CN106847691B - 一种整流二极管清洗方法 - Google Patents
一种整流二极管清洗方法 Download PDFInfo
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- -1 dimethyl phenyl propylene ester Chemical class 0.000 claims description 13
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- AEQDJSLRWYMAQI-UHFFFAOYSA-N 2,3,9,10-tetramethoxy-6,8,13,13a-tetrahydro-5H-isoquinolino[2,1-b]isoquinoline Chemical compound C1CN2CC(C(=C(OC)C=C3)OC)=C3CC2C2=C1C=C(OC)C(OC)=C2 AEQDJSLRWYMAQI-UHFFFAOYSA-N 0.000 claims description 11
- DHVLDKHFGIVEIP-UHFFFAOYSA-N 2-bromo-2-(bromomethyl)pentanedinitrile Chemical compound BrCC(Br)(C#N)CCC#N DHVLDKHFGIVEIP-UHFFFAOYSA-N 0.000 claims description 11
- OCOBFMZGRJOSOU-UHFFFAOYSA-N 3-o-tert-butyl 1-o-ethyl propanedioate Chemical compound CCOC(=O)CC(=O)OC(C)(C)C OCOBFMZGRJOSOU-UHFFFAOYSA-N 0.000 claims description 11
- 239000005632 Capric acid (CAS 334-48-5) Substances 0.000 claims description 11
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- 244000037364 Cinnamomum aromaticum Species 0.000 claims description 11
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 claims description 11
- IEPRKVQEAMIZSS-UHFFFAOYSA-N Di-Et ester-Fumaric acid Natural products CCOC(=O)C=CC(=O)OCC IEPRKVQEAMIZSS-UHFFFAOYSA-N 0.000 claims description 11
- IEPRKVQEAMIZSS-WAYWQWQTSA-N Diethyl maleate Chemical compound CCOC(=O)\C=C/C(=O)OCC IEPRKVQEAMIZSS-WAYWQWQTSA-N 0.000 claims description 11
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- YPJUNDFVDDCYIH-UHFFFAOYSA-N perfluorobutyric acid Chemical compound OC(=O)C(F)(F)C(F)(F)C(F)(F)F YPJUNDFVDDCYIH-UHFFFAOYSA-N 0.000 claims description 11
- 239000000176 sodium gluconate Substances 0.000 claims description 11
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- 229940005574 sodium gluconate Drugs 0.000 claims description 11
- CCEKAJIANROZEO-UHFFFAOYSA-N sulfluramid Chemical compound CCNS(=O)(=O)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)C(F)(F)F CCEKAJIANROZEO-UHFFFAOYSA-N 0.000 claims description 11
- HNXGGWNCFXZSAI-UHFFFAOYSA-N 2-morpholin-2-ylethanesulfonic acid Chemical compound OS(=O)(=O)CCC1CNCCO1 HNXGGWNCFXZSAI-UHFFFAOYSA-N 0.000 claims description 9
