CN103421609A - Production method for extracting essential oil from plant artemisia argyi - Google Patents
Production method for extracting essential oil from plant artemisia argyi Download PDFInfo
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- CN103421609A CN103421609A CN2013103256890A CN201310325689A CN103421609A CN 103421609 A CN103421609 A CN 103421609A CN 2013103256890 A CN2013103256890 A CN 2013103256890A CN 201310325689 A CN201310325689 A CN 201310325689A CN 103421609 A CN103421609 A CN 103421609A
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- Prior art keywords
- argy wormwood
- essential oil
- artemisia argyi
- argy
- wormwood essential
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- 239000000341 volatile oil Substances 0.000 title claims abstract description 40
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 20
- 241001435059 Artemisia argyi Species 0.000 title abstract 8
- 235000003261 Artemisia vulgaris Nutrition 0.000 claims abstract description 53
- 238000000034 method Methods 0.000 claims abstract description 18
- 239000002994 raw material Substances 0.000 claims abstract description 12
- 230000036571 hydration Effects 0.000 claims abstract description 3
- 238000006703 hydration reaction Methods 0.000 claims abstract description 3
- 239000007788 liquid Substances 0.000 claims abstract description 3
- 235000009051 Ambrosia paniculata var. peruviana Nutrition 0.000 claims description 52
- 235000003097 Artemisia absinthium Nutrition 0.000 claims description 52
- 240000001851 Artemisia dracunculus Species 0.000 claims description 52
- 235000017731 Artemisia dracunculus ssp. dracunculus Nutrition 0.000 claims description 52
- 239000001138 artemisia absinthium Substances 0.000 claims description 51
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 claims description 51
- 239000000203 mixture Substances 0.000 claims description 12
- 241000196324 Embryophyta Species 0.000 claims description 8
- 238000012545 processing Methods 0.000 claims description 8
- 238000013517 stratification Methods 0.000 claims description 7
- 239000002699 waste material Substances 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 4
- 238000011109 contamination Methods 0.000 claims description 3
- 239000012535 impurity Substances 0.000 claims description 3
- 239000012452 mother liquor Substances 0.000 claims description 3
- 238000012216 screening Methods 0.000 claims description 3
- 229910001220 stainless steel Inorganic materials 0.000 claims description 3
- 239000010935 stainless steel Substances 0.000 claims description 3
- 150000001875 compounds Chemical class 0.000 claims description 2
- 239000003921 oil Substances 0.000 claims description 2
- 238000002203 pretreatment Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 abstract description 4
- 235000010894 Artemisia argyi Nutrition 0.000 abstract 7
- 239000002893 slag Substances 0.000 abstract 4
- 239000010779 crude oil Substances 0.000 abstract 3
- 235000003826 Artemisia Nutrition 0.000 abstract 1
- 244000030166 artemisia Species 0.000 abstract 1
- 235000009052 artemisia Nutrition 0.000 abstract 1
- 238000003825 pressing Methods 0.000 abstract 1
- 238000001256 steam distillation Methods 0.000 description 7
- 238000004821 distillation Methods 0.000 description 5
- 235000019476 oil-water mixture Nutrition 0.000 description 5
- 239000003960 organic solvent Substances 0.000 description 5
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 3
- 239000000470 constituent Substances 0.000 description 3
- 238000000194 supercritical-fluid extraction Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 239000012043 crude product Substances 0.000 description 2
- 230000007613 environmental effect Effects 0.000 description 2
- 230000003203 everyday effect Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 239000010659 mugwort oil Substances 0.000 description 2
- 230000000630 rising effect Effects 0.000 description 2
- 238000010924 continuous production Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003337 fertilizer Substances 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000013467 fragmentation Methods 0.000 description 1
- 238000006062 fragmentation reaction Methods 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 238000011031 large-scale manufacturing process Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 235000019198 oils Nutrition 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 238000004886 process control Methods 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000000638 solvent extraction Methods 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
- 239000002912 waste gas Substances 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Landscapes
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Abstract
The invention aims to provide artemisia argyi essential oil production process which can shorten production process procedures, lowers production cost, and is safe, environmental-friendly, relatively lower in the requirement on workers' quality and easy to process slag. The production method can realize continuous and mass production of artemisia argyi essential oil, and comprises the following steps: 1. pretreatment of the artemisia argyi; 2, pressing of artemisia crude oil; 3, standing and layering of artemisia argyi crude oil hydrate; 4, rectification of artemisia argyi essential oil, namely a hydration liquid containing the artemisisa argyi at the upper part of the stood and layered artemisia argyi crude oil hydrate is led to the rectification procedure for rectification, as a result, the artemisia argyi is obtained. The slag is treated, the slag contains organic substances, and the pressed slag is shattered so as to obtain a raw material containing more than 45 percent of organic substances.
