CN106835816A - A kind of disinfecting tissue - Google Patents

A kind of disinfecting tissue Download PDF

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Publication number
CN106835816A
CN106835816A CN201611252526.4A CN201611252526A CN106835816A CN 106835816 A CN106835816 A CN 106835816A CN 201611252526 A CN201611252526 A CN 201611252526A CN 106835816 A CN106835816 A CN 106835816A
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CN
China
Prior art keywords
pulp
antibacterial agent
drying
tissue
potent antibacterial
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201611252526.4A
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Chinese (zh)
Inventor
许亦南
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
ANHUI BILUN LIVING PAPER Co Ltd
Original Assignee
ANHUI BILUN LIVING PAPER Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by ANHUI BILUN LIVING PAPER Co Ltd filed Critical ANHUI BILUN LIVING PAPER Co Ltd
Priority to CN201611252526.4A priority Critical patent/CN106835816A/en
Publication of CN106835816A publication Critical patent/CN106835816A/en
Pending legal-status Critical Current

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Classifications

    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H15/00Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution
    • D21H15/02Pulp or paper, comprising fibres or web-forming material characterised by features other than their chemical constitution characterised by configuration
    • D21H15/10Composite fibres
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H11/00Pulp or paper, comprising cellulose or lignocellulose fibres of natural origin only
    • D21H11/12Pulp from non-woody plants or crops, e.g. cotton, flax, straw, bagasse
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H17/00Non-fibrous material added to the pulp, characterised by its constitution; Paper-impregnating material characterised by its constitution
    • D21H17/63Inorganic compounds
    • D21H17/67Water-insoluble compounds, e.g. fillers, pigments
    • D21H17/68Water-insoluble compounds, e.g. fillers, pigments siliceous, e.g. clays
    • DTEXTILES; PAPER
    • D21PAPER-MAKING; PRODUCTION OF CELLULOSE
    • D21HPULP COMPOSITIONS; PREPARATION THEREOF NOT COVERED BY SUBCLASSES D21C OR D21D; IMPREGNATING OR COATING OF PAPER; TREATMENT OF FINISHED PAPER NOT COVERED BY CLASS B31 OR SUBCLASS D21G; PAPER NOT OTHERWISE PROVIDED FOR
    • D21H21/00Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties
    • D21H21/14Non-fibrous material added to the pulp, characterised by its function, form or properties; Paper-impregnating or coating material, characterised by its function, form or properties characterised by function or properties in or on the paper
    • D21H21/36Biocidal agents, e.g. fungicidal, bactericidal, insecticidal agents

Landscapes

  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Pest Control & Pesticides (AREA)
  • Dispersion Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Sanitary Thin Papers (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

A kind of disinfecting tissue of disclosure of the invention, is made up of following component:Bamboo pulp, roundleaf wood pulp, straw pulp, polyvinyl alcohol, purple sweet potato starch, polyethyleneimine, potent antibacterial agent, titanium dioxide, nanoscale sericite in powder.Toilet paper prepared by the inventive method possess raw material extensively, reaction gentle, asepsis environment-protecting the advantages of, meet the theory of " Green Chemistry " of modern requirements, after tissue prepared by the present invention wipes hand, can cause that surface skin is salubriouser on hand, moisturizing, moist, antifreeze, anticracking and other effects can be played, hand can be made soft, with good maintenance action, long-term use can also play certain whitening function.