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- MRUAUOIMASANKQ-UHFFFAOYSA-O carboxymethyl-[3-(dodecanoylamino)propyl]-dimethylazanium Chemical compound CCCCCCCCCCCC(=O)NCCC[N+](C)(C)CC(O)=O MRUAUOIMASANKQ-UHFFFAOYSA-O 0.000 claims description 9
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- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical compound OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 claims description 8
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- 235000019301 disodium ethylene diamine tetraacetate Nutrition 0.000 claims description 6
- CMCBDXRRFKYBDG-UHFFFAOYSA-N 1-dodecoxydodecane Chemical compound CCCCCCCCCCCCOCCCCCCCCCCCC CMCBDXRRFKYBDG-UHFFFAOYSA-N 0.000 claims description 3
- LXOFYPKXCSULTL-UHFFFAOYSA-N 2,4,7,9-tetramethyldec-5-yne-4,7-diol Chemical compound CC(C)CC(C)(O)C#CC(C)(O)CC(C)C LXOFYPKXCSULTL-UHFFFAOYSA-N 0.000 claims description 3
- 239000002202 Polyethylene glycol Substances 0.000 claims description 3
- 239000004147 Sorbitan trioleate Substances 0.000 claims description 3
- PRXRUNOAOLTIEF-ADSICKODSA-N Sorbitan trioleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](OC(=O)CCCCCCC\C=C/CCCCCCCC)[C@H]1OC[C@H](O)[C@H]1OC(=O)CCCCCCC\C=C/CCCCCCCC PRXRUNOAOLTIEF-ADSICKODSA-N 0.000 claims description 3
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- 235000019337 sorbitan trioleate Nutrition 0.000 claims description 3
- 229960000391 sorbitan trioleate Drugs 0.000 claims description 3
- JOLVQSLAOYDVGN-UHFFFAOYSA-N CN(C)CC1=CC=CC=C1.CCCCCCCCCCCCCCCl Chemical compound CN(C)CC1=CC=CC=C1.CCCCCCCCCCCCCCCl JOLVQSLAOYDVGN-UHFFFAOYSA-N 0.000 claims description 2
- PHNZVRCKNCHOGA-UHFFFAOYSA-N P(=O)(O)(O)O.OCC([K])[K] Chemical compound P(=O)(O)(O)O.OCC([K])[K] PHNZVRCKNCHOGA-UHFFFAOYSA-N 0.000 claims description 2
- 229960001484 edetic acid Drugs 0.000 claims description 2
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- BDOYKFSQFYNPKF-UHFFFAOYSA-N 2-[2-[bis(carboxymethyl)amino]ethyl-(carboxymethyl)amino]acetic acid;sodium Chemical compound [Na].[Na].OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O BDOYKFSQFYNPKF-UHFFFAOYSA-N 0.000 description 3
