CN106835856A - A kind of preparation method of the wallpaper with air-cleaning function - Google Patents
A kind of preparation method of the wallpaper with air-cleaning function Download PDFInfo
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- CN106835856A CN106835856A CN201611221150.0A CN201611221150A CN106835856A CN 106835856 A CN106835856 A CN 106835856A CN 201611221150 A CN201611221150 A CN 201611221150A CN 106835856 A CN106835856 A CN 106835856A
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- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H27/00—Special paper not otherwise provided for, e.g. made by multi-step processes
- D21H27/18—Paper- or board-based structures for surface covering
- D21H27/20—Flexible structures being applied by the user, e.g. wallpaper
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
- D21H17/25—Cellulose
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/21—Macromolecular organic compounds of natural origin; Derivatives thereof
- D21H17/24—Polysaccharides
- D21H17/25—Cellulose
- D21H17/26—Ethers thereof
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/20—Macromolecular organic compounds
- D21H17/33—Synthetic macromolecular compounds
- D21H17/34—Synthetic macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
- D21H17/36—Polyalkenyalcohols; Polyalkenylethers; Polyalkenylesters
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/675—Oxides, hydroxides or carbonates
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H17/00—Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
- D21H17/63—Inorganic compounds
- D21H17/67—Water-insoluble compounds, e.g. fillers, pigments
- D21H17/68—Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
-
- D—TEXTILES; PAPER
- D21—PAPER-MAKING; PRODUCTION OF CELLULOSE
- D21H—PULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
- D21H25/00—After-treatment of paper not provided for in groups D21H17/00 - D21H23/00
- D21H25/04—Physical treatment, e.g. heating, irradiating
- D21H25/06—Physical treatment, e.g. heating, irradiating of impregnated or coated paper
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Paper (AREA)
- Synthetic Leather, Interior Materials Or Flexible Sheet Materials (AREA)
Abstract
The invention discloses a kind of preparation method of the wallpaper with air-cleaning function, belong to technical field of wallpaper.The present invention prepares nano titanium oxide by titanium source of butyl titanate, again with tetraethyl orthosilicate as silicon source, form nano-silica film and be coated on nano titanium oxide surface, by it, grinding is configured to coating liquid with diatomite, tourmaline, polyvinyl alcohol etc. again, the wallpaper with air-cleaning function can be obtained after coating liquid finally is coated in into non-woven paper surface, then embossing drying.The present invention is by the use of diatomite, cellulose ether and wood-fibred etc. as the matrix of coating liquid, the free formaldehyde in air can efficiently be adsorbed, the anion for being generated by modified nano-titanium dioxide and tourmaline again is catalytically decomposed to reach the purpose removed formaldehyde and purify the air of a room.
Description
Technical field
The invention discloses a kind of preparation method of the wallpaper with air-cleaning function, belong to technical field of wallpaper.
Background technology
Wallpaper, is a kind of quite extensive indoor hardware fitting of application.Because it has color various, pattern enriches, luxurious
The characteristics of various other house decorative materials institutes such as style, safety and environmental protection, easy construction, affordable are incomparable, therefore in Europe
The developed countries and regions such as U.S., Southeast Asia, Japan obtain considerable degree of popularization.In recent years, China's indoor decorating continues
Heat up, the wallpaper being once given the cold shoulder has been come into parlor, bedroom, hotel, meeting room etc., got over again with its gorgeous new attitude
It is widely applied to get over.With going deep into for application, people are more and more stronger to the individual demand of wallpaper decorative effect, especially
The three-dimensional, wallpaper of simulated decorative effect.
In the past, wallpaper came into the life of people as just a kind of decorative material, and people require it many in dicoration
Above aesthetic property, with the development and the continuous improvement of people's living standard of social economy, people are to indoor fitting-up
It is required that also gradually stepping up.People need the wallpaper of high-quality to decorate the life of oneself, so to other features of wallpaper
It is required that also more and more.While pursuing attractive in appearance, it is also desirable to which interior wall wallpaper material can embody certain function and personalization is chased after
Ask.And existing wallpaper is generally polyvinyl chloride product, polyvinyl chloride glue surface wallpaper is to currently use widest one kind.Simple point
Say, exactly polyvinyl chloride is equably coated in body paper surface, constitute glue surface wallpaper.It is that cannot exclude formaldehyde in this kind of wallpaper
, it is primarily due to body paper and is possible to contain formaldehyde in itself.And body paper is made up of wood pulp cellulose, the feature of environmental protection is dependent on wood
Slurry is using pure natural wood pulp or chemical wood pulp.In addition, also containing a kind of nuisance in pvc coating in fact
Matter --- monomeric vinyl chloride.Under home state, the chlorine contained by it will not produce harm to people.Only it is in the condition of high temperature
During generation fire, can just decompose it is free produce chlorine, such as content overproof will then make one to be choked to death, it is impossible to escape.