Description

A kind of disinfecting tissue
Technical field
The present invention relates to paper for daily use preparation field, more particularly to a kind of disinfecting tissue.
Background technology
Tissue is also napkin paper, is a kind of our relatively common paper usually in life, it be mainly used in some food and drink, Family expenses, automobile-used, hotel and public place are used, and its purposes is than wide, and less expensive, deep to be liked by consumer.
Existing tissue is all a common paper, does not possess other any characteristics, except pliability, water imbibition ratio Preferably and cost is than beyond less expensive, just and common paper there is not difference, the requirement continuous improvement with people to daily necessities, singly Pure tissue cannot meet the demand of society, such as, when some public arenas are washed one's hands, typically all open water Tap is washed one's hands, and the hand after washing is clean, but when water wring tap is closed, hand can contact the tap for being stained with bacterium again Handle, some invisible germs return on hand from newly again, at this moment would generally be wiped with hand towel, but general tissue Do not possess the effect of antibacterial, it is impossible to protect the health of user;Meanwhile, some tissues savory can all be produced on the market, Some chemical compositions are typically all with the addition of, has been heard long and dizzy situation is occurred, it is impossible to ensured the safety in utilization of tissue.
The content of the invention
It is an object of the invention to provide a kind of disinfecting tissue, it is achieved through the following technical solutions:
A kind of disinfecting tissue, is made up of following component by weight:Bamboo pulp 50-55, roundleaf wood pulp 25-30, straw pulp 18-23, polyvinyl alcohol 1-4, purple sweet potato starch 6-8, polyethyleneimine 0.5-0.8, potent antibacterial agent 0.2-0.4, titanium dioxide 0.3-0.6, nanoscale sericite in powder 0.2-0.4;The potent antibacterial agent is made up of following component by weight:Tartaric acid 2, Shitosan 6, xylitol 3, mugwort wormwood artemisia 8, sweet wormwood 12, grass 1 of taking drugs.
Further, the straw pulp presses 3 by oldenlandia diffusa, Common Sage Herb, Leymus racemosus:2:40 mass ratios are made.
Further:The potent antibacterial agent preparation method is:Soaked using clear water after mugwort wormwood artemisia is mixed with sweet wormwood 20min, then use again mass concentration be 0.65% liquor natrii hypochloritis immersion 10min, filtering, clear water washing, then with drug abuse Grass mixing, is crushed to 120 mesh, then using 90% concentration of volume percent alcohol solvent, by solid-liquid ratio 1:15, at 40 DEG C next time Stream extracts 2h, and supernatant is centrifuged to obtain, then is concentrated by rotary evaporation, and then freeze-drying is obtained mixed extract, then will be mixed Extract is closed uniformly to mix with tartaric acid, shitosan, xylitol.
Further, described bamboo pulp presses 50 by mao bamboon and mottled bamboo:1 mass ratio is mixed.
A kind of preparation method of disinfecting tissue, comprises the following steps:
1), first bamboo pulp, roundleaf wood pulp, straw pulp ratio are mixed, mixing time is 25mim, then carries out defibrination, Tentatively it is beaten with 1200r/min speed, the time is 2 hours;
2)And then polyvinyl alcohol, purple sweet potato starch, polyethyleneimine are uniformly added in slurry, by temperature adjustment to 80 DEG C, After stirring 40min, stop stirring, add potent antibacterial agent, continue to stir 20min, finally add titanium dioxide and nanoscale Sericite in powder, then secondary mashing is carried out with the speed of 2400r/min, the time is 2 hours;
3)By 2)Middle raw material is centrifuged treatment, and then decontamination is copied into page using paper machine, and is dehydrated, then Squeezed, carried out drying and processing, the temperature of drying is set to 50 DEG C, and drying time is 2 hours;
4)The paper of drying is cut, arranged, packed, stored, that is, obtained finished product tissue.
The present invention prepares paper pulp by rational, and bamboo pulp, roundleaf wood pulp, straw pulp are mixed and made into paper pulp, and wherein bamboo pulp is with hair Bamboo is mixed with mottled bamboo, and straw pulp is mixed with oldenlandia diffusa, Common Sage Herb, Leymus racemosus, is made such that it is able to improve Paper flexibility, can also improve feel, the pliability of the tissue being made is greatly improved, good toughness.
The beneficial effects of the invention are as follows:Toilet paper prepared by the inventive method possess raw material extensively, reaction it is gentle, without poison ring The advantages of guarantor, meet the theory of " Green Chemistry " of modern requirements, the toilet paper phase being made by being acted synergistically between each composition Than in general toilet paper, with tensile strength higher, tear-resistant degree is high, and the present invention is by with oldenlandia diffusa, Common Sage Herb, new Wheat straw is mixed and made into straw pulp, and the effect of the potent antibacterial agent that the coordinated present invention is prepared greatly improves the wiping hand being made The disinfecting, antimicrobial effect of paper, also, it is nontoxic to human body, the potent antibacterial agent that the present invention is prepared is with tartaric acid, shitosan, wood Sugar alcohol, mugwort wormwood artemisia and Artemisinin play functional component for main, and the extract with grass of taking drugs is efficacy-enhancing ingredient, so that not only very big Improve the effect of tissue disinfecting, antimicrobial, and improve Durability of antimicrobial effect, preserve 1 under the tissue conventional environment being made Year, bacteriostasis rate reduction is no more than 2%, after tissue prepared by the present invention wipes hand, can cause that surface skin is salubriouser on hand, energy Moisturizing, moist, antifreeze, anticracking and other effects are enough played, hand can be made soft, with good maintenance action, long-term use can also Play certain whitening function.
