CN106833213A - A kind of environment-friendly waterborne aerosol paint and preparation method thereof - Google Patents
A kind of environment-friendly waterborne aerosol paint and preparation method thereof Download PDFInfo
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- CN106833213A CN106833213A CN201710136143.9A CN201710136143A CN106833213A CN 106833213 A CN106833213 A CN 106833213A CN 201710136143 A CN201710136143 A CN 201710136143A CN 106833213 A CN106833213 A CN 106833213A
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D133/00—Coating compositions based on homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and at least one being terminated by only one carboxyl radical, or of salts, anhydrides, esters, amides, imides, or nitriles thereof; Coating compositions based on derivatives of such polymers
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/20—Diluents or solvents
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/61—Additives non-macromolecular inorganic
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/60—Additives non-macromolecular
- C09D7/63—Additives non-macromolecular organic
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09D—COATING COMPOSITIONS, e.g. PAINTS, VARNISHES OR LACQUERS; FILLING PASTES; CHEMICAL PAINT OR INK REMOVERS; INKS; CORRECTING FLUIDS; WOODSTAINS; PASTES OR SOLIDS FOR COLOURING OR PRINTING; USE OF MATERIALS THEREFOR
- C09D7/00—Features of coating compositions, not provided for in group C09D5/00; Processes for incorporating ingredients in coating compositions
- C09D7/40—Additives
- C09D7/65—Additives macromolecular
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08K—Use of inorganic or non-macromolecular organic substances as compounding ingredients
- C08K2201/00—Specific properties of additives
- C08K2201/014—Additives containing two or more different additives of the same subgroup in C08K
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- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08L—COMPOSITIONS OF MACROMOLECULAR COMPOUNDS
- C08L2205/00—Polymer mixtures characterised by other features
- C08L2205/03—Polymer mixtures characterised by other features containing three or more polymers in a blend
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Paints Or Removers (AREA)
Abstract
The present invention relates to paint technology field, more particularly to a kind of environment-friendly waterborne aerosol paint suitable for woodenware, ironware and plastic cement and preparation method thereof.The environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：60 75 parts of organosilicon modified crylic acid resin, 20 35 parts of titanium dioxide, 0.2 0.5 parts of alkyl phenol polyglycol ether, 0.2 0.5 parts of fluorine surfactant, 0.1 0.2 parts of dimethyl silicone polymer, 0.5 2.0 parts of glycol monoethyl ether, 0.5 2.0 parts of ammonium hydroxide, 95% 5 10 parts of ethanol, appropriate deionized water, 100 120 parts of propellant.By designing and optimizing influence gloss of film, adhesive force, with the factor of weatherability etc., prepare that a kind of adhesive force is good, weatherability is strong, environment friendly and pollution-free waterborne aerosol paint, the environment-friendly waterborne aerosol paint is mainly used in the body surfaces such as ironware, woodwork, plastic cement, and the preparation method of the environment-friendly waterborne aerosol paint is simple, it is adaptable to industrial production.
Description
Technical field
The present invention relates to paint technology field, more particularly to a kind of environment-friendly water-based gas suitable for woodenware, ironware and plastic cement
Mist paint and preparation method thereof.
Background technology
Aerosol paint is also referred to as self-spraying paint or manually spray painting, generally by inhalator jar, aerosol valve, content (paint) and propellant group
Into, it is high-pressure filling after paint is processed by specific process, a kind of of convenient spraying paints.Self-spraying paint purposes is extremely wide,
Purposes repairing paint flaw from the outset develops into mould, industrial machinery, toy, handicraft, musical instrument, building, steel knot
The industry-by-industries such as structure, advertising industry, mark, scribble.Aerosol paint used on Vehicles Collected from Market, major part is to be with oil-based resin
Base-material, existing aerosol paint has that the content of organic solvent in high cost, and solvent-based paints is generally up to 50%
More than, the organic solvent in paint of being sprayed when using all can be evaporate into air, and this not only waste of resource is also caused sternly to environment
The pollution of weight, and more seriously the organic solvent in aerosol paint has certain toxicity mostly, these organic solvents can be straight
Connect the health of harmful to human.It is aqueous and waterborne aerosol paint then can well solve the environmentally friendly sex chromosome mosaicism of solvent-borne type aerosol paint presence
Aerosol paint has nontoxic, tasteless, free of contamination advantage, and water paint is the main development direction of current coating.But, existing water
Property aerosol paint need in terms of weatherability and adhesive force further raising.