- PUSKHXMZPOMNTQ-UHFFFAOYSA-N ethyl 2,1,3-benzoselenadiazole-5-carboxylate Chemical group CCOC(=O)C1=CC=C2N=[Se]=NC2=C1 PUSKHXMZPOMNTQ-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
- GFEYTYKRXGPQJN-UHFFFAOYSA-N [K].OCC(P(O)(O)=O)P(O)(O)=O Chemical compound [K].OCC(P(O)(O)=O)P(O)(O)=O GFEYTYKRXGPQJN-UHFFFAOYSA-N 0.000 description 1
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Abstract
本发明公开了一种整流二级管清洗方法,其特征在于，包括以下步骤：对整流二级管表面进行抛光作业，然后喷洒清洗剂一；喷洒清洗剂一后静置30‑40min,然后将整流二级管送入装有清洗剂二的清洗池中进行清洗，清洗温度为35‑40℃;取出清洗池中的整流二级管，干燥，即可。本发明整流二级管清洗方法，先通过清洗剂一喷洒到元件表面，对表面的杂质、污渍进行初步分散，然后再通过清洗剂二进行彻底清洗。通过该方法，清洗彻底，且不会对元件本身产生不利影响。
Description
技术领域
本发明涉及一种整流二极管清洗方法，属于电子元器件清洗领域。
背景技术
整流二极管是一种将交流电能转变为直流电能的半导体器件。通常它包含一个PN结，有正极和负极两个端子。二极管最重要的特性就是单方向导电性。在电路中，电流只能从二极管的正极流入，负极流出。在整流二极管过程中，由于各种外在原因，使得其表面会有污渍，需要对其进行清洗，以使其达到产品的合格。
发明内容
本发明目的是提供一种整流二极管清洗方法，可以将整流二极管外表面的杂质颗粒、污渍清洗干净，同时还对整流二极管本身产生不利影响。
本发明的方案如下：一种整流二极管清洗方法,包括以下步骤：
步骤一：对整流二极管表面进行抛光作业，然后喷洒清洗剂一；
所述的清洗剂一由质量比为0.3：0.62：0.34：500的木质素磺酸钠、山梨醇酐三油酸酯、聚乙二醇单月桂醚、去离子水混合而成；
步骤二：喷洒清洗剂一后静置30-40min,然后将整流二极管送入装有清洗剂二的清洗池中进行清洗，清洗温度为35-40℃；
所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇18-26份、苄基二甲基四癸基氯化铵9-14份、癸酸6-10份、甲壳素25-29份、叔丁基丙二酸乙酯6-10份、亚麻酸甲酯5-9份、桂皮油45-55份、七氟丁酸6-10份、二甲基苯基丙烯酯22-28份、2-吗啉乙磺酸9-14份、溴菌腈10-18份、N-乙基全氟辛基磺酰胺乙醇6-18份、2-十一酮10-14份、乙二胺四乙酸二钠16-24份、月桂酰胺丙基甜菜碱26-30份、马来酸二乙酯5-9份、葡萄糖酸钠14-19份、羟基乙叉二膦酸钾10-15份、去离子水14000-15000份；
步骤三：取出清洗池中的整流二极管，干燥，即可。
进一步，所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇22份、苄基二甲基四癸基氯化铵10份、癸酸8份、甲壳素28份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份、桂皮油46份、七氟丁酸9份、二甲基苯基丙烯酯26份、2-吗啉乙磺酸10份、溴菌腈14份、N-乙基全氟辛基磺酰胺乙醇9份、2-十一酮12份、乙二胺四乙酸二钠18份、月桂酰胺丙基甜菜碱29份、马来酸二乙酯6份、葡萄糖酸钠16份、羟基乙叉二膦酸钾12份、去离子水14800份。
进一步，所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇25份、苄基二甲基四癸基氯化铵10份、癸酸9份、甲壳素26份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份、桂皮油52份、七氟丁酸9份、二甲基苯基丙烯酯24份、2-吗啉乙磺酸10份、溴菌腈16份、N-乙基全氟辛基磺酰胺乙醇9份、2-十一酮14份、乙二胺四乙酸二钠22份、月桂酰胺丙基甜菜碱28份、马来酸二乙酯8份、葡萄糖酸钠14份、羟基乙叉二膦酸钾11份、去离子水14600份。
进一步，所述的清洗剂二的制备方法如下：