Specific embodiment
Embodiment 1
A kind of disinfecting tissue, is made up of following component by weight:Bamboo pulp 50, roundleaf wood pulp 25, straw pulp 18, poly- second Enol 1, purple sweet potato starch 6, polyethyleneimine 0.5, potent antibacterial agent 0.2, titanium dioxide 0.3, nanoscale sericite in powder 0.2;Institute Potent antibacterial agent is stated to be made up of following component by weight:Tartaric acid 2, shitosan 6, xylitol 3, mugwort wormwood artemisia 8, sweet wormwood 12, Drug abuse grass 1.
Embodiment 2
A kind of disinfecting tissue, is made up of following component by weight:Bamboo pulp 55, roundleaf wood pulp 30, straw pulp 23, poly- second Enol 4, purple sweet potato starch 8, polyethyleneimine 0.8, potent antibacterial agent 0.4, titanium dioxide 0.6, nanoscale sericite in powder 0.4;Institute Potent antibacterial agent is stated to be made up of following component by weight:Tartaric acid 2, shitosan 6, xylitol 3, mugwort wormwood artemisia 8, sweet wormwood 12, Drug abuse grass 1.
Embodiment 3
A kind of disinfecting tissue, is made up of following component by weight:Bamboo pulp 52, roundleaf wood pulp 28, straw pulp 20, poly- second Enol 2, purple sweet potato starch 7, polyethyleneimine 0.6, potent antibacterial agent 0.3, titanium dioxide 0.4, nanoscale sericite in powder 0.3;Institute Potent antibacterial agent is stated to be made up of following component by weight:Tartaric acid 2, shitosan 6, xylitol 3, mugwort wormwood artemisia 8, sweet wormwood 12, Drug abuse grass 1.
In above example:
The straw pulp presses 3 by oldenlandia diffusa, Common Sage Herb, Leymus racemosus:2:40 mass ratios are made.
The potent antibacterial agent preparation method is:20min, Ran Houzai are soaked using clear water after mugwort wormwood artemisia is mixed with sweet wormwood Use mass concentration that 10min, filtering, clear water washing are soaked for 0.65% liquor natrii hypochloritis, then mix with grass of taking drugs, crush To 120 mesh, then using 90% concentration of volume percent alcohol solvent, by solid-liquid ratio 1:15, the refluxing extraction 2h at 40 DEG C, from Gains in depth of comprehension supernatant, then concentrated by rotary evaporation, then freeze-drying is obtained mixed extract, then by mixed extract and wine Stone acid, shitosan, xylitol uniformly mix.
Described bamboo pulp presses 50 by mao bamboon and mottled bamboo:1 mass ratio is mixed.
A kind of preparation method of disinfecting tissue, comprises the following steps:
1), first bamboo pulp, roundleaf wood pulp, straw pulp ratio are mixed, mixing time is 25mim, then carries out defibrination, Tentatively it is beaten with 1200r/min speed, the time is 2 hours;
2)And then polyvinyl alcohol, purple sweet potato starch, polyethyleneimine are uniformly added in slurry, by temperature adjustment to 80 DEG C, After stirring 40min, stop stirring, add potent antibacterial agent, continue to stir 20min, finally add titanium dioxide and nanoscale Sericite in powder, then secondary mashing is carried out with the speed of 2400r/min, the time is 2 hours;
3)By 2)Middle raw material is centrifuged treatment, and then decontamination is copied into page using paper machine, and is dehydrated, then Squeezed, carried out drying and processing, the temperature of drying is set to 50 DEG C, and drying time is 2 hours;
4)The paper of drying is cut, arranged, packed, stored, that is, obtained finished product tissue.
Comparative example 1:It is only without potent antibacterial agent with the difference of embodiment 1.
Comparative example 2:Differed only in potent antibacterial agent without grass of taking drugs with embodiment 1.
Comparative example 3:The common straw pulp that straw pulp is made of straw, straw is differed only in embodiment 1.
The napkin paper antibacterial characteristics detection prepared to embodiment and comparative example is as follows:
Table 1
Escherichia coli 15min bacteriostasis rates % Candida albicans 15min bacteriostasis rates % Staphylococcus aureus 15min bacteriostasis rates % Water imbibition mm
Embodiment 1 99.99 99.99 99.99 72
Embodiment 2 99.99 99.99 99.99 70
Embodiment 3 99.99 99.99 99.99 71
Comparative example 1 80.24 79.35 76.61 69
Comparative example 2 85.28 84.14 82.34 70
Comparative example 3 93.92 94.93 93.35 52
Above antibacterial detects foundation:GB15979 Disposable Sanitary Accessory sanitary standards.
As can be seen from Table 1, the antibacterial efficiency of napkin paper that prepared by the present invention is notable.
Tissue and sterile towel prepared by the present invention are carried out multiple spot it is many when Bacteria Culture, detect bacterium colony number, knot Fruit is as follows:
Table 2
Time 0h 1h 2h 3h 4h
Sterile towel 0 0 1 6 12
Table 3
Time 0h 1h 12h 3 days 6 days
Tissue of the present invention 0 0 0 0 1
By Tables 1 and 2 as can be seen that tissue Disinfection Effect of the present invention is more preferable.