The content of the invention
The present invention needs the problem of further raising for existing waterborne aerosol paint adhesive force and weatherability, there is provided a kind of
Suitable for the environment-friendly waterborne aerosol paint of woodenware, ironware and plastic cement, and this kind of preparation method of environment-friendly waterborne aerosol paint.
To achieve the above object, the present invention uses following technical scheme.
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
The present invention is made using this environment-friendly type aqueous resin of organosilicon modified crylic acid resin as film forming matter with deionized water
It is primary solvent, is designed and optimizes by the factor for influenceing the gloss of film of aerosol paint, adhesive force and weatherability etc., wraps
Include screening collocation, coalescents, wetting dispersing agent, adhesive agent, toughener etc. of research resin, have devised by said components and
The environment-friendly waterborne aerosol paint that ratio is prepared.
Preferably, the mean molecule quantity of organosilicon modified crylic acid resin is 20000-30000.
If the mean molecule quantity of the organosilicon modified crylic acid resin selected is too low, easy sagging during spraying, influence paint
Construction；If the mean molecule quantity of organosilicon modified crylic acid resin is too high paint film can be caused too thin, influence paint film adheres to and gloss
Deng paint performance.Organosilicon modified crylic acid resin is main film forming matter.
Preferably, the consumption of deionized water causes that viscosity of the environment-friendly waterborne aerosol paint before propellant is added is 36s.Go from
Sub- water is used as Principal diluent.
Preferably, titanium dioxide is rutile type titanium white.
Preferably, propellant is dimethyl ether.
It is another aspect of this invention to provide that there is provided a kind of preparation method of environment-friendly waterborne aerosol paint, comprising the following steps：
S1, weighs organosilicon modified crylic acid resin 25-30 parts, titanium dioxide 20-35 parts, the poly- second two of alkyl phenol by weight
Alcohol ether 0.2-0.5 parts, fluorine surfactant 0.2-0.5 parts, 95% ethanol 5-10 parts, it is well mixed, is ground to fineness less than 25 μ
m；
S2, to sequentially adding organosilicon modified crylic acid resin 35-45 parts, poly dimethyl in compound obtained in step S1
Siloxanes 0.1-0.2 parts, glycol monoethyl ether 0.5-2.0 parts, ammonium hydroxide 0.5-2.0 parts, with the speed of 800-1200r/min
Stirring 10-20 minutes；
S3, compound obtained in step S2 is diluted with deionized water, and viscosity is adjusted into 36s by deionized water, so
It is filling afterwards and fill 100-120 parts of dimethyl ether.
The preparation method is simple, and it is to control the grinding of paint less than 25 μm that mixture is ground into fineness in step S1
Degree；It is the viscosity in order to control paint filling that viscosity is controlled into 36s in step S3.
Preferably, mixing speed is 1000r/min in step S2, and mixing time is 15min.
Compared with prior art, the beneficial effects of the invention are as follows：The present invention is by design and optimization influence gloss of film, attached
Put forth effort the factor with weatherability etc., prepared that a kind of adhesive force is good, weatherability is strong, environment friendly and pollution-free waterborne aerosol paint,
The environment-friendly waterborne aerosol paint is mainly used in the body surfaces such as ironware, woodwork, plastic cement, and the environment-friendly waterborne aerosol paint preparation side
Method is simple, it is adaptable to industrial production.
Specific embodiment
In order to more fully understand technology contents of the invention, with reference to specific embodiment to technical scheme
It is described further and illustrates.
