CN106833918A - A kind of quantitative softness detergent - Google Patents

A kind of quantitative softness detergent Download PDF

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Publication number
CN106833918A
CN106833918A CN201710006657.2A CN201710006657A CN106833918A CN 106833918 A CN106833918 A CN 106833918A CN 201710006657 A CN201710006657 A CN 201710006657A CN 106833918 A CN106833918 A CN 106833918A
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CN
China
Prior art keywords
detergent
softness
polyvinyl alcohol
surfactant
quantify
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN201710006657.2A
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Chinese (zh)
Other versions
CN106833918B (en
Inventor
曾艳
曾宇曼
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Guangdong Youkai Technology Co ltd
Original Assignee
Guangzhou Holy Washing Products Co Ltd
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Priority to CN201710006657.2A priority Critical patent/CN106833918B/en
Publication of CN106833918A publication Critical patent/CN106833918A/en
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Publication of CN106833918B publication Critical patent/CN106833918B/en
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Classifications

    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/66—Non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/90—Betaines
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D1/00—Detergent compositions based essentially on surface-active compounds; Use of these compounds as a detergent
    • C11D1/88—Ampholytes; Electroneutral compounds
    • C11D1/94—Mixtures with anionic, cationic or non-ionic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/2003—Alcohols; Phenols
    • C11D3/2065—Polyhydric alcohols
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/20—Organic compounds containing oxygen
    • C11D3/22—Carbohydrates or derivatives thereof
    • C11D3/222—Natural or synthetic polysaccharides, e.g. cellulose, starch, gum, alginic acid or cyclodextrin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/16—Organic compounds
    • C11D3/34—Organic compounds containing sulfur
    • C11D3/349—Organic compounds containing sulfur additionally containing nitrogen atoms, e.g. nitro, nitroso, amino, imino, nitrilo, nitrile groups containing compounds or their derivatives or thio urea
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/40—Dyes ; Pigments
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11D—DETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D3/00—Other compounding ingredients of detergent compositions covered in group C11D1/00
    • C11D3/50—Perfumes
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M15/00—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment
    • D06M15/19—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with synthetic macromolecular compounds
    • D06M15/21—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D06M15/327—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof
    • D06M15/333—Macromolecular compounds obtained by reactions only involving carbon-to-carbon unsaturated bonds of unsaturated alcohols or esters thereof of vinyl acetate; Polyvinylalcohol
    • D—TEXTILES; PAPER
    • D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
    • D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
    • D06M2200/00—Functionality of the treatment composition and/or properties imparted to the textile material
    • D06M2200/50—Modified hand or grip properties; Softening compositions

Abstract

The invention discloses a kind of quantitative softness detergent, including polyvinyl alcohol water soluble film, the quantitative liquid detergent of parcel in the polyvinyl alcohol water soluble film, the polyvinyl alcohol water soluble film includes polyvinyl alcohol and cationic surfactant, and the liquid detergent includes non-anion surfactant.The present invention simultaneously comprising with submissive effect cationic surfactant and cleaning function nonionic surfactant, can a step complete washing and submissive operation, using very facilitate, and product storage the time limit in product stabilization.