步骤一、将四甲基癸炔二醇、苄基二甲基四癸基氯化铵、癸酸、桂皮油、七氟丁酸、二甲基苯基丙烯酯、溴菌腈、2-十一酮、乙二胺四乙酸二钠、马来酸二乙酯、羟基乙叉二膦酸钾加入到去离子水中，然后进行超声波分散；分散时间为1-2h，分散速度为4000-4500r/min,超声波频率为30-35KHz；
步骤二、接着加入甲壳素、叔丁基丙二酸乙酯、亚麻酸甲酯，然后进行超声波分散；分散时间为30-40min，分散速度为3000-4000r/min,超声波频率为35-40KHz；
步骤三、接着加入N-乙基全氟辛基磺酰胺乙醇、葡萄糖酸钠，然后进行超声波分散；分散时间为20-30min，分散速度为4000-5000r/min,超声波频率为40-50KHz；
步骤四、接着加入余料，然后进行超声波分散；分散时间为20-30min，分散速度为5000-6000r/min,超声波频率为40-45KHz；
步骤五，即得。
本发明整流二极管清洗方法，先通过清洗剂一喷洒到元件表面，对表面的杂质、污渍进行初步分散，然后再通过清洗剂二进行彻底清洗。通过该方法，清洗彻底，且不会对元件本身产生不利影响。
具体实施方式
实施例1
一种整流二极管清洗方法,包括以下步骤：
步骤一：对整流二极管表面进行抛光作业，然后喷洒清洗剂一；清洗剂一由质量比为0.3：0.62：0.34：500的木质素磺酸钠、山梨醇酐三油酸酯、聚乙二醇单月桂醚、去离子水混合而成；
步骤二：喷洒清洗剂一后静置30-40min,然后将整流二极管送入装有清洗剂二的清洗池中进行清洗，清洗温度为35-40℃；
步骤三：取出清洗池中的整流二极管，干燥，即可。
清洗剂二的制备方法如下：
步骤一、将四甲基癸炔二醇22份、苄基二甲基四癸基氯化铵10份、癸酸8份、桂皮油46份、七氟丁酸9份、二甲基苯基丙烯酯26份、溴菌腈14份、2-十一酮12份、乙二胺四乙酸二钠18份、马来酸二乙酯6份、羟基乙叉二膦酸钾12份加入到去离子水14800份中，然后进行超声波分散；分散时间为1.3h，分散速度为4600r/min,超声波频率为32KHz；
步骤二、接着加入甲壳素28份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份，然后进行超声波分散；分散时间为33min，分散速度为3700r/min,超声波频率为38KHz；
步骤三、接着加入N-乙基全氟辛基磺酰胺乙醇9份、葡萄糖酸钠16份，然后进行超声波分散；分散时间为25min，分散速度为4500r/min,超声波频率为43KHz；
步骤四、接着加入2-吗啉乙磺酸10份、月桂酰胺丙基甜菜碱29份，然后进行超声波分散；分散时间为22min，分散速度为5400r/min,超声波频率为40KHz；
步骤五，即得。
实施例2
与实施例1区别处在于，清洗剂二的制备方法如下：
步骤一、将四甲基癸炔二醇25份、苄基二甲基四癸基氯化铵10份、癸酸9份、桂皮油52份、七氟丁酸9份、二甲基苯基丙烯酯24份、溴菌腈16份、2-十一酮14份、乙二胺四乙酸二钠22份、马来酸二乙酯8份、羟基乙叉二膦酸钾11份加入到去离子水14600份中，然后进行超声波分散；分散时间为2h，分散速度为4300r/min,超声波频率为31KHz；
步骤二、接着加入甲壳素26份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份，然后进行超声波分散；分散时间为36min，分散速度为3600r/min,超声波频率为31KHz；
步骤三、接着加入N-乙基全氟辛基磺酰胺乙醇9份、葡萄糖酸钠14份，然后进行超声波分散；分散时间为27min，分散速度为4400r/min,超声波频率为46KHz；
步骤四、接着加入2-吗啉乙磺酸10份、月桂酰胺丙基甜菜碱28份，然后进行超声波分散；分散时间为28min，分散速度为5900r/min,超声波频率为40KHz；
步骤五，即得。
实施例3
与实施例1区别处在于，清洗剂二的制备方法如下：
步骤一、将四四甲基癸炔二醇18份、苄基二甲基四癸基氯化铵10份、癸酸9份、桂皮油48份、七氟丁酸9份、二甲基苯基丙烯酯25份、溴菌腈13份、2-十一酮12份、乙二胺四乙酸二钠19份、马来酸二乙酯8份、羟基乙叉二膦酸钾10份加入到去离子水14200份中，然后进行超声波分散；分散时间为1-2h，分散速度为4000-4500r/min,超声波频率为30-35KHz；
步骤二、接着加入甲壳素26份、叔丁基丙二酸乙酯8份、亚麻酸甲酯6份、然后进行超声波分散；分散时间为30-40min，分散速度为3000-4000r/min,超声波频率为35-40KHz；
步骤三、接着加入N-乙基全氟辛基磺酰胺乙醇7份、葡萄糖酸钠18份，然后进行超声波分散；分散时间为20-30min，分散速度为4000-5000r/min,超声波频率为40-50KHz；
步骤四、接着加入2-吗啉乙磺酸11份、月桂酰胺丙基甜菜碱27份，然后进行超声波分散；分散时间为20-30min，分散速度为5000-6000r/min,超声波频率为40-45KHz；
步骤五，即得。
使用实施例1-3的清洗方法对整流二极管进行清洗效果试验。结果如下：