The content of the invention
The technical problems to be solved by the invention：For, containing the harmful substance such as formaldehyde, and cannot being excluded in conventional wallpaper
The defect of formaldehyde, the present invention improves a kind of preparation method of the wallpaper with air-cleaning function, and the present invention is with the fourth of metatitanic acid four
Ester prepares nano titanium oxide for titanium source, then with tetraethyl orthosilicate as silicon source, forms nano-silica film and be coated on nanometer two
Titania surface, then grinding is configured to film slurries with diatomite, tourmaline, polyvinyl alcohol etc. by it, finally by film slurries
The wallpaper with air-cleaning function can be obtained after being coated in non-woven paper surface, then embossing drying.The present invention utilizes diatom
Soil, cellulose ether and wood-fibred etc. can efficiently adsorb the free formaldehyde in air, then pass through as the matrix of film slurries
Modified nano-titanium dioxide and the anion of tourmaline generation are catalytically decomposed to reach the mesh removed formaldehyde and purify the air of a room
's.
In order to solve the above technical problems, the present invention is using technical scheme as described below：
（1）20~24mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and 10 are added dropwise with 1~2mL/min in solution
~12mL butyl titanates, 30~40min is stirred after completion of dropping with 500~600r/min, is subsequently added the positive silicic acid of 1~3mL
Ethyl ester, 20~30mL absolute ethyl alcohols, 20~30mL mass fractions are 1% hydrochloric acid, continue to stir 1~2h, obtain mixed liquor；
（2）Above-mentioned mixed liquor is aged 8~12h, then filtering, is washed with deionized filter residue 3~5 times, then filter residue is inserted
In drying box, 3~5h is dried at 80~90 DEG C, dried filter residue is placed in Muffle furnace, 2 are calcined at 550~600 DEG C
~3h, after being cooled to room temperature, is transferred to 1~2h of ball milling in ball mill, obtains modified nano-titanium dioxide；
（3）Count by weight, weigh 5~10 parts of diatomite, 2~3 parts of polyvinyl alcohol, 0.5~1.0 part of cellulose ether, 0.5~
1.0 parts of wood-fibreds, 2~3 parts of tourmaline, 5~8 parts of above-mentioned modified nano-titanium dioxides, 20~30 parts of deionized waters load horizontal
In sand mill, with 800~1000r/min, 2~3h of grinding distribution, film slurries are obtained；
（4）10m × 53cm thickness is taken for 0.15~0.20mm non-woven papers, and non-woven paper surface is coated in above-mentioned film slurries,
Coating thickness is 0.01~0.03mm, then suppresses a layer thickness successively for 0.02~0.03mm patterns in film coated surface with graining roll
Layer and embossed layers, are subsequently placed in drying box, and 3~5h is dried at 50~60 DEG C, obtain the wallpaper with air-cleaning function.
Application process of the invention is：Metope is polished flat with sand paper first, and removes floating ash, it is then uniform on the wall to apply
The moistureproof basement membrane of one layer of brush, after spontaneously drying 15~24h, wallpaper glue is uniformly brushed to whole metope, and then the present invention is obtained
The wallpaper with air-cleaning function it is smooth be affixed on metope, and, from left to right, wallpaper is scraped with scraper plate from top to bottom
It is flat, and door and window is closed, dry in the shade 36~48h naturally.After testing, using the present invention obtained by with air-cleaning function
Wallpaper after using 48~60h formaldehyde elimination factor reach 99.4%~99.9%, and with antibacterial, it is mould proof, safely, eliminate the unusual smell it
Special efficacy.