Embodiment 1
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
Environment-friendly waterborne aerosol paint is prepared as follows：
S1,25 parts of organosilicon modified crylic acid resin is weighed by weight, 35 parts of rutile type titanium white, the poly- second of alkyl phenol
0.2 part of glycol ethers, 0.2 part of fluorine surfactant, 95% 5 parts of ethanol is well mixed, and is ground with sand mill, is ground to thin
Degree is less than 25 μm；
S2, in step S1 prepare compound in sequentially add 35 parts of organosilicon modified crylic acid resin, poly dimethyl
0.1 part of siloxanes, 0.5 part of ethylene glycol single methyl ether, 0.5 part of ammonium hydroxide, 1000r/min high-speed stirreds 15 minutes；
S3, obtained compound in step S2 is diluted with deionized water, and adjusts viscosity for 36s, filling and 100 parts of filling
Dimethyl ether, thus obtains environment-friendly waterborne aerosol paint.(viscosity unit s is Chai Shi glasss of viscosity unit herein, with the full oil of Chai Shi cups
Paint, makes to calculate the delivery time under paint vertical current and with stopwatch.)
Embodiment 2
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
Environment-friendly waterborne aerosol paint is prepared as follows：
S1,30 parts of organosilicon modified crylic acid resin is weighed by weight, 35 parts of rutile type titanium white, the poly- second of alkyl phenol
0.2 part of glycol ethers, 0.2 part of fluorine surfactant, 95% 5 parts of ethanol is well mixed, and is ground with sand mill, is ground to thin
Degree is less than 25 microns；
S2, in step S1 prepare compound in sequentially add 35 parts of organosilicon modified crylic acid resin, poly dimethyl
0.1 part of siloxanes, 0.5 part of ethylene glycol single methyl ether, 1.0 parts of ammonium hydroxide, 1000r/min high-speed stirreds 15 minutes；
S3, obtained compound in step S2 is diluted with deionized water, and adjusts viscosity for 36s, filling and 110 parts of filling
Dimethyl ether, thus obtains environment-friendly waterborne aerosol paint.
Embodiment 3
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
Environment-friendly waterborne aerosol paint is prepared as follows：
S1,25 parts of organosilicon modified crylic acid resin is weighed by weight, 35 parts of rutile type titanium white, the poly- second of alkyl phenol
0.2 part of glycol ethers, 0.2 part of fluorine surfactant, 95% 5 parts of ethanol is well mixed, and is ground with sand mill, is ground to thin
Degree is less than 25 μm；
S2, in step S1 prepare compound in sequentially add 35 parts of organosilicon modified crylic acid resin, poly dimethyl
0.1 part of siloxanes, 0.5 part of ethylene glycol single methyl ether, 2.0 parts of ammonium hydroxide, 1000r/min high-speed stirreds 15 minutes；
S3, obtained compound in step S2 is diluted with deionized water, and adjusts viscosity for 36s, filling and 120 parts of filling
Dimethyl ether, thus obtains environment-friendly waterborne aerosol paint.
Embodiment 4
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
75 parts of organosilicon modified crylic acid resin,
20 parts of rutile type titanium white,
0.5 part of alkyl phenol polyglycol ether,
2.0 parts of fluorine surfactant,
0.2 part of dimethyl silicone polymer,
2.0 parts of glycol monoethyl ether,
1.5 parts of ammonium hydroxide,
95% 10 parts of ethanol,
Appropriate deionized water,
110 parts of dimethyl ether.