Description

A kind of quantitative softness detergent
Technical field
The present invention relates to a kind of detergent, more particularly to a kind of quantitative softness detergent.
Background technology
With the improvement of living standards, convenience requirement of the consumer to daily chemical products is gradually stepped up, it is often desired to washed Wash and completed with a submissive step.Common detergent finished product cannot simultaneously provide quantitatively submissive performance, this be due to softener into Point often all it is cationic surfactant, and anion surfactant or non-ionic surface during the main component of detergent Activating agent.When cationic surfactant and anion surfactant all with liquid simultaneously in the presence of, it may occur that charging neutrality Electric charge is lost, and the mutual adsorption-flocculation of meeting is settled, and makes surfactant ineffective.And cationic surfactant and Nonionic surfactant simultaneously in the presence of, can hydrolyze during storage, cationic surfactant is separated out, and detergent deposits Put stability poor.It can be seen that, if cationic surfactant coexists with anion or nonionic surfactant, detergent Stability is all excessively poor.Thus current liquid detergent and softener are all the products separately individually sold, and also separate independent Use, typically first detergent washing uses softener afterwards.
The content of the invention
It is an object of the invention to provide a kind of quantitative softness detergent, it is simultaneously comprising the sun with submissive effect The nonionic surfactant of ionic surface active agent and cleaning function, can a step complete washing and submissive operation, use Facilitate very much, and product product stabilization within the storage time limit.
The purpose of the present invention is achieved through the following technical solutions：A kind of quantitative softness detergent, including it is poly- The quantitative liquid detergent of parcel, the polyvinyl alcohol water soluble film bag in vinyl alcohol (PVA) water soluble film, the polyvinyl alcohol water soluble film Containing polyvinyl alcohol and cationic surfactant, the liquid detergent includes non-anion surfactant.
Mass percentage content of the cationic surfactant of the present invention in polyvinyl alcohol water soluble film is 1-50%.
The polyvinyl alcohol water soluble film also includes auxiliary agent and water.And as one embodiment of the present of invention, polyvinyl alcohol water The each component content included in molten film is as follows：
Polyvinyl alcohol 40-95%
Cationic surfactant 1-50%
Auxiliary agent 0-20% but it is not zero
Water 0-20% but it is not zero.
The preferred quaternary ammonium salt of cationic surfactant or ester quat.The auxiliary agent includes but is not limited to glycerine, forms sediment Powder.
In the liquid detergent, the mass percentage content of non-anion surfactant is 25-99%.Certainly, it is described Can also be comprising builder, preservative and water etc. in detergent.As one embodiment of the present of invention, the liquid detergent bag Component containing following mass percent：
Non-anion surfactant 25-99%
Builder 0-70%
Preservative 0.01-1%
Water 0-15% but it is not zero.
Non-anion surfactant of the present invention is in nonionic surfactant and zwitterionic surfactant One or two combination.The nonionic surfactant includes but is not limited to fatty acid methyl ester ethoxylate.Described two Property ionic surface active agent includes but is not limited to glycine betaine, amine-oxides.
The builder includes but is not limited to chelating agent, fluorescent whitening agent, anti redeposition agent etc..
The preservative includes but is not limited to methylisothiazolinone (MIT), methylchloroisothiazandnone (CMIT).
The present invention has advantages below compared with prior art：
(1) detergent that the present invention is provided is made up of the quantitative liquid detergent of polyvinyl alcohol water soluble film parcel, is one independent PVA water soluble films pack product, due to containing quantitative detergent, adding multiple using one or according to washing loads every time, it is to avoid mistake It is many to cause to waste using detergent.
(2) in the present invention, cationic surfactant is included in polyvinyl alcohol water soluble film, is existed in film solid-state form, Avoid being reacted with the surfactant in liquid detergent, improve product stability.In addition, the surfactant of detergent Using the non-anion surfactant such as nonionic surfactant or zwitterionic surfactant, then cationic surface is lived Property agent after soluble in water will not with above-mentioned surfactant occur charging neutrality, so as to maintain cationic surfactant Compliance function and surfactant wash function, so as to realize that washing and a submissive step are completed, use very comfortable side Just.
Specific embodiment
Quantitative softness detergent preparation method：Each component consumption is referring to table 1
1.PVA water soluble films：PVA, ester quat or quaternary ammonium salt, water, auxiliary agent are mixed, heating stirring is dried to being completely dissolved Film forming.
2. detergent：Surfactant, essence non-anion surfactant, preservative, pigment, auxiliary agent, water are mixed Close uniform into uniform detergent liquid.Non-anion surfactant is that nonionic surfactant and amphion surface are lived Property agent in one or two combination.The nonionic surfactant includes but is not limited to fatty acid methyl ester ethoxylate. The zwitterionic surfactant includes but is not limited to glycine betaine, amine-oxides.
3. pack：The uniform detergent liquid for mixing is got to heat sealing machine or water seal packing machine, with PVA water soluble film bags Dress.
The detergent of Example 1-3 is placed in 40 DEG C, ester quat, quaternary surfactant in film is determined after January remaining Rate.Ester quat, quaternary surfactant surplus ratio in film=（Ester quat, quaternary ammonium salt cationic table in sample film after 40 DEG C of January Face active agent content）/（Ester quat, quaternary cationics content in fresh sample film）, surplus ratio more it is low more not Stabilization.Submissive Contrast on effect test：Sample is A after 40 DEG C of January, and fresh sample is B, soaks same with same consumption, water, time One specification towel, dries, and the towel soaked with sample A is recorded as A groups, and the towel soaked with sample B is recorded as B groups, takes an A Group one B group towel of towel, number consecutively be a, b, touched to 25 staff pick out with submissiveer towel, pick out fresh sample The submissive preferable percentage of effect=select fresh sample（B samples）Number/25 of the towel b of immersion, it is clear that percentage is got over and connect Nearly 50%, the submissive degree of a, b towel is closer to sample A and fresh sample B is closer to, that is to say, that cation after that is, 40 DEG C January It is more stable.Conversely, percentage is closer to 100%, cation is more unstable.
Shown by the result of table 2, the cationic surfactant stabilization inside the detergent and film of embodiment 1-3 coexists, And submissive effect is without substantially decrease.1 ~ comparative example of comparative example 3 is by respectively by the PVA water soluble film water of 1 ~ embodiment of embodiment 3 After dissolving, it is all added to be obtained in commercially available ordinary liquid laundry detergent.As seen from Table 3, cationic surfactant is unable to stable existence, holds Easily it is hydrolyzed, submissive effect has substantially decrease.
The present invention can be summarized with others without prejudice to the concrete form of spirit or essential characteristics of the invention.It is of the invention Above-described embodiment can only all be considered the description of the invention rather than limitation.Therefore it is every according to substantial technological pair of the invention Any trickle amendment, equivalent variations and modification that above example is made, belong in the range of technical solution of the present invention.

