CN106829219A - A kind of safe storage method of thiazole - Google Patents
A kind of safe storage method of thiazole Download PDFInfo
- Publication number
- CN106829219A CN106829219A CN201611233091.9A CN201611233091A CN106829219A CN 106829219 A CN106829219 A CN 106829219A CN 201611233091 A CN201611233091 A CN 201611233091A CN 106829219 A CN106829219 A CN 106829219A
- Authority
- CN
- China
- Prior art keywords
- thiazole
- hermetically sealed
- container
- mentioned
- freezer
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
- B65D85/70—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for
- B65D85/82—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for for poisons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D53/00—Sealing or packing elements; Sealings formed by liquid or plastics material
- B65D53/06—Sealings formed by liquid or plastic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
- B65D81/18—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
- B65D81/18—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient
- B65D81/20—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas
- B65D81/2007—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas under vacuum
- B65D81/2038—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas under vacuum with means for establishing or improving vacuum
Landscapes
- Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Toxicology (AREA)
- Packages (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
A kind of conventional storage method of thiazole, is related to medicine intermediate processing technique field, and the water seal after collecting thiazole pretreatment, packet is bottled, then after hermetically sealed can storage, you can.Beneficial effects of the present invention are：Present invention determine that being conducive to the suitable condition of the storage of thiazole, rational temperature, humidity in storehouse when ensure that thiazole is stored, solve the problems, such as that thiazole volatilizees and be denatured during preservation, improve the storage time of thiazole, the actual performance of thiazole will not be destroyed, is easy to long storage.
Description
Technical field
The present invention relates to medicine intermediate processing technique field, and in particular to a kind of safe storage method of thiazole.
Background technology
Thiazole, molecular formula：C3H3NS, outward appearance and proterties are colourless or faint yellow, have off-odor, liquid, can serve as
Organic synthesis reagent, for synthetic drug, dyestuff, rubber accelerator, film quality, bactericide and dyestuff etc.；Thiazole has necessarily
Toxicity, suction, intake or after skin absorption it is harmful to body, have stimulation to eyes and skin, meanwhile, thiazole is also
Combustible material, meet naked light, hyperpyrexia or and oxidising agent, have the danger for causing combustion explosion, therefore when stored, it is necessary to pacify
Entirely, but do not have a kind of store method of comparatively scientific system presently, therefore research is a kind of with safe, simple
And systematic science thiazole storage method, it is the technology of current more active demand.
The content of the invention：
The technical problems to be solved by the invention are to provide a kind of storage method scientific system, it is ensured that thiazole performance safety
Thiazole conventional storage method.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of conventional storage method of thiazole, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must pure substance remaining impurity；
2., the thiazole by above-mentioned collection is tentatively cleared up, and goes the removal of impurity, is placed in multiple containers respectively, then will
Container is placed in freezer, and regulation storehouse temperature is 2-5 DEG C；
3., by humidity regulation in above-mentioned freezer to 20-30%, then regulation of carbon dioxide content is 24-35%；
4., clear water will be filled in the container of above-mentioned filling thiazole, clear water to be higher by thiazole liquid level 3-5cm, then gently
It is micro- rock after, stand；
5. a hermetically sealed can, is taken, hermetically sealed can is for glass jar and glass is dark-brown glass, and seals pot bottom and lay one layer
Quick lime, then lays one layer of soft cloth on quick lime, per 6-8 is then one group by said vesse, is placed in hermetically sealed can,
Sealing；
6. air humidity in above-mentioned hermetically sealed can, is adjusted to 25-30%, after being then evacuated to vacuum, is sealed, and close
Sealed cans tank mouth smears sealing using wax oil；
7., each is once checked in freezer air humidity in humiture and hermetically sealed can for one week, and checks hermetically sealed can
Interior vacuum, the clear water content in container, until taking-up is used.
