CN106857695A - Plant growth regulator composition and preparation method thereof - Google Patents
Plant growth regulator composition and preparation method thereof Download PDFInfo
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- CN106857695A CN106857695A CN201611269240.7A CN201611269240A CN106857695A CN 106857695 A CN106857695 A CN 106857695A CN 201611269240 A CN201611269240 A CN 201611269240A CN 106857695 A CN106857695 A CN 106857695A
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- polypentenol
- cepha
- ethephon
- chloroethyl
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- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N31/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic oxygen or sulfur compounds
- A01N31/02—Acyclic compounds
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N57/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds
- A01N57/18—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds
- A01N57/20—Biocides, pest repellants or attractants, or plant growth regulators containing organic phosphorus compounds having phosphorus-to-carbon bonds containing acyclic or cycloaliphatic radicals
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
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- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Wood Science & Technology (AREA)
- Plant Pathology (AREA)
- Dentistry (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Biotechnology (AREA)
- Microbiology (AREA)
- Mycology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
Plant growth regulator composition, it is characterised in that be made up of following raw material and its parts by weight:Polypentenol:4.0 10.0%, ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0001 0.0005%, piroctone olamine salt:4.0 4.5%, epoxidized soybean oil:0.01 0.1%;Because polypentenol is the chemical substance of natural botanical source, to the metabolic mechanism for having correlation in human body and plant, nontoxic, environmental sound, therefore have great importance using polypentenol exploitation natural green plant growth regulator, it may have good commercial promise.
Description
Technical field
The present invention relates to crop plants growth regulator composition, more particularly, to plant growth regulator composition and
Its preparation method, belongs to agricultural chemicals development field.
Background technology
Plant growth regulator, is the class agricultural chemicals for coordinate plant growth development, including artificial synthesized with day
The compound of right plant hormone similar action and the natural phytohormone extracted from biology.
Polypentenol is also known as Polyprenol.It is isoprene unit(Isopentene group)Into the chemical combination of the most polymerizations of straight-chain
The general name of thing, is widely present in nature.Plant kingdom exists especially has the 9-23 compound of isopentene group.In animal
It is known to exist with 17-22 dolichol of isopentene group.These compounds are characterized in only have hydroxyl(α)It is different
The saturated structures of pentenyl.The microsome of mouse liver contain can glucose from UDP suction pressure to dolichol phosphate on enzyme,
Thus the polysaccharide biosynthesis system with dolichol phosphate glucose as precursor substance for synthesizing.So the physiology of polypentenol
One of function is relevant with the biosynthesis of polysaccharide.Retinol(Vitamin A)It is also the derivative of pentenol, and known and GDP
Mannose reaction becomes retinol phosphomannose.The biological conjunction that polypentenol participates in polysaccharide is more specifically demonstrated in bacterium
Into.
Plant growth regulator is organic synthesis, micro-analysis, plant physiology and biochemistry and Modern Agriculture wooden land skill
The product of various scientific and technical comprehensive developments such as cultivation.20~thirties of 20th century, find to exist in plant micro natural
Plant hormone such as ethene, 3-indolyl acetic acid and gibberellin etc., with the effect that control is grown.To the forties, start artificial
The research of synthetic analogues, develops 2,4-D, diethyl aminoethyl hexanoate successively(DA-6), CPPU, compound sodium nitrophenolate, α-polypentenol, suppression bud
Pellet etc., gradually promotes the use of, and forms a classification of agricultural chemicals(It is shown in Table).Artificial synthesized plant growth regulator is got over over more than 30 years
Come more, but because application technology is more complicated, its development is rapid not as insecticide, bactericide, herbicide, using scale also compared with
It is small.But from the point of view of the need for the agricultural modernization, plant growth regulator has very big development potentiality, hair is accelerated in the eighties
The trend of exhibition.China since the fifties production and appliable plant growth regulator.