Claims (10)

1. a kind of quantitative softness detergent, including polyvinyl alcohol water soluble film, it is characterized in that, in the polyvinyl alcohol water soluble film The quantitative liquid detergent of parcel, the polyvinyl alcohol water soluble film includes polyvinyl alcohol and cationic surfactant, the liquid Detergent includes non-anion surfactant.
2. it is according to claim 1 to quantify softness detergent, it is characterized in that, in the polyvinyl alcohol water soluble film, institute The mass percentage content of polyvinyl alcohol is stated for 40-95%, the mass percentage content of the cationic surfactant is 1- 50%。
3. it is according to claim 1 and 2 to quantify softness detergent, it is characterized in that, the polyvinyl alcohol water soluble film is also Comprising auxiliary agent and water.
4. it is according to claim 3 to quantify softness detergent, it is characterized in that, what is included in polyvinyl alcohol water soluble film is each Constituent content is as follows：
Polyvinyl alcohol 40-95%
Cationic surfactant 1-50%
Auxiliary agent 0-20% but it is not zero
Water 0-20% but it is not zero.
5. it is according to claim 4 to quantify softness detergent, it is characterized in that, the cationic surfactant is season Ammonium type surfactant or ester quat.
6. it is according to claim 4 to quantify softness detergent, it is characterized in that, the auxiliary agent is including but not limited to sweet Oil, starch.
7. it is according to claim 1 and 2 to quantify softness detergent, it is characterized in that, in the liquid detergent, non-the moon The mass percentage content of ionic surface active agent is 25-99%.
8. it is according to claim 7 to quantify softness detergent, it is characterized in that, certainly, also included in the detergent One or more in builder, preservative and water, i.e., component of the described liquid detergent comprising following mass percent：
Non-anion surfactant 25-99%
Builder 0-70% but it is not zero
Preservative 0.01-1% but it is not zero
Water 0-15% but it is not zero.
9. it is according to claim 7 to quantify softness detergent, it is characterized in that, the non-anion surfactant is One or two combinations in nonionic surfactant and zwitterionic surfactant.
10. it is according to claim 7 to quantify softness detergent, it is characterized in that, the builder is included but is not limited to Chelating agent, fluorescent whitening agent, anti redeposition agent；The preservative includes but is not limited to the different thiophene of methylisothiazolinone, methyl chloride Oxazoline ketone.
CN201710006657.2A 2017-01-05 2017-01-05 Quantitative fabric softening detergent Active CN106833918B (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
CN201710006657.2A CN106833918B (en) 2017-01-05 2017-01-05 Quantitative fabric softening detergent