Description
Technical field
The present invention relates to the production method of plants essential oil, specifically utilize the plant argy wormwood to make raw material, the method for by physical squeezing processing treatment, high temperature rectifying separation, producing the argy wormwood essential oil.
Background technology
The main method of domestic production argy wormwood essential oil is steam distillation, organic solvent extractionprocess, carbon dioxide supercritical extraction method at present.
Steam distillation, the production technique circuit is long, and distil process is controlled on the plant argy wormwood, and distillation time is long, the product mix complicated component, and recovery rate is low, and the waste residue of generation is difficult for broken, and effective constituent wherein can not be extracted fully.
Organic solvent extractionprocess, with an organic solvent be generally methyl alcohol, acetone, after these chemical organic solvent extraction argy wormwood essential oils, must carry out nuisanceless disposal, has greater environmental impacts, and the organic solvent price of use is high, so production cost is higher.
Carbon dioxide supercritical extraction method, the postcritical meticulous equipment of requirement buying, one-time investment is large, and the operation work condition environment that supercritical extraction needs is good, and safety in production requires highly difficult large, and high to the requirement of workman's self diathesis, production cost is higher.
Summary of the invention
The purpose of this invention is to provide and a kind ofly can shorten the technological process of production, reduce production costs, safety and environmental protection, quality of workers requires relatively low, and waste residue easy to handle argy wormwood essential oil production technique.Can realize serialization, the large-scale production of argy wormwood essential oil.
A kind of production method of producing essential oil from the plant argy wormwood, step is as follows: 1, the pre-treatment of argy wormwood: by air-dry 3-5 days after bright argy wormwood screening, removal of impurities, remove surface-moisture, be cut into 10 millimeter, be the raw material of argy wormwood essential oil processing; 2, the squeezing of the thick oil of argy wormwood: raw material to be processed is dropped into and fills argy wormwood essential oil mother liquor jacket reactor, heat to 70 ℃, dissolve 1 hour, argy wormwood mixture after dissolving is dropped into to the squeezing of connecting rod squeezing machine, obtain argy wormwood essential oil hydrated mixture, to flow into subsequent processing from the lower end outlet containing the hydrated mixture of argy wormwood essential oil, waste residue therefrom brings out a mouthful discharge; 3, the thick profit compound of argy wormwood stratification: the hydrated mixture containing the argy wormwood essential oil is stored in stainless steel vessel, carries out the coarse filtration removal of contamination, stratification 4 hours; 4, the rectifying of argy wormwood essential oil: the hydration liquid input rectification working process rectifying by the upper part of stratification containing the argy wormwood essential oil obtain the argy wormwood essential oil.
The processing of tailings, tailings contains organic matter, and the residue after squeezing can be obtained containing raw material organic more than 45% through pulverizing.
The present invention and traditional steam distillation relatively have following advantages:
1, the comprehensive consumption of product significantly reduces.The tradition steam distillation adopts without squeezing argy wormwood raw material straight run distillation, and steam consumption is large, the time is long, 8 kilograms of vapor pressures of distillation maintenance for the first time 6 hours.The effective constituent of argy wormwood raw material needs the long period, and part is distilled out.After the squeezing of this process using rising temperature for dissolving, the effective constituent in argy wormwood is extruded out, and the just oil-water mixture of argy wormwood essential oil of this technique rectifying, can reduce steam consumption in a large number.(standing oil-water mixture rectifying gets final product in 2 hours on year-on-year basis) simple and clear process control condition.Residual essential oil in waste residue still can distill.
2, can continuous industrial production.The tradition steam distillation, must adopt still one a still distillation, is interrupted and produces, and can't reach the ability that industrial scale is produced, and the maximum yearly capacity of domestic like product is 20 tons.After the squeezing of this process using rising temperature for dissolving, the mugwort oil water mixture can store, and the mugwort oil water mixture stored is used in product rectifying, and rectification working process can be produced continuously.Tradition steam distillation and continuous processing are relatively.5 kg/hours of tradition steam distillation rectifying, 4 hours effective rectifying time of every day, i.e. 4 * 5=20 kilogram.Annual in 300 days, 6 tons of turnout.24 hours effective rectifying time of every day is produced in continuous processing rectifying, and 24 * 5=120 kilogram, annual in 300 days, 36 tons of turnout.