For target plant, plant growth regulator is the non-nutritive chemical substance of external source, generally can be in plant
Interior conduction can just promote or suppress some links of its life process to site of action, with very low concentration, be allowed to meeting people
Develop the need for class.There is specific purposes per plant growth regulators, and application technology requirement is quite strict, only exists
Specific application conditions(Including extraneous factor)Under could produce specific effect to target plant.Often changing concentration will obtain
To opposite result, for example, there is facilitation at low concentrations, and then become inhibitory action in higher concentrations.Plant growth regulating
Agent has many purposes, different because of kind and target plant.For example:Control rudiment and dormancy;Hestening rooting;Promote cell elongation
And division;Control lateral bud or tiller;Control plant type(Short strong lodging-prevention);Control is bloomed or male and female sex, induces s.m.p fruit;Dredge
Flower fruit thinning, controls shedding;Control shape or the maturity period of fruit;Enhancing resistance(It is disease-resistant, drought resisting, salt resistance point, freeze proof);Enhancing absorbs
Fertilizer ability;Increase sugar or change acidity;Improve fragrance and color and luster;Promote latex or resin secretion;Disleave or urge is estimated(It is easy to
Mechanical harvesting);It is fresh-keeping etc..Certain plants growth regulator is used with high concentration just turns into herbicide, and some herbicides are low
Also growth regulating acts under concentration.
The content of the invention
For problem present in above-mentioned background technology, the invention provides plant growth regulator composition and its preparation
Method.Solved using scheme as described below.
Plant growth regulator composition, is made up of following raw material and its parts by weight:
Polypentenol:4.0-10.0%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0001-0.0005%;
Piroctone olamine salt:4.0-4.5%;
Epoxidized soybean oil:0.01-0.1%;
Preferably, the present composition contains following component (by weight):
Polypentenol:4.0-4.6%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0002%;
Piroctone olamine salt:4.17%;
Epoxidized soybean oil:0.01%.
The preparation method of wherein polypentenol is:The preparation of polypentenol:By plant leaf powder by extraction, saponification,
Washing, after drying.
The invention further relates to plant growth regulator composition preparation method, it is characterised in that the method includes following step
Suddenly:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;Said composition can promote plant root to grow.
Finally, using the effective content of liquid chromatography for measuring polypentenol, using liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Effective content, obtains Wheat plant growth regulating composition of the invention if qualified.
Specific embodiment
The present invention is further described in detail below according to embodiment.
Embodiment 1
Plant growth regulator composition, is made up of following raw material and its parts by weight:
Polypentenol:4.5%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0002%;
Piroctone olamine salt:4.17%;
Epoxidized soybean oil:0.01%.
The method comprises the following steps:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;
Finally, using the effective content of liquid chromatography for measuring polypentenol, using the effective of liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Content, obtains Wheat plant growth regulating composition of the invention if qualified.
Embodiment 2
Plant growth regulator composition, is made up of following raw material and its parts by weight:
Polypentenol:4.7%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0001%;
Piroctone olamine salt:4.1%;
Epoxidized soybean oil:0.07%;
The method comprises the following steps:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;
Finally, using the effective content of liquid chromatography for measuring polypentenol, using the effective of liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Content, obtains Wheat plant growth regulating composition of the invention if qualified.
Embodiment 3
Plant growth regulator composition, is made up of following raw material and its parts by weight:
Polypentenol:4.8%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0004%;
Piroctone olamine salt:4.1%;
Epoxidized soybean oil:0.07%;
The method comprises the following steps:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;
Finally, using the effective content of liquid chromatography for measuring polypentenol, using the effective of liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Content, obtains Wheat plant growth regulating composition of the invention if qualified.
Embodiment 4
Plant growth regulator composition, is made up of following raw material and its parts by weight:
Polypentenol:4.4%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0003%;
Piroctone olamine salt:4.2%;
Epoxidized soybean oil:0.06%;
The method comprises the following steps:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;
Finally, using the effective content of liquid chromatography for measuring polypentenol, using the effective of liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Content, obtains Wheat plant growth regulating composition of the invention if qualified.
Test example:
Selected in the same size, the wheat seed of full seed in ultra-clean aseptic working platform, is soaked with 5% NaClO solution
20min, with distilled water flushing for several times.Aseptically take out, be transferred in polypentenol sample, blank pair is made with distilled water
According to using 20mg/L IAA (heteroauxin) as positive control, each is processed as 100 seeds, if 3 repetitions;Seed soaks
After 4h, use distilled water flushing the surface of the seed, seed is fitly arranged in be placed in it is auxiliary have a glass training shape wares of 2 layers of gauze, put
Enter in illumination box, cultivated 7 days under the conditions of 25 DEG C.Observed daily during germination, kept the skin wet, record germination grain number is surveyed
Its amylase activity.Result is as shown in the table:
Described above not limitation of the present invention, the present invention is also not limited to the example above.The art it is common
In essential scope of the invention, change, remodeling, addition or the replacement made should also belong to protection of the invention to technical staff
Scope.