Compared with other method, Advantageous Effects are the present invention：
（1）The wallpaper with air-cleaning function obtained by the present invention can be by the innoxious decomposition of the pernicious gases such as formaldehyde, and tool
There is the effect of sterilizing；
（2）The wallpaper with air-cleaning function obtained by the present invention can also solve room air dirty to user's non-hazardous
The problem of dye, for people provide a more preferable living environment.
Specific embodiment
20~24mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and 10 are added dropwise with 1~2mL/min in solution
~12mL butyl titanates, 30~40min is stirred after completion of dropping with 500~600r/min, is subsequently added the positive silicic acid of 1~3mL
Ethyl ester, 20~30mL absolute ethyl alcohols, 20~30mL mass fractions are 1% hydrochloric acid, continue to stir 1~2h, obtain mixed liquor；Will be above-mentioned
Mixed liquor is aged 8~12h, and then filtering, is washed with deionized filter residue 3~5 times, then filter residue is inserted in drying box, 80
3~5h is dried at~90 DEG C, dried filter residue is placed in Muffle furnace, 2~3h is calcined at 550~600 DEG C, be cooled to room
Wen Hou, is transferred to 1~2h of ball milling in ball mill, obtains modified nano-titanium dioxide；Count by weight, weigh 5~10 parts of diatomite,
2~3 parts of polyvinyl alcohol, 0.5~1.0 part of cellulose ether, 0.5~1.0 part of wood-fibred, 2~3 parts of tourmaline, 5~8 parts above-mentioned to change
Property nano titanium oxide, 20~30 parts of deionized waters are fitted into horizontal sand mill, with 800~1000r/min grinding distributions 2~
3h, obtains film slurries；10m × 53cm thickness is taken for 0.15~0.20mm non-woven papers, and nonwoven is coated in above-mentioned film slurries
Paper surface, coating thickness is 0.01~0.03mm, then with graining roll film coated surface suppress successively a layer thickness for 0.02~
0.03mm patterned layers and embossed layers, are subsequently placed in drying box, and 3~5h is dried at 50~60 DEG C, are obtained with purification of air work(
The wallpaper of energy.
Example 1
20mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and the fourth of 10mL metatitanic acids four is added dropwise with 1mL/min in solution
Ester, 30min is stirred after completion of dropping with 500r/min, is subsequently added 1mL tetraethyl orthosilicates, 20mL absolute ethyl alcohols, 20mL mass
Fraction is 1% hydrochloric acid, continues to stir 1h, obtains mixed liquor；Above-mentioned mixed liquor is aged 8h, then filtering, is washed with deionized filter
Slag 3 times, then filter residue is inserted in drying box, 3h is dried at 80 DEG C, dried filter residue is placed in Muffle furnace, at 550 DEG C
Lower calcining 2h, after being cooled to room temperature, is transferred to ball milling 1h in ball mill, obtains modified nano-titanium dioxide；Count by weight, weigh
5 parts of diatomite, 2 parts of polyvinyl alcohol, 0.5 part of cellulose ether, 0.5 part of wood-fibred, 2 parts of tourmaline, 5 parts of above-mentioned modified nano-silicas
Change titanium, 20 parts of deionized waters are fitted into horizontal sand mill, with 800r/min grinding distribution 2h, obtain film slurries；Take 10m ×
53cm thickness is 0.15mm non-woven papers, and is coated in non-woven paper surface with above-mentioned film slurries, and coating thickness is 0.01mm, then is used
Graining roll suppresses a layer thickness for 0.02mm patterned layers and embossed layers successively in film coated surface, is subsequently placed in drying box, 50
3h is dried at DEG C, the wallpaper with air-cleaning function is obtained.
Metope is polished flat with sand paper first, and removes floating ash, one layer of moistureproof basement membrane is then uniformly brushed on the wall, it is natural
After drying 15h, wallpaper glue is uniformly brushed to whole metope, then by the wallpaper with air-cleaning function obtained in the present invention
Smooth is affixed on metope, and, from left to right, wallpaper is struck off with scraper plate from top to bottom, and door and window is closed, and is dried in the shade naturally
36h.After testing, the formaldehyde elimination factor after using 48h of the wallpaper with air-cleaning function obtained by the present invention is being used
Reach 99.4%, and with antibacterial, it is mould proof, safely, the special efficacy that eliminates the unusual smell.