Environment-friendly waterborne aerosol paint is prepared as follows：
S1,35 parts of organosilicon modified crylic acid resin is weighed by weight, 20 parts of rutile type titanium white, the poly- second of alkyl phenol
0.5 part of glycol ethers, 2.0 parts of fluorine surfactant, 95% 10 parts of ethanol is well mixed, and is ground with sand mill, is ground to thin
Degree is less than 25 μm；
S2, in step S1 prepare compound in sequentially add 40 parts of organosilicon modified crylic acid resin, poly dimethyl
0.2 part of siloxanes, 2.0 parts of ethylene glycol single methyl ether, 1.5 parts of ammonium hydroxide, 800r/min high-speed stirreds 20 minutes；
S3, obtained compound in step S2 is diluted with deionized water, and adjusts viscosity for 36s, filling and 110 parts of filling
Dimethyl ether, thus obtains environment-friendly waterborne aerosol paint.
Embodiment 5
A kind of environment-friendly waterborne aerosol paint, is made up of the component of following weight portion：
Environment-friendly waterborne aerosol paint is prepared as follows：
S1,30 parts of organosilicon modified crylic acid resin is weighed by weight, 25 parts of rutile type titanium white, the poly- second of alkyl phenol
0.3 part of glycol ethers, 0.5 part of fluorine surfactant, 95% 8 parts of ethanol is well mixed, and is ground with sand mill, is ground to thin
Degree is less than 25 μm；
S2, in step S1 prepare compound in sequentially add 35 parts of organosilicon modified crylic acid resin, poly dimethyl
0.15 part of siloxanes, 1.0 parts of ethylene glycol single methyl ether, 1.5 parts of ammonium hydroxide, 1200r/min high-speed stirreds 10 minutes；
S3, obtained compound in step S2 is diluted with deionized water, and adjust viscosity for 36s, it is filling and fill 120 parts
Dimethyl ether, thus obtains environment-friendly waterborne aerosol paint.
Performance test
The environment-friendly waterborne aerosol paint prepared for embodiment 1-3 carries out various performance tests, and test result is as shown in the table：
Paint service check table
From above-described embodiment and the performance test results, waterborne aerosol paint adhesive force of the invention is good, weatherability strong, ring
Protect pollution-free.
The above only further illustrates technology contents of the invention with embodiment, is easier to understand in order to reader,
But embodiments of the present invention not being represented and being only limitted to this, any technology done according to the present invention extends or recreates, and is sent out by this
Bright protection.
Claims (7)
1. a kind of environment-friendly waterborne aerosol paint, it is characterised in that be made up of the component of following weight portion：
2. environment-friendly waterborne aerosol paint according to claim 1, it is characterised in that the organosilicon modified crylic acid resin
Mean molecule quantity is 20000-30000.
3. environment-friendly waterborne aerosol paint according to claim 1, it is characterised in that the consumption of the deionized water causes described
Viscosity of the environment-friendly waterborne aerosol paint before propellant is added is 36s.
4. environment-friendly waterborne aerosol paint according to claim 1, it is characterised in that the titanium dioxide is rutile titanium dioxide
Powder.
5. environment-friendly waterborne aerosol paint according to claim 1, it is characterised in that the propellant is dimethyl ether.
6. a kind of preparation method of environment-friendly waterborne aerosol paint as claimed in claim 1, it is characterised in that comprise the following steps：
S1, weighs 25-30 parts of organosilicon modified crylic acid resin resin, titanium dioxide 20-35 parts, the poly- second two of alkyl phenol by weight
Alcohol ether 0.2-0.5 parts, fluorine surfactant 0.2-0.5 parts, 95% ethanol 5-10 parts, it is well mixed, is ground to fineness less than 25 μ
m；
S2, to sequentially adding organosilicon modified crylic acid resin 35-45 parts, poly dimethyl in compound obtained in the step S1
Siloxanes 0.1-0.2 parts, glycol monoethyl ether 0.5-2.0 parts, ammonium hydroxide 0.5-2.0 parts, stirred with the speed of 1000r/min
10-20 minutes；
S3, compound obtained in the step S2 is diluted with deionized water, and adjusts viscosity for 36s, filling and fill 100-120
Part dimethyl ether, thus obtains the environment-friendly waterborne aerosol paint.
