CN106833903A - Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively - Google Patents
Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively Download PDFInfo
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- CN106833903A CN106833903A CN201710195339.5A CN201710195339A CN106833903A CN 106833903 A CN106833903 A CN 106833903A CN 201710195339 A CN201710195339 A CN 201710195339A CN 106833903 A CN106833903 A CN 106833903A
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- chinese mugwort
- essential oil
- mugwort essential
- green
- distillation
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Medicines Containing Plant Substances (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The present invention disclose a kind of blue or green argy wormwood distillation, sedimentation separation and quenches respectively and takes Chinese mugwort essential oil method, it is characterized in that using fresh argy wormwood blue or green be raw material, segment is rolled stone roller and is crushed, soaking and stirring, the part distillation volatile Chinese mugwort essential oil of acquisition.Sedimentation separation obtains not volatile Chinese mugwort essential oil after the filter of slag hydraulic pressure after the distillation of part.The present invention compared with prior art, using a blue or green argy wormwood, the operation such as saves priming leaf, dries in the shade, store and bothering, and squeezes the essential oil that all ended contained by argy wormwood cauline leaf, output efficiency is high, the utilization of resources is abundant, production process water-saving energy-conservation, very of low pollution.Volatile Chinese mugwort essential oil and not volatile Chinese mugwort essential oil are obtained simultaneously, it respectively has characteristic and effect, expanding new application and exploitation new product for Chinese mugwort essential oil provides more guarantees.
Description
First, technical field：
The present invention relates to the fine chemistry industry in farming industry, more particularly to a kind of blue or green argy wormwood distillation, sedimentation
Separation is quenched take Chinese mugwort essential oil method respectively.
2nd, background technology：
Chinese mugwort, another name " family Chinese mugwort ", " argy wormwood " belong to composite family, perennial herb.Because the essential oil that ended contained by its cauline leaf can make blending original
Material, kills pest expelling, has promoting qi circulation and removing obstruction in the collateral in traditional Chinese medicine, warming channel and expelling cold, yang invigorating, acts on the effects such as enhancing is immune, at me
Life between its people, production and existing more than 2,000 years of traditional Chinese medical science field extensively using history, modern times for Chinese mugwort active ingredient and
Effect is analyzed and researched, and the Chinese mugwort essential oil to core has carried out industrializing to quench taking processing.Prior art extracts Chinese mugwort essential oil,
Be mostly will screen, dry in the shade, crush after folium artemisiae argyi, distilled after directly heat distillation, steam distillation or organic solvent diacolation
Produced etc. method, the subject matter for existing is：1st, folium artemisiae argyi it is selected, to dry in the shade, collect and store all be a time-consuming, laborious fiber crops
Tired process, is difficult to form large-scale production.2nd, argy wormwood utilization rate is low.3rd, Chinese mugwort essential oil obtain ratio be limited, be only extracted normal temperature, often
Not volatile residual fraction under state, resource utilization is low.
3rd, the content of the invention：
The purpose of the present invention is directed to above present situation and problem, there is provided utilize whole Ai Qing cauline leaf of strain, effective acquisition easily to wave
One kind blue or green argy wormwood distillation, sedimentation separation of hair and not volatile Chinese mugwort essential oil are quenched take Chinese mugwort essential oil method respectively.
The purpose of the present invention is achieved through the following technical solutions：
A kind of blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively, it is characterized in that using fresh argy wormwood green grass or young crops,
Segment is rolled stone roller and is crushed, and whole scum juices load reactor, and add water closing soaking and stirring, and 1/3rd liquid are distilled by bottom normal heating
Body；Settlement separator being input into after the condensed device condensation of distillation vapour to stand, obtaining aqueous volatile Chinese mugwort essential oil, distilled water returns defeated reaction
Kettle is used as addition water circulation use；Lower the temperature after reactor distillation, clear out whole slag liquid and be transferred to filter-pressing cauldron, filter liquor transfers sedimentation point
Stood from device, obtain not volatile Chinese mugwort essential oil crude product；Decolourized through centrifugation, filter cleaning dregs, obtain clean aqueous not volatile Chinese mugwort essence
Oil.
Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively, it is characterized in that aqueous volatile Chinese mugwort essential oil is obtained,
Aqueous not volatile Chinese mugwort essential oil adds anhydrous sodium sulfate stirring dehydration in capping kettle respectively, is obtained after clarification and pure easily waved
Hair Chinese mugwort essential oil and not volatile Chinese mugwort essential oil.
Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively, it is characterized in that being noted in distillate and filter liquor
Enter water aerosol, improve the smart oil quenching of Chinese mugwort and take ratio and speed.
Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively, it is characterized in that being quenched using same method and flow
Take dried whole strain Chinese mugwort cauline leaf.
Blue or green argy wormwood of the invention distillation, sedimentation separation are quenched takes Chinese mugwort essential oil method compared with prior art respectively, with
Lower distinguishing feature and many merits：
1st, directly quenched using blue or green Chinese mugwort and take Chinese mugwort essential oil, eliminate many expenses that are selected, winning folium artemisiae argyi, dry in the shade, store keeping
When, the laborious, trouble of occupied ground, storehouse and cost, be more convenient for accomplishing scale production.
2nd, quenched Chinese mugwort essential oil using whole cauline leafs of blue or green Chinese mugwort, resource utilization is high, and processing link is few, is easy to machining,
Efficiency is improved, acquisition Chinese mugwort essential oil is more, cost is lower.
3rd, a blue or green Chinese mugwort to be applied settle two steps after distillation and distillation and quench and takes Chinese mugwort essential oil scheme, can simultaneously obtain volatile and not
Volatile, property and function all have two kinds of Chinese mugwort essential oils of difference, are the more Chinese mugwort essential oil preparations differed from one another with purposes of production,
Open up broader market and more guarantees are provided.
4th, in kind quenched with flow and take dried whole strain Chinese mugwort cauline leaf, the seasonal production cycle can be extended, desalination Chinese mugwort
Restricted influence of the wormwood artemisia growth cycle on producing.
5th, prepare Chinese mugwort essential oil emulsion by volatility and substitute agricultural chemicals, for before agriculture fruit and vegetable picking or in growth, it is quick
Or long-acting insect expelling, desinsection, produce the ecological product of green safety.
4th, illustrate：
Without accompanying drawing.
5th, specific embodiment：
The present invention is done with reference to embodiment is illustrated in further detail below：
Blue or green of the ripe argy wormwood of harvesting, the segment of feeder greens disintegrating machine is crushed, and further with twin rollers rolls stone roller, cracks argy wormwood
After structure, scum juice coefficient is inserted into steeping tank or reactor is directly loadable into, soaked.Heated in reactor, in stirring and steamed
Juice 1/3rd is evaporated to stop.The condensed device of distillation vapour containing water and volatile Chinese mugwort essential oil recovers liquid, is input into the sedimentation of closing
Knockout tower stands shunting, and volatile Chinese mugwort essential oil is obtained by knockout tower top.By remaining scum juice falls defeated pressure after distillation in reactor
Filter tank, leaches juice and transfers to be stood into sedimentation splitter column and shunt, and obtaining being difficult containing impurity and moisture by splitter column top waves
Hair Chinese mugwort essential oil, then obtain the clean not volatile Chinese mugwort essential oil of clarification through being centrifuged and filtering.The volatile Chinese mugwort essential oil and not that will be obtained
Volatile Chinese mugwort essential oil is input into treatment tank respectively, adds anhydrous sodium sulfate, stirs the dehydration that is mixed, that is, obtain pure volatile Chinese mugwort essence
Oily and not volatile Chinese mugwort two kinds of products of essential oil, closing is packaged as enterprise's finished product.
Above-mentioned flow describes basic technology method of the invention, to those skilled in the art, can understand and not take off
In the case of operation principle of the present invention, the specific embodiment for implement various increases and decreases, modification, replacing all should be encompassed within the present invention
Within protective scope of the claims.