| 实施例1 | 实施例2 | 实施例3 | 常规清洗液 | |
| 清洗效果（总分5份） | 4.8分 | 4.9分 | 4.8分 | 4.2分 |
| 清洗后外观 | 明亮，无积液 | 明亮，无积液 | 明亮，无积液 | 有少许积液 |
尽管上文对本发明的具体实施方式给予了详细描述和说明，但是应该指明的是，我们可以依据本发明的构想对上述实施方式进行各种等效改变和修改，其所产生的功能作用仍未超出说明书所涵盖的精神时，均应在本发明的保护范围之内。
Claims (4)
1.一种整流二极管清洗方法,其特征在于，包括以下步骤：
步骤一：对整流二极管表面进行抛光作业，然后喷洒清洗剂一；
所述的清洗剂一由质量比为0.3：0.62：0.34：500的木质素磺酸钠、山梨醇酐三油酸酯、聚乙二醇单月桂醚、去离子水混合而成；
步骤二：喷洒清洗剂一后静置30-40min,然后将整流二极管送入装有清洗剂二的清洗池中进行清洗，清洗温度为35-40℃；
所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇18-26份、苄基二甲基四癸基氯化铵9-14份、癸酸6-10份、甲壳素25-29份、叔丁基丙二酸乙酯6-10份、亚麻酸甲酯5-9份、桂皮油45-55份、七氟丁酸6-10份、二甲基苯基丙烯酯22-28份、2-吗啉乙磺酸9-14份、溴菌腈10-18份、N-乙基全氟辛基磺酰胺乙醇6-18份、2-十一酮10-14份、乙二胺四乙酸二钠16-24份、月桂酰胺丙基甜菜碱26-30份、马来酸二乙酯5-9份、葡萄糖酸钠14-19份、羟基乙叉二膦酸钾10-15份、去离子水14000-15000份；
步骤三：取出清洗池中的整流二极管，干燥，即可。
2.根据权利要求1所述的一种整流二极管清洗方法,其特征在于，所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇22份、苄基二甲基四癸基氯化铵10份、癸酸8份、甲壳素28份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份、桂皮油46份、七氟丁酸9份、二甲基苯基丙烯酯26份、2-吗啉乙磺酸10份、溴菌腈14份、N-乙基全氟辛基磺酰胺乙醇9份、2-十一酮12份、乙二胺四乙酸二钠18份、月桂酰胺丙基甜菜碱29份、马来酸二乙酯6份、葡萄糖酸钠16份、羟基乙叉二膦酸钾12份、去离子水14800份。
3.根据权利要求1所述的一种整流二极管清洗方法,其特征在于，所述的清洗剂二由以下重量份组分制得：四甲基癸炔二醇25份、苄基二甲基四癸基氯化铵10份、癸酸9份、甲壳素26份、叔丁基丙二酸乙酯7份、亚麻酸甲酯8份、桂皮油52份、七氟丁酸9份、二甲基苯基丙烯酯24份、2-吗啉乙磺酸10份、溴菌腈16份、N-乙基全氟辛基磺酰胺乙醇9份、2-十一酮14份、乙二胺四乙酸二钠22份、月桂酰胺丙基甜菜碱28份、马来酸二乙酯8份、葡萄糖酸钠14份、羟基乙叉二膦酸钾11份、去离子水14600份。
4.根据权利要求1所述的一种整流二极管清洗方法,其特征在于，所述的清洗剂二的制备方法如下：
步骤一、将四甲基癸炔二醇、苄基二甲基四癸基氯化铵、癸酸、桂皮油、七氟丁酸、二甲基苯基丙烯酯、溴菌腈、2-十一酮、乙二胺四乙酸二钠、马来酸二乙酯、羟基乙叉二膦酸钾加入到去离子水中，然后进行超声波分散；分散时间为1-2h，分散速度为4000-4500r/min,超声波频率为30-35KHz；
步骤二、接着加入甲壳素、叔丁基丙二酸乙酯、亚麻酸甲酯，然后进行超声波分散；分散时间为30-40min，分散速度为3000-4000r/min,超声波频率为35-40KHz；
步骤三、接着加入N-乙基全氟辛基磺酰胺乙醇、葡萄糖酸钠，然后进行超声波分散；分散时间为20-30min，分散速度为4000-5000r/min,超声波频率为40-50KHz；
步骤四、接着加入余料，然后进行超声波分散；分散时间为20-30min，分散速度为5000-6000r/min,超声波频率为40-45KHz；
步骤五，即得。
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Denomination of invention: A Cleaning Method for Rectifier Diodes Effective date of registration: 20230821 Granted publication date: 20200522 Pledgee: CITIC financing Company Limited by Guarantee in Dongzhi County Pledgor: ANHUI ZHAOLI OPTO-ELECTRONICS TECHNOLOGY Co.,Ltd. Registration number: Y2023980053091 |