replacements, and improvements etc., should all be included in the protection scope of the present invention within mind and principle.
Claims (4)
1. a kind of cassiterite mineralogy ore-dressing technique, specifically comprises the following steps:
The cassiterite for needing ore dressing concentration coarse grain is crushed by the broken screening of S1, cassiterite, carry out coarse grain it is broken after by shaking table into
Row grading vibration screening, and collecting respectively by size fractionated range;
Collected cassiterite is crushed by S2, preconcentration again, and the particle size range of cassiterite is 0.5-1mm after being crushed;So
Afterwards again by next stage separation by shaking table, and the tailing on shaking tables at different levels is abandoned, the thin mud of sortings at different levels is put together;
The thin mud put together after sorting is sieved by filter mud and carries out separating and filtering by S3, graded desliming, obtains crude separation screening tin
Stone;
Collectors for cassiterite is added in crude separation screening cassiterite, and activating agent is added in collectors for cassiterite by S4, cassiterite collecting
And stabilizer, strong mixing is carried out after adding reagent, is stood after strong mixing, classified filtering is carried out after standing and obtains
The filter screen mesh number of by-pass filtration liquid and secondary filtration liquid, secondary filtration is higher than primary filter mesh number;
S5, tin-lead soldering inject air into by-pass filtration liquid, and flocculant are added while injecting air, collect surface
Secondary filtration liquid is carried out high temperature concentration, puts into step S4 and be recycled after concentration by the cassiterite dross floated;
Cassiterite dross is dried and obtains cassiterite product by S6, drying forming;In the step S4, the stirring speed of strong mixing
Rate is 3600-4000r/min;Time of repose is 2-4h, and in the step S4, the collectors for cassiterite is fatty acid collecting agent
Or with one of alkyl sulfosuccinate acids, phosphonic acids and organic sequestering agent or a variety of mixtures;In the step S5, gas injection
Speed is 40-50L/min.
2. cassiterite mineralogy ore-dressing technique according to claim 1, which is characterized in that in the step S3, filtered
Hot-air seasoning is first carried out before mud, water content is lower than 20% after drying.
3. cassiterite mineralogy ore-dressing technique according to claim 1, which is characterized in that in the step S4, the activity
Agent is lead chloride, and the stabilizer is iron chloride.
4. cassiterite mineralogy ore-dressing technique according to claim 1, which is characterized in that time of repose is in the step S4
2-3 hours.
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CN102284353A (en) * | 2011-08-15 | 2011-12-21 | 大余县东宏锡制品有限公司 | Method for recovering tungsten-tin metal from ethylene-propylene terpolymerisate (APT) wastes |
CN103230831A (en) * | 2013-05-06 | 2013-08-07 | 河北联合大学 | Processing and utilizing method for extracting carbon and iron from blast furnace metallurgy dust and sludge |
CN103386375A (en) * | 2013-07-31 | 2013-11-13 | 浙江泰正钼业开发有限公司 | Molybdenum concentrate screening method |
CN105080730A (en) * | 2015-09-10 | 2015-11-25 | 刘海平 | Silicon reduction and impurity removal method for low-grade bauxite |
CN105327785A (en) * | 2015-11-16 | 2016-02-17 | 合肥万泉非金属矿科技有限公司 | Flotation technology of PPM level low-iron high-purity quartz sand |
CN205436031U (en) * | 2015-12-25 | 2016-08-10 | 辽宁东和新材料股份有限公司 | Low -grade floatation device for magnesite |
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SU706118A1 (en) * | 1978-07-06 | 1979-12-30 | Северо-Западный Политехнический Институт "Сзпи" | Jig for enriching minerals |
GB2099728A (en) * | 1981-05-21 | 1982-12-15 | Ici Australia Ltd | Recovering tin from cassiterite |
CN102172560A (en) * | 2010-12-29 | 2011-09-07 | 昆明冶金研究院 | Method for recovering tin by centrifugal concentration |
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CN103230831A (en) * | 2013-05-06 | 2013-08-07 | 河北联合大学 | Processing and utilizing method for extracting carbon and iron from blast furnace metallurgy dust and sludge |
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CN105080730A (en) * | 2015-09-10 | 2015-11-25 | 刘海平 | Silicon reduction and impurity removal method for low-grade bauxite |
CN105327785A (en) * | 2015-11-16 | 2016-02-17 | 合肥万泉非金属矿科技有限公司 | Flotation technology of PPM level low-iron high-purity quartz sand |
CN205436031U (en) * | 2015-12-25 | 2016-08-10 | 辽宁东和新材料股份有限公司 | Low -grade floatation device for magnesite |
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