Claims (5)

1. a kind of disinfecting tissue, it is characterised in that:It is made up of following component by weight:Bamboo pulp 50-55, roundleaf wood Slurry 25-30, straw pulp 18-23, polyvinyl alcohol 1-4, purple sweet potato starch 6-8, polyethyleneimine 0.5-0.8, potent antibacterial agent 0.2- 0.4th, titanium dioxide 0.3-0.6, nanoscale sericite in powder 0.2-0.4;The potent antibacterial agent is by weight by following component It is made:Tartaric acid 2, shitosan 6, xylitol 3, mugwort wormwood artemisia 8, sweet wormwood 12, grass 1 of taking drugs.
2. a kind of disinfecting tissue according to claim 1, it is characterised in that the straw pulp by oldenlandia diffusa, Common Sage Herb, Leymus racemosus press 3:2:40 mass ratios are made.
3. a kind of disinfecting tissue according to claim 1, it is characterised in that:The potent antibacterial agent preparation method For:After mugwort wormwood artemisia is mixed with sweet wormwood using clear water soak 20min, then use again mass concentration for 0.65% sodium hypochlorite Solution soaks 10min, filtering, clear water washing, then mixes with grass of taking drugs, and 120 mesh is crushed to, then using 90% percent by volume Concentration ethanol solvent, by solid-liquid ratio 1:15, the refluxing extraction 2h at 40 DEG C, are centrifuged to obtain supernatant, then dense by rotary evaporation Contracting, then freeze-drying is obtained mixed extract, then uniformly mixes mixed extract with tartaric acid, shitosan, xylitol .
4. a kind of disinfecting tissue according to claim 1, it is characterised in that described bamboo pulp is by mao bamboon and mottled bamboo By 50:1 mass ratio is mixed.
5. the preparation method of a kind of disinfecting tissue according to claim 1, it is characterised in that:Including following step Suddenly:
1), first bamboo pulp, roundleaf wood pulp, straw pulp ratio are mixed, mixing time is 25mim, then carries out defibrination, Tentatively it is beaten with 1200r/min speed, the time is 2 hours;
2)And then polyvinyl alcohol, purple sweet potato starch, polyethyleneimine are uniformly added in slurry, by temperature adjustment to 80 DEG C, After stirring 40min, stop stirring, add potent antibacterial agent, continue to stir 20min, finally add titanium dioxide and nanoscale Sericite in powder, then secondary mashing is carried out with the speed of 2400r/min, the time is 2 hours;
3)By 2)Middle raw material is centrifuged treatment, and then decontamination is copied into page using paper machine, and is dehydrated, then Squeezed, carried out drying and processing, the temperature of drying is set to 50 DEG C, and drying time is 2 hours;
4)The paper of drying is cut, arranged, packed, stored, that is, obtained finished product tissue.
CN201611252526.4A 2016-12-30 2016-12-30 A kind of disinfecting tissue Pending CN106835816A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201611252526.4A CN106835816A (en) 2016-12-30 2016-12-30 A kind of disinfecting tissue