Example 2
24mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and the fourth of 12mL metatitanic acids four is added dropwise with 2mL/min in solution
Ester, 40min is stirred after completion of dropping with 600r/min, is subsequently added 3mL tetraethyl orthosilicates, 30mL absolute ethyl alcohols, 30mL mass
Fraction is 1% hydrochloric acid, continues to stir 2h, obtains mixed liquor；Above-mentioned mixed liquor is aged 12h, then filtering, is washed with deionized
Filter residue 5 times, then filter residue is inserted in drying box, 5h is dried at 90 DEG C, dried filter residue is placed in Muffle furnace, 600
3h is calcined at DEG C, after being cooled to room temperature, ball milling 2h in ball mill is transferred to, modified nano-titanium dioxide is obtained；Count by weight, claim
Take 10 parts of diatomite, 3 parts of polyvinyl alcohol, 1.0 parts of cellulose ethers, 1.0 parts of wood-fibreds, 3 parts of tourmaline, 8 parts of above-mentioned modified Nanos
Titanium dioxide, 30 parts of deionized waters, is fitted into horizontal sand mill, with 1000r/min grinding distribution 3h, obtains film slurries；Take 10m
× 53cm thickness is 0.20mm non-woven papers, and is coated in non-woven paper surface with above-mentioned film slurries, and coating thickness is 0.03mm, then
It is 0.03mm patterned layers and embossed layers to suppress a layer thickness successively in film coated surface with graining roll, is subsequently placed in drying box,
5h is dried at 60 DEG C, the wallpaper with air-cleaning function is obtained.
Metope is polished flat with sand paper first, and removes floating ash, one layer of moistureproof basement membrane is then uniformly brushed on the wall, it is natural
After drying 24h, wallpaper glue is uniformly brushed to whole metope, then by the wallpaper with air-cleaning function obtained in the present invention
Smooth is affixed on metope, and, from left to right, wallpaper is struck off with scraper plate from top to bottom, and door and window is closed, and is dried in the shade naturally
48h.After testing, the formaldehyde elimination factor after using 60h of the wallpaper with air-cleaning function obtained by the present invention is being used
Reach 99.9%, and with antibacterial, it is mould proof, safely, the special efficacy that eliminates the unusual smell.
Example 3
22mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and the fourth of 11mL metatitanic acids four is added dropwise with 2mL/min in solution
Ester, 35min is stirred after completion of dropping with 550r/min, is subsequently added 2mL tetraethyl orthosilicates, 25mL absolute ethyl alcohols, 25mL mass
Fraction is 1% hydrochloric acid, continues to stir 2h, obtains mixed liquor；Above-mentioned mixed liquor is aged 10h, then filtering, is washed with deionized
Filter residue 4 times, then filter residue is inserted in drying box, 4h is dried at 85 DEG C, dried filter residue is placed in Muffle furnace, 575
2h is calcined at DEG C, after being cooled to room temperature, ball milling 1h in ball mill is transferred to, modified nano-titanium dioxide is obtained；Count by weight, claim
Take 7 parts of diatomite, 2 parts of polyvinyl alcohol, 0.8 part of cellulose ether, 0.8 part of wood-fibred, 2 parts of tourmaline, 6 parts of above-mentioned modified Nanos two
Titanium oxide, 25 parts of deionized waters, is fitted into horizontal sand mill, with 900r/min grinding distribution 2h, obtains film slurries；Take 10m ×
53cm thickness is 0.18mm non-woven papers, and is coated in non-woven paper surface with above-mentioned film slurries, and coating thickness is 0.02mm, then is used
Graining roll suppresses a layer thickness for 0.02mm patterned layers and embossed layers successively in film coated surface, is subsequently placed in drying box, 55
4h is dried at DEG C, the wallpaper with air-cleaning function is obtained.
Metope is polished flat with sand paper first, and removes floating ash, one layer of moistureproof basement membrane is then uniformly brushed on the wall, it is natural
After drying 20h, wallpaper glue is uniformly brushed to whole metope, then by the wallpaper with air-cleaning function obtained in the present invention
Smooth is affixed on metope, and, from left to right, wallpaper is struck off with scraper plate from top to bottom, and door and window is closed, and is dried in the shade naturally
42h.After testing, the formaldehyde elimination factor after using 44h of the wallpaper with air-cleaning function obtained by the present invention is being used
Reach 99.7%, and with antibacterial, it is mould proof, safely, the special efficacy that eliminates the unusual smell.