Described container is the conical flask added a cover, and bore is smaller, it is to avoid volatilization；
Beneficial effects of the present invention are：Present invention determine that being conducive to the suitable condition of the storage of thiazole, it is ensured that thiazole
Rational temperature, humidity in storehouse during storage, solve the problems, such as that thiazole volatilizees and be denatured during preservation, improve thiazole
Storage time, the actual performance of thiazole will not be destroyed, be easy to long storage.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of conventional storage method of Beta-alanine, comprises the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must pure substance remaining impurity；
2., the thiazole by above-mentioned collection is tentatively cleared up, and goes the removal of impurity, is placed in multiple containers respectively, then will
Container is placed in freezer, and regulation storehouse temperature is 5 DEG C；
3., by humidity regulation in above-mentioned freezer to 30%, then regulation of carbon dioxide content is 35%；
4., clear water will be filled in the container of above-mentioned filling thiazole, clear water to be higher by thiazole liquid level 5cm, then slightly
After rocking, stand；
5. a hermetically sealed can, is taken, hermetically sealed can is for glass jar and glass is dark-brown glass, and seals pot bottom and lay one layer
Quick lime, then lays one layer of soft cloth on quick lime, is then one group by every 8 of said vesse, is placed in hermetically sealed can, close
Envelope；
6. air humidity in above-mentioned hermetically sealed can, is adjusted to 30%, after being then evacuated to vacuum, is sealed, and in sealing
Tank tank mouth smears sealing using wax oil；
7., each is once checked in freezer air humidity in humiture and hermetically sealed can for one week, and checks hermetically sealed can
Interior vacuum, the clear water content in container, until taking-up is used.
Embodiment 2
A kind of conventional storage method of Beta-alanine, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must pure substance remaining impurity；
2., the thiazole by above-mentioned collection is tentatively cleared up, and goes the removal of impurity, is placed in multiple containers respectively, then will
Container is placed in freezer, and regulation storehouse temperature is 2 DEG C；
3., by humidity regulation in above-mentioned freezer to 20%, then regulation of carbon dioxide content is 24%；
4., clear water will be filled in the container of above-mentioned filling thiazole, clear water to be higher by thiazole liquid level 3cm, then slightly
After rocking, stand；
5. a hermetically sealed can, is taken, hermetically sealed can is for glass jar and glass is dark-brown glass, and seals pot bottom and lay one layer
Quick lime, then lays one layer of soft cloth on quick lime, is then one group by every 6 of said vesse, is placed in hermetically sealed can, close
Envelope；
6. air humidity in above-mentioned hermetically sealed can, is adjusted to 25%, after being then evacuated to vacuum, is sealed, and in sealing
Tank tank mouth smears sealing using wax oil；
7., each is once checked in freezer air humidity in humiture and hermetically sealed can for one week, and checks hermetically sealed can
Interior vacuum, the clear water content in container, until taking-up is used.
General principle of the invention and principal character and advantages of the present invention has been shown and described above.The technology of the industry
Personnel it should be appreciated that the present invention is not limited to the above embodiments, simply explanation described in above-described embodiment and specification this
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appending claims and its
Equivalent thereof.
Claims (2)
1. a kind of conventional storage method of thiazole, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must pure substance remaining impurity；
2., the thiazole by above-mentioned collection is tentatively cleared up, and goes the removal of impurity, is placed in multiple containers respectively, then by container
It is placed in freezer, regulation storehouse temperature is 2-5 DEG C；
3., by humidity regulation in above-mentioned freezer to 20-30%, then regulation of carbon dioxide content is 24-35%；
4., clear water will be filled in the container of above-mentioned filling thiazole, then clear water slightly shakes to be higher by thiazole liquid level 3-5cm
After rolling, stand；
5. a hermetically sealed can, is taken, hermetically sealed can is for glass jar and glass is dark-brown glass, and seals pot bottom and lay one layer of raw stone
Ash, then lays one layer of soft cloth on quick lime, per 6-8 is then one group by said vesse, is placed in hermetically sealed can, close
Envelope；
6. air humidity in above-mentioned hermetically sealed can, is adjusted to 25-30%, after being then evacuated to vacuum, is sealed, and in hermetically sealed can
Tank mouth smears sealing using wax oil；
7., each is once checked in freezer air humidity in humiture and hermetically sealed can for one week, and is checked in hermetically sealed can
Vacuum, the clear water content in container, until taking-up is used.