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CN106833918B CN106833918B (en) 2020-08-04

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Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108642876A (en) * 2018-04-30 2018-10-12 安徽恒益纺织科技有限公司 A kind of fragrant softening agent for textile fabric
WO2019144371A1 (en) * 2018-01-26 2019-08-01 The Procter & Gamble Company Unitary laundry detergent article
CN110846842A (en) * 2019-10-31 2020-02-28 久株电气(无锡)有限公司 Special box type detergent for clothes and cleaning method thereof
CN114540135A (en) * 2022-03-17 2022-05-27 广州大白生物科技有限公司 Solid detergent coated by water-soluble film

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1935972A (en) * 2006-09-20 2007-03-28 王涛 Washing capsule and its preparing method
CN102597203A (en) * 2009-11-06 2012-07-18 宝洁公司 High efficiency particle comprising benefit agent
CN104694275A (en) * 2014-12-16 2015-06-10 江南大学 Solid clothes laundering composition coated with polymeric membrane and preparation method thereof
WO2016105333A1 (en) * 2014-12-22 2016-06-30 Colgate-Palmolive Company Unit dose fabric softener
CN105779159A (en) * 2016-04-09 2016-07-20 福建省金鹿日化股份有限公司 Softening clothes washing condensate ball and preparation method thereof

Patent Citations (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1935972A (en) * 2006-09-20 2007-03-28 王涛 Washing capsule and its preparing method
CN102597203A (en) * 2009-11-06 2012-07-18 宝洁公司 High efficiency particle comprising benefit agent
CN104694275A (en) * 2014-12-16 2015-06-10 江南大学 Solid clothes laundering composition coated with polymeric membrane and preparation method thereof
WO2016105333A1 (en) * 2014-12-22 2016-06-30 Colgate-Palmolive Company Unit dose fabric softener
CN105779159A (en) * 2016-04-09 2016-07-20 福建省金鹿日化股份有限公司 Softening clothes washing condensate ball and preparation method thereof

Cited By (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2019144371A1 (en) * 2018-01-26 2019-08-01 The Procter & Gamble Company Unitary laundry detergent article
CN111511887A (en) * 2018-01-26 2020-08-07 宝洁公司 Integrated laundry detergent article
US11015153B2 (en) 2018-01-26 2021-05-25 The Procter & Gamble Company Unitary laundry detergent article
CN111511887B (en) * 2018-01-26 2022-04-08 宝洁公司 Integrated laundry detergent article
CN108642876A (en) * 2018-04-30 2018-10-12 安徽恒益纺织科技有限公司 A kind of fragrant softening agent for textile fabric
CN110846842A (en) * 2019-10-31 2020-02-28 久株电气(无锡)有限公司 Special box type detergent for clothes and cleaning method thereof
CN110846842B (en) * 2019-10-31 2020-11-17 久株电气(无锡)有限公司 Special box type detergent for clothes and cleaning method thereof
CN114540135A (en) * 2022-03-17 2022-05-27 广州大白生物科技有限公司 Solid detergent coated by water-soluble film

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Effective date of registration: 20170710

Address after: Nanhai District of Guangdong town water road 528244 city of Foshan Province in 2 block F No. two Room 202

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Address before: 510510 A, Guangzhou industrial center, north industry, No. 1 Mei Gang Road, Baiyun District, Guangdong, 503, Guangzhou, China

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Denomination of invention: A quantitative clothing softening detergent

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Granted publication date: 20200804

Pledgee: Industrial and Commercial Bank of China Limited Foshan Nanhai Lishui Sub branch

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Address before: Room 202, 2nd Floor, Building F, No. 2 Zhongjin Road, Lishui Town, Nanhai District, Foshan City, Guangdong Province, 528244

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