Claims (4)
1. a kind of blue or green argy wormwood distillation, sedimentation separation is quenched take Chinese mugwort essential oil method respectively, it is characterized in that using fresh argy wormwood green grass or young crops, cutting
Section is rolled stone roller and is crushed, and whole scum juices load reactor, and add water closing soaking and stirring, and 1/3rd liquid are distilled by bottom normal heating
Body；Settlement separator being input into after the condensed device condensation of distillation vapour to stand, obtaining aqueous volatile Chinese mugwort essential oil, distilled water returns defeated reaction
Kettle is used as addition water circulation use；Lower the temperature after reactor distillation, clear out whole slag liquid and be transferred to filter-pressing cauldron, filter liquor transfers sedimentation point
Stood from device, obtain not volatile Chinese mugwort essential oil crude product；Decolourized through centrifugation, filter cleaning dregs, obtain clean aqueous not volatile Chinese mugwort essence
Oil.
2. blue or green argy wormwood distillation, sedimentation separation according to claim 1 is quenched take Chinese mugwort essential oil method respectively, it is characterized in that being obtained
Aqueous volatile Chinese mugwort essential oil, aqueous not volatile Chinese mugwort essential oil adds anhydrous sodium sulfate stirring dehydration in capping kettle respectively,
Pure volatile Chinese mugwort essential oil and not volatile Chinese mugwort essential oil are obtained after clarification.
3. blue or green argy wormwood distillation, sedimentation separation according to claim 1 is quenched take Chinese mugwort essential oil method respectively, it is characterized in that to steaming
Injection water aerosol in distillate and filter liquor, improves the smart oil quenching of Chinese mugwort and takes ratio and speed.
4. blue or green argy wormwood distillation, sedimentation separation according to claim 1 is quenched take Chinese mugwort essential oil method respectively, it is characterized in that utilizing
Same method and flow are quenched and take dried whole strain Chinese mugwort cauline leaf.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710195339.5A CN106833903A (en) | 2017-03-29 | 2017-03-29 | Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710195339.5A CN106833903A (en) | 2017-03-29 | 2017-03-29 | Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively |
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| Publication Number | Publication Date |
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| CN106833903A true CN106833903A (en) | 2017-06-13 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201710195339.5A Pending CN106833903A (en) | 2017-03-29 | 2017-03-29 | Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively |
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| CN103421609A (en) * | 2013-07-31 | 2013-12-04 | 天门华普医药化工有限公司 | Production method for extracting essential oil from plant artemisia argyi |
| CN104322570A (en) * | 2014-11-05 | 2015-02-04 | 湖北中医药大学 | Chinese mugwort air sterilization spray and preparation method thereof |
| CN105296143A (en) * | 2015-12-04 | 2016-02-03 | 威海皓菲集团有限公司 | Preparation method of artemisia argyi essential oil |
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2017
- 2017-03-29 CN CN201710195339.5A patent/CN106833903A/en active Pending
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| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101365668A (en) * | 2005-12-16 | 2009-02-11 | 巴克多天然防腐剂有限公司 | Recovery of residual plant components after distillation of essential oils |
| CN102757136A (en) * | 2012-08-10 | 2012-10-31 | 董兰田 | Fine filtration device for oily sewage twice treating by water aerosol filled outside filter |
| CN103421609A (en) * | 2013-07-31 | 2013-12-04 | 天门华普医药化工有限公司 | Production method for extracting essential oil from plant artemisia argyi |
| CN104322570A (en) * | 2014-11-05 | 2015-02-04 | 湖北中医药大学 | Chinese mugwort air sterilization spray and preparation method thereof |
| CN105296143A (en) * | 2015-12-04 | 2016-02-03 | 威海皓菲集团有限公司 | Preparation method of artemisia argyi essential oil |
| CN205501255U (en) * | 2016-02-19 | 2016-08-24 | 湖北艾家人健康产业有限公司 | Chinese mugwort essential oil distillation extractor |
| CN106318642A (en) * | 2016-10-20 | 2017-01-11 | 北京玫瑰谷香露有限公司 | Preparation method of high-purity essential oil by low-temperature distillation extraction |
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