Claims (5)
1. plant growth regulator composition, it is characterised in that contain following raw material and its parts by weight composition:
Polypentenol:4.0-10.0%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0001-0.0005%;
Piroctone olamine salt:4.0-4.5%;
Epoxidized soybean oil:0.01-0.1%.
2. plant growth regulator composition according to claim 1, it is characterised in that preferably comprise following raw material and its
Parts by weight are constituted:
Polypentenol:4.0-4.6%;
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid:0.0002%;
Piroctone olamine salt:4.17%;
Epoxidized soybean oil:0.01%.
3. plant growth regulator composition according to claim 1, it is characterised in that the preparation method of polypentenol is:
The preparation of polypentenol:By plant leaf powder by extraction, saponification, washing, after drying.
4. plant growth regulator composition according to claim 1, it is characterised in that the method comprises the following steps:
First, 1 part of 80% polypentenol is taken by weight plus solvent that 2.5 parts of concentration is 25%, 1 part of water is added after stirring, mix
Conjunction is made the aqueous solution, after being sufficiently stirred for and fully reacting, stands, and takes out 3.75 portions of supernatants, then adds 0-7.5 parts of water, obtains
3.75-11.25 parts of piroctone olamine salt solution;
Secondly, 3 × 10-5 parts of 99.9% ethephon (CEPHA),2-(chloroethyl) phosphonic acid is taken, a little ethanol solution, stirring and dissolving is added, then adds 3.75 parts of water, obtained
Ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution;
Then, above-mentioned piroctone olamine salt solution is sufficiently mixed with ethephon (CEPHA),2-(chloroethyl) phosphonic acid ethanol solution, obtains 7.5-15.0 parts of mixing
Liquid, is subsequently adding 0.0015 part of auxiliary agent, then carries out filtering after being sufficiently stirred for;
Finally, using the effective content of liquid chromatography for measuring polypentenol, using the effective of liquid chromatography for measuring ethephon (CEPHA),2-(chloroethyl) phosphonic acid
Content, obtains Wheat plant growth regulating composition of the invention if qualified.
5. plant growth regulator composition according to claim 1, it is characterised in that application ion choosing in above-mentioned steps
Selecting property determination of electrode ethephon (CEPHA),2-(chloroethyl) phosphonic acid content.
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107114203A (en) * | 2017-07-03 | 2017-09-01 | 合肥卓畅农业科技有限公司 | A kind of grape planting process |
CN116569841A (en) * | 2023-04-24 | 2023-08-11 | 玉林师范学院 | Application of small molecular organic compound Prenol in Mo Langen-like stem root differentiation culture |
CN116602208A (en) * | 2023-04-24 | 2023-08-18 | 玉林师范学院 | Method for regenerating cymbidium sinense rhizome plants |
Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102771496A (en) * | 2012-07-26 | 2012-11-14 | 中国林业科学研究院林产化学工业研究所 | Plant growth regulator composition containing polyprenols and preparation method thereof |
CN103524589A (en) * | 2013-10-15 | 2014-01-22 | 中国林业科学研究院林产化学工业研究所 | Method for extracting and separating triterpenic acid and polyprenol from fir needle |
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2016
- 2016-12-31 CN CN201611269240.7A patent/CN106857695A/en active Pending
Patent Citations (2)
Publication number | Priority date | Publication date | Assignee | Title |
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CN102771496A (en) * | 2012-07-26 | 2012-11-14 | 中国林业科学研究院林产化学工业研究所 | Plant growth regulator composition containing polyprenols and preparation method thereof |
CN103524589A (en) * | 2013-10-15 | 2014-01-22 | 中国林业科学研究院林产化学工业研究所 | Method for extracting and separating triterpenic acid and polyprenol from fir needle |
Non-Patent Citations (1)
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107114203A (en) * | 2017-07-03 | 2017-09-01 | 合肥卓畅农业科技有限公司 | A kind of grape planting process |
CN116569841A (en) * | 2023-04-24 | 2023-08-11 | 玉林师范学院 | Application of small molecular organic compound Prenol in Mo Langen-like stem root differentiation culture |
CN116602208A (en) * | 2023-04-24 | 2023-08-18 | 玉林师范学院 | Method for regenerating cymbidium sinense rhizome plants |
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Application publication date: 20170620 |