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Application Number Priority Date Filing Date Title
CN201611252526.4A CN106835816A (en) 2016-12-30 2016-12-30 A kind of disinfecting tissue

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CN106835816A true CN106835816A (en) 2017-06-13

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107869091A (en) * 2017-12-26 2018-04-03 合肥洁诺无纺布制品有限公司 A kind of comfortable medical tissue of fragrance
CN108103847A (en) * 2017-12-26 2018-06-01 合肥洁诺无纺布制品有限公司 A kind of medical tissue of disinfection
CN108130798A (en) * 2017-12-26 2018-06-08 合肥洁诺无纺布制品有限公司 A kind of antibacterial medical tissue
CN114507998A (en) * 2022-01-21 2022-05-17 余时画 Packaging paper production equipment based on nano copper oxide antivirus and production process thereof

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104846685A (en) * 2015-04-27 2015-08-19 浙江华川实业集团有限公司 Disinfectant health-care aromatic hand paper towel and preparation method thereof
CN106149449A (en) * 2016-08-17 2016-11-23 安庆市新宜纸业有限公司 A kind of preparation method of the napkin containing jasmine aroma
CN106192579A (en) * 2016-08-17 2016-12-07 安庆市新宜纸业有限公司 A kind of preparation method of the napkin containing orchid fragrance

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104846685A (en) * 2015-04-27 2015-08-19 浙江华川实业集团有限公司 Disinfectant health-care aromatic hand paper towel and preparation method thereof
CN106149449A (en) * 2016-08-17 2016-11-23 安庆市新宜纸业有限公司 A kind of preparation method of the napkin containing jasmine aroma
CN106192579A (en) * 2016-08-17 2016-12-07 安庆市新宜纸业有限公司 A kind of preparation method of the napkin containing orchid fragrance

Non-Patent Citations (1)

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Title
王文蜀主编: "《中国民族地区药用植物化学成分与药理作用》", 30 September 2013 *

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107869091A (en) * 2017-12-26 2018-04-03 合肥洁诺无纺布制品有限公司 A kind of comfortable medical tissue of fragrance
CN108103847A (en) * 2017-12-26 2018-06-01 合肥洁诺无纺布制品有限公司 A kind of medical tissue of disinfection
CN108130798A (en) * 2017-12-26 2018-06-08 合肥洁诺无纺布制品有限公司 A kind of antibacterial medical tissue
CN114507998A (en) * 2022-01-21 2022-05-17 余时画 Packaging paper production equipment based on nano copper oxide antivirus and production process thereof

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Application publication date: 20170613

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