Claims (1)
1. a kind of preparation method of the wallpaper with air-cleaning function, it is characterised in that specific preparation process is：
（1）20~24mL mass fractions are measured for 5% acetylacetone,2,4-pentanedione ethanol solution, and 10 are added dropwise with 1~2mL/min in solution
~12mL butyl titanates, 30~40min is stirred after completion of dropping with 500~600r/min, is subsequently added the positive silicic acid of 1~3mL
Ethyl ester, 20~30mL absolute ethyl alcohols, 20~30mL mass fractions are 1% hydrochloric acid, continue to stir 1~2h, obtain mixed liquor；
（2）Above-mentioned mixed liquor is aged 8~12h, then filtering, is washed with deionized filter residue 3~5 times, then filter residue is inserted
In drying box, 3~5h is dried at 80~90 DEG C, dried filter residue is placed in Muffle furnace, 2 are calcined at 550~600 DEG C
~3h, after being cooled to room temperature, is transferred to 1~2h of ball milling in ball mill, obtains modified nano-titanium dioxide；
（3）Count by weight, weigh 5~10 parts of diatomite, 2~3 parts of polyvinyl alcohol, 0.5~1.0 part of cellulose ether, 0.5~
1.0 parts of wood-fibreds, 2~3 parts of tourmaline, 5~8 parts of above-mentioned modified nano-titanium dioxides, 20~30 parts of deionized waters load horizontal
In sand mill, with 800~1000r/min, 2~3h of grinding distribution, film slurries are obtained；
（4）10m × 53cm thickness is taken for 0.15~0.20mm non-woven papers, and non-woven paper surface is coated in above-mentioned film slurries,
Coating thickness is 0.01~0.03mm, then suppresses a layer thickness successively for 0.02~0.03mm patterns in film coated surface with graining roll
Layer and embossed layers, are subsequently placed in drying box, and 3~5h is dried at 50~60 DEG C, obtain the wallpaper with air-cleaning function.
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN107433185A (en) * | 2017-09-05 | 2017-12-05 | 霍邱金木鱼农业科技有限公司 | A kind of material for air purification and preparation method thereof |
| CN107497414A (en) * | 2017-09-07 | 2017-12-22 | 吉林化工学院 | A kind of TiO2The preparation method of/diatomite composite material |
| CN107537451A (en) * | 2017-09-05 | 2018-01-05 | 霍邱金木鱼农业科技有限公司 | A kind of porous zeolite material for air purification and preparation method thereof |
| CN107974109A (en) * | 2017-11-28 | 2018-05-01 | 马鞍山蓝科再制造技术有限公司 | A kind of preparation method of hot spray coating |
| CN108018745A (en) * | 2017-12-11 | 2018-05-11 | 许水仙 | A kind of preparation method of high anti-bacterial wear-resisting wallpaper |
| CN108359290A (en) * | 2018-04-04 | 2018-08-03 | 江苏新亿源环保科技有限公司 | A kind of preparation method of diatom ooze coating |
| CN108837815A (en) * | 2018-07-11 | 2018-11-20 | 合肥帧讯低温科技有限公司 | Material with air purification function and preparation method thereof |
| CN108976501A (en) * | 2018-07-22 | 2018-12-11 | 南京市雨花台区绿宝工业设计服务中心 | A kind of wallpaper material and preparation method thereof with air-cleaning function |
| CN108978335A (en) * | 2018-07-25 | 2018-12-11 | 邹德琨 | A kind of photocatalyst is dispelled formaldehyde wallpaper |
| CN110128905A (en) * | 2019-05-30 | 2019-08-16 | 黎明职业大学 | A kind of fiber base decorative material for wall surface |
| CN110467902A (en) * | 2019-08-02 | 2019-11-19 | 上海嗣高新材料科技有限公司 | A kind of marine fireproof sealant and preparation method thereof |
| CN110671655A (en) * | 2019-09-02 | 2020-01-10 | 施骏涛 | Multifunctional lamp for classroom and lighting system thereof |
| CN111155731A (en) * | 2019-12-25 | 2020-05-15 | 安徽赛驰通讯科技有限公司 | Non-woven wallpaper capable of purifying indoor air and preparation method thereof |
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Application publication date: 20170613 |