3, environment protection and comprehensive utilization.This technique is the sealing continuous process system, and steam heating system, material transport system, distillation system are not used any chemical goods and materials, do not produce waste gas waste water, and the waste residue frustillatum contains a large amount of organic matters, can make the raw material of fertilizer after fragmentation.
Specific embodiment
The enforcement embodiments of the invention below are provided, but are not limited to the present embodiment:
A kind of production method of producing essential oil from the plant argy wormwood is provided, and its step is as follows:
1,30 kilograms of screenings of bright argy wormwoods, removal of impurities are dried in the shade 3-5 days, be cut into 10 millimeters with interior short stem, is weighed as 21.5 kilograms;
2,21.5 kilograms of argy wormwood raw materials are dropped into to chuck reacting by heating still, in reactor, containing 10 kilograms of 10% argy wormwood essential oils, be warming up to 70 ℃ of insulations and within one hour, make the raw material preliminarily solubilised; With air compressor machine, mixture is pressed into to the squeezing of connecting rod squeezing machine, obtains 17.4 kilograms of argy wormwood essential oil water mixture, 13.6 kilograms, waste residue, detecting the argy wormwood essential oil content is 1.95 kilograms of 11.2%(argy wormwood essential oil net contents);
3, argy wormwood hydrated mixture crude product first carries out the coarse filtration removal of contamination, is stored in stainless steel vessel standing 4 little layereds;
4, the upper part hydrated mixture crude product of stratification carries out the rectifying filtration, controls 110 ℃ of rectification temperatures, time 2 h can obtain 1.68 kilograms of argy wormwood essential oils, deducts 1 kilogram of mother liquor preparation argy wormwood essential oil, and reality is received to obtain 0.68 kilogram of argy wormwood essential oil.
Although above shown detailed embodiment of the present invention, apparent, those skilled in the art is under prerequisite of the present invention, can carry out the part modifications and changes; The content that description is above mentioned is only as illustrative case, not as limitation of the present invention; Utilization with technical characterictic described herein provides a kind of production method of producing essential oil from the plant argy wormwood, all falls into this patent protection domain.
Claims (1)
1. a production method of producing essential oil from the plant argy wormwood, it is characterized in that: step is as follows: 1, the pre-treatment of argy wormwood: by air-dry 3-5 days after bright argy wormwood screening, removal of impurities, remove surface-moisture, be cut into 10 millimeter, be the raw material of argy wormwood essential oil processing; 2, the squeezing of the thick oil of argy wormwood: raw material to be processed is dropped into and fills argy wormwood essential oil mother liquor jacket reactor, heat to 70 ℃, dissolve 1 hour, argy wormwood mixture after dissolving is dropped into to the squeezing of connecting rod squeezing machine, obtain argy wormwood essential oil hydrated mixture, to flow into subsequent processing from the lower end outlet containing the hydrated mixture of argy wormwood essential oil, waste residue therefrom brings out a mouthful discharge; 3, the thick profit compound of argy wormwood stratification: the hydrated mixture containing the argy wormwood essential oil is stored in stainless steel vessel, carries out the coarse filtration removal of contamination, stratification 4 hours; 4, the rectifying of argy wormwood essential oil: the hydration liquid input rectification working process rectifying by the upper part of stratification containing the argy wormwood essential oil obtain the argy wormwood essential oil.