7. the preparation method of the environment-friendly waterborne aerosol paint described in claim 6, it is characterised in that mixing speed in the step S2
It is 1000r/min, mixing time is 15min.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710136143.9A CN106833213A (en) | 2017-03-08 | 2017-03-08 | A kind of environment-friendly waterborne aerosol paint and preparation method thereof |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201710136143.9A CN106833213A (en) | 2017-03-08 | 2017-03-08 | A kind of environment-friendly waterborne aerosol paint and preparation method thereof |
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ID=59144162
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| CN201710136143.9A Pending CN106833213A (en) | 2017-03-08 | 2017-03-08 | A kind of environment-friendly waterborne aerosol paint and preparation method thereof |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108084822A (en) * | 2017-12-18 | 2018-05-29 | 肇庆欧迪斯实业有限公司 | The reflective aerosol paint of aqueous, environmental protective and the reflective aerosol paint device of aqueous, environmental protective |
| CN114687237A (en) * | 2020-12-28 | 2022-07-01 | 广东三和化工科技有限公司 | Environment-friendly type document file protection aerosol paint and preparation method thereof |
| CN115851029A (en) * | 2022-11-03 | 2023-03-28 | 广东自由能科技股份有限公司 | Production process and application of road marking paint |
| CN116082900A (en) * | 2022-10-19 | 2023-05-09 | 广东自由能科技股份有限公司 | Aerosol paint suitable for asphalt pavement marking and preparation method thereof |
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| EP1132443A2 (en) * | 2000-02-29 | 2001-09-12 | Dow Corning Toray Silicone Company, Ltd. | Method for producing water based coating compositions |
| CN105820643A (en) * | 2016-05-04 | 2016-08-03 | 雅图高新材料有限公司 | Diluent special for waterborne single-component automobile paint |
| CN105860710A (en) * | 2016-06-06 | 2016-08-17 | 广东莱雅化工有限公司 | Waterborne gas spray paint |
| CN105949914A (en) * | 2016-06-16 | 2016-09-21 | 中山市汉艺涂料有限公司 | Waterborne glass baking paint and preparation method thereof |
| CN106118399A (en) * | 2016-07-01 | 2016-11-16 | 太仓市金新涂料有限公司 | A kind of high-strength abrasion-proof modified poly ester amino-stoving varnish and preparation method thereof |
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2017
- 2017-03-08 CN CN201710136143.9A patent/CN106833213A/en active Pending
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP1132443A2 (en) * | 2000-02-29 | 2001-09-12 | Dow Corning Toray Silicone Company, Ltd. | Method for producing water based coating compositions |
| CN105820643A (en) * | 2016-05-04 | 2016-08-03 | 雅图高新材料有限公司 | Diluent special for waterborne single-component automobile paint |
| CN105860710A (en) * | 2016-06-06 | 2016-08-17 | 广东莱雅化工有限公司 | Waterborne gas spray paint |
| CN105949914A (en) * | 2016-06-16 | 2016-09-21 | 中山市汉艺涂料有限公司 | Waterborne glass baking paint and preparation method thereof |
| CN106118399A (en) * | 2016-07-01 | 2016-11-16 | 太仓市金新涂料有限公司 | A kind of high-strength abrasion-proof modified poly ester amino-stoving varnish and preparation method thereof |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108084822A (en) * | 2017-12-18 | 2018-05-29 | 肇庆欧迪斯实业有限公司 | The reflective aerosol paint of aqueous, environmental protective and the reflective aerosol paint device of aqueous, environmental protective |
| CN114687237A (en) * | 2020-12-28 | 2022-07-01 | 广东三和化工科技有限公司 | Environment-friendly type document file protection aerosol paint and preparation method thereof |
| CN116082900A (en) * | 2022-10-19 | 2023-05-09 | 广东自由能科技股份有限公司 | Aerosol paint suitable for asphalt pavement marking and preparation method thereof |
| CN115851029A (en) * | 2022-11-03 | 2023-03-28 | 广东自由能科技股份有限公司 | Production process and application of road marking paint |
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Application publication date: 20170613 |
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