2. the conventional storage method of a kind of Beta-alanine according to claim 1, it is characterised in that：Described container is to add
The conical flask of lid.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611233091.9A CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611233091.9A CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106829219A true CN106829219A (en) | 2017-06-13 |
| CN106829219B CN106829219B (en) | 2018-02-27 |
Family
ID=59113856
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611233091.9A Active CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106829219B (en) |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1523020A (en) * | 2003-02-20 | 2004-08-25 | Process for preparing storage-stable benzothiazolyl sulfenamides | |
| WO2016042980A1 (en) * | 2014-09-16 | 2016-03-24 | 株式会社サクラクレパス | Ink composition for plasma treatment detection, and plasma treatment detection indicator |
-
2016
- 2016-12-28 CN CN201611233091.9A patent/CN106829219B/en active Active
Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1523020A (en) * | 2003-02-20 | 2004-08-25 | Process for preparing storage-stable benzothiazolyl sulfenamides | |
| WO2016042980A1 (en) * | 2014-09-16 | 2016-03-24 | 株式会社サクラクレパス | Ink composition for plasma treatment detection, and plasma treatment detection indicator |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106829219B (en) | 2018-02-27 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| JP2020023363A (en) | Container with excellent airtightness, and method for holding gas molecules or volatile components in container | |
| AR010980A1 (en) | METHOD AND APPARATUS FOR PACKING A PRODUCT IN A DOUBLE-LID PACK | |
| CN101401769A (en) | Package container for sodium bicarbonate injection and method of preparing the same | |
| CN103381933B (en) | Extend the apparatus and method of seed storage time | |
| CN106829219B (en) | A kind of safe storage method of thiazole | |
| CN101631726A (en) | Method for storing ampoules containing pharmaceutical agents in a closed container containing an oxygen scavenger | |
| CN204416084U (en) | A kind of precision instrument storage and conveying box | |
| CN203776007U (en) | Liquid nitrogen container for long-term storage of cells and biological materials | |
| JP2006206140A (en) | Sterilization packing method of two-closure-having pouch | |
| CN201971273U (en) | Packaging container for storing and transporting anaerobically fermented food | |
| CN206851647U (en) | Plant cultivation box structure | |
| CN206219609U (en) | Tissue cultuer bottle | |
| CN205274120U (en) | A get wine device for wine jar | |
| CN204184673U (en) | Gathering formula packing box | |
| CN203227028U (en) | Sodium bicarbonate injection flexible package container | |
| CN203107694U (en) | Sodium bicarbonate injection flexible package | |
| CN205145121U (en) | Medicinal bottle of dampproofing formula | |
| CN106497768A (en) | A kind of Cordyceps militaris culture dish of sealing ventilation | |
| CN204643839U (en) | A kind of preparation facilities of chlorine dioxide with high purity | |
| CN210028601U (en) | Novel bottle for vacuum preservation | |
| CN218641358U (en) | Armillaria mellea packaging bottle | |
| CN205161804U (en) | Special pickle jar in laboratory | |
| CN204016863U (en) | A kind of vertical polypropylene transfusion bag | |
| CN203263810U (en) | Sodium bicarbonate injection flexible package container | |
| CN203139110U (en) | Flexible package for sodium bicarbonate injection |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PB01 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20191202 Address after: 264200 Qingdao middle road-132f-09009, Weihai Economic and Technological Development Zone, Shandong Province Patentee after: Weihai Houpu Biotechnology Co.,Ltd. Address before: 233700 Guzhen Economic Development Zone, Bengbu, Anhui Patentee before: ANHUI HONGSHENG BIOLOGICAL CO.,LTD. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20220228 Address after: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee after: Chenghong Pharmaceutical (Weihai) Co.,Ltd. Address before: 264200-132f-09009, Qingdao Middle Road, Weihai Economic and Technological Development Zone, Shandong Province Patentee before: Weihai Houpu Biotechnology Co.,Ltd. |
|
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20230724 Address after: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee after: Chenghong Pharmaceutical (Weihai) Co.,Ltd. Patentee after: Weihai Houpu Biotechnology Co.,Ltd. Address before: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee before: Chenghong Pharmaceutical (Weihai) Co.,Ltd. |