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| CN2013103256890A CN103421609A (en) | 2013-07-31 | 2013-07-31 | Production method for extracting essential oil from plant artemisia argyi |
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| CN2013103256890A CN103421609A (en) | 2013-07-31 | 2013-07-31 | Production method for extracting essential oil from plant artemisia argyi |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105462690A (en) * | 2015-11-18 | 2016-04-06 | 广州暨南生物医药研究开发基地有限公司 | Argy wormwood leaf essence oil and preparing method thereof |
| CN105713329A (en) * | 2016-02-01 | 2016-06-29 | 武汉威骏进出口贸易有限公司 | Preparation method of cinnamon essential oil slow-release type functional decorative material |
| CN105753369A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of eucalyptus essential oil slow-releasing type functional decorating material |
| CN105753368A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of jasminum essential oil sustained-release type functional decorative material |
| CN105754274A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of lavender essential oil slowly-releasing type functional decorative material |
| CN106188083A (en) * | 2016-07-28 | 2016-12-07 | 莫明鑫 | A method for extracting 1,8-cineole volatile oil from leaves of mugwort |
| CN106701326A (en) * | 2017-03-29 | 2017-05-24 | 董兰田 | Method for extracting mugwort essential oil with different volatility at different temperatures through segmented distillation refining |
| CN106833903A (en) * | 2017-03-29 | 2017-06-13 | 董兰田 | Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively |
| CN107164099A (en) * | 2017-07-10 | 2017-09-15 | 徐吉哲 | A kind of method that utilization way of distillation extracts wormwood essential oil |
| CN107384590A (en) * | 2017-06-15 | 2017-11-24 | 广东药科大学 | A kind of method for preparing high anti-aging effects sieve fairy maiden's essential oil and application |
| CN110655990A (en) * | 2019-10-08 | 2020-01-07 | 宫鹏 | Preparation method and application of traditional Chinese medicine wormwood essential oil |
| CN114507570A (en) * | 2022-03-11 | 2022-05-17 | 高州市健源农业有限公司 | Process for manufacturing high-purity moxa oil |
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| CN102600224A (en) * | 2012-04-20 | 2012-07-25 | 河南省医药科学研究院 | Wormwood leaf volatile oil and application thereof to preparation of anti-hepatitis B virus medicines |
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| CN101768516A (en) * | 2010-02-09 | 2010-07-07 | 浙江工业大学 | Tangerine oil and preparation method and application thereof |
| CN102600224A (en) * | 2012-04-20 | 2012-07-25 | 河南省医药科学研究院 | Wormwood leaf volatile oil and application thereof to preparation of anti-hepatitis B virus medicines |
Non-Patent Citations (1)
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Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105462690B (en) * | 2015-11-18 | 2019-02-15 | 广东暨晴生物医药科技有限公司 | A kind of mugwort essential oil and preparation method thereof |
| CN105462690A (en) * | 2015-11-18 | 2016-04-06 | 广州暨南生物医药研究开发基地有限公司 | Argy wormwood leaf essence oil and preparing method thereof |
| CN105754274B (en) * | 2016-02-01 | 2017-10-27 | 威骏（湖北）高新实业股份有限公司 | A kind of preparation method of Lavender spacetabs type functional ornamentation material |
| CN105713329A (en) * | 2016-02-01 | 2016-06-29 | 武汉威骏进出口贸易有限公司 | Preparation method of cinnamon essential oil slow-release type functional decorative material |
| CN105753369A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of eucalyptus essential oil slow-releasing type functional decorating material |
| CN105753368A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of jasminum essential oil sustained-release type functional decorative material |
| CN105754274A (en) * | 2016-02-01 | 2016-07-13 | 武汉威骏进出口贸易有限公司 | Preparation method of lavender essential oil slowly-releasing type functional decorative material |
| CN105753368B (en) * | 2016-02-01 | 2018-02-06 | 威骏（湖北）高新实业股份有限公司 | A kind of preparation method of refined jasmine oil spacetabs type functional ornamentation material |
| CN106188083B (en) * | 2016-07-28 | 2018-10-02 | 莫明鑫 | Method for extracting 1, 8-cineole volatile oil from folium artemisiae argyi |
| CN106188083A (en) * | 2016-07-28 | 2016-12-07 | 莫明鑫 | A method for extracting 1,8-cineole volatile oil from leaves of mugwort |
| CN106833903A (en) * | 2017-03-29 | 2017-06-13 | 董兰田 | Blue or green argy wormwood distillation, sedimentation separation are quenched take Chinese mugwort essential oil method respectively |
| CN106701326A (en) * | 2017-03-29 | 2017-05-24 | 董兰田 | Method for extracting mugwort essential oil with different volatility at different temperatures through segmented distillation refining |
| CN107384590A (en) * | 2017-06-15 | 2017-11-24 | 广东药科大学 | A kind of method for preparing high anti-aging effects sieve fairy maiden's essential oil and application |
| CN107164099A (en) * | 2017-07-10 | 2017-09-15 | 徐吉哲 | A kind of method that utilization way of distillation extracts wormwood essential oil |
| CN110655990A (en) * | 2019-10-08 | 2020-01-07 | 宫鹏 | Preparation method and application of traditional Chinese medicine wormwood essential oil |
| CN114507570A (en) * | 2022-03-11 | 2022-05-17 | 高州市健源农业有限公司 | Process for manufacturing high-purity moxa oil |
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Application publication date: 20131204 |