CN106829219B - A kind of safe storage method of thiazole - Google Patents
A kind of safe storage method of thiazole Download PDFInfo
- Publication number
- CN106829219B CN106829219B CN201611233091.9A CN201611233091A CN106829219B CN 106829219 B CN106829219 B CN 106829219B CN 201611233091 A CN201611233091 A CN 201611233091A CN 106829219 B CN106829219 B CN 106829219B
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- CN
- China
- Prior art keywords
- thiazole
- hermetically sealed
- container
- freezer
- clear water
- Prior art date
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Classifications
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D85/00—Containers, packaging elements or packages, specially adapted for particular articles or materials
- B65D85/70—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for
- B65D85/82—Containers, packaging elements or packages, specially adapted for particular articles or materials for materials not otherwise provided for for poisons
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D53/00—Sealing or packing elements; Sealings formed by liquid or plastics material
- B65D53/06—Sealings formed by liquid or plastic material
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
- B65D81/18—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B65—CONVEYING; PACKING; STORING; HANDLING THIN OR FILAMENTARY MATERIAL
- B65D—CONTAINERS FOR STORAGE OR TRANSPORT OF ARTICLES OR MATERIALS, e.g. BAGS, BARRELS, BOTTLES, BOXES, CANS, CARTONS, CRATES, DRUMS, JARS, TANKS, HOPPERS, FORWARDING CONTAINERS; ACCESSORIES, CLOSURES, OR FITTINGS THEREFOR; PACKAGING ELEMENTS; PACKAGES
- B65D81/00—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents
- B65D81/18—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient
- B65D81/20—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas
- B65D81/2007—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas under vacuum
- B65D81/2038—Containers, packaging elements, or packages, for contents presenting particular transport or storage problems, or adapted to be used for non-packaging purposes after removal of contents providing specific environment for contents, e.g. temperature above or below ambient under vacuum or superatmospheric pressure, or in a special atmosphere, e.g. of inert gas under vacuum with means for establishing or improving vacuum
Abstract
A kind of conventional storage method of thiazole, is related to medicine intermediate processing technique field, by collect thiazole pretreatment after water seal, packet it is bottled, then hermetically sealed can storage after, you can.Beneficial effects of the present invention are：Present invention determine that be advantageous to the suitable condition of the storage of thiazole, rational temperature, humidity in storehouse when ensure that thiazole storage, solve the problems, such as that thiazole volatilizees and is denatured during preservation, improve the storage time of thiazole, the actual performance of thiazole will not be destroyed, is easy to long storage.
Description
Technical field
The present invention relates to medicine intermediate processing technique field, and in particular to a kind of safe storage method of thiazole.
Background technology
Thiazole, molecular formula：C3H3NS, outward appearance and character are colourless or faint yellow, have off-odor, liquid, be may be used as
Organic synthesis reagent, for synthetic drug, dyestuff, rubber accelerator, film quality, bactericide and dyestuff etc.；Thiazole has necessarily
Toxicity, suction, intake or body is harmful to after skin absorbs, have stimulation to eyes and skin, meanwhile, thiazole is also
Combustible material, meet naked light, high fever or contacted with oxidant, there is the danger for causing combustion explosion, therefore when stored, it is necessary to pacify
Entirely, but do not have a kind of store method of comparatively scientific system presently, therefore study a kind of with safe, simple
And systematic science thiazole storage method, be more active demand at present technology.
The content of the invention：
The technical problems to be solved by the invention are to provide a kind of storage method scientific system, guarantee thiazole performance safety
Thiazole conventional storage method.
The technical problems to be solved by the invention are realized using following technical scheme：
A kind of conventional storage method of thiazole, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must be pure without remaining impurity；
2., the thiazole of above-mentioned collection tentatively cleared up, be placed in multiple containers, be then placed in container respectively
In freezer, regulation storehouse temperature is 2-5 DEG C；
3., by humidity regulation in above-mentioned freezer to 20-30%, then regulation of carbon dioxide content is 24-35%；
4., clear water will be filled in the container of filling thiazole, then clear water is slightly shaken with being higher by thiazole liquid level 3-5cm
After rolling, stand；
5., take a hermetically sealed can, hermetically sealed can is glass jar and glass is dark-brown glass, and seal pot bottom lay one layer
Quick lime, one layer of soft cloth is then laid on quick lime, is then one group per 6-8 by said vesse, is placed in hermetically sealed can,
Sealing；
6., air humidity in above-mentioned hermetically sealed can is adjusted to 25-30%, after being then evacuated to vacuum, seal, and close
Sealed cans tank mouth smears sealing using wax oil；
7., air humidity in humiture and hermetically sealed can in examinations occur every other week freezer, and check hermetically sealed can
Interior vacuum, the clear water content in container, used until taking out.
Described container is the conical flask of capping, and bore is smaller, avoids volatilizing；
Beneficial effects of the present invention are：Present invention determine that being advantageous to the suitable condition of the storage of thiazole, thiazole ensure that
Rational temperature, humidity in storehouse during storage, solve the problems, such as that thiazole volatilizees and is denatured during preservation, improve thiazole
Storage time, the actual performance of thiazole will not be destroyed, be easy to long storage.
Embodiment
In order that the technical means, the inventive features, the objects and the advantages of the present invention are easy to understand, tie below
Specific embodiment is closed, the present invention is expanded on further.
Embodiment 1
A kind of conventional storage method of thiazole, comprises the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must be pure without remaining impurity；
2., the thiazole of above-mentioned collection tentatively cleared up, be placed in multiple containers, be then placed in container respectively
In freezer, regulation storehouse temperature is 5 DEG C；
3., by humidity regulation in above-mentioned freezer to 30%, then regulation of carbon dioxide content is 35%；
4., clear water will be filled in the container of filling thiazole, clear water is to be higher by thiazole liquid level 5cm, then slight wobble
Afterwards, stand；
5., take a hermetically sealed can, hermetically sealed can is glass jar and glass is dark-brown glass, and seal pot bottom lay one layer
Quick lime, one layer of soft cloth is then laid on quick lime, be then one group by every 8 of said vesse, be placed in hermetically sealed can, it is close
Envelope；
6., air humidity in above-mentioned hermetically sealed can is adjusted to 30%, after being then evacuated to vacuum, seal, and sealing
Tank tank mouth smears sealing using wax oil；
7., air humidity in humiture and hermetically sealed can in examinations occur every other week freezer, and check hermetically sealed can
Interior vacuum, the clear water content in container, used until taking out.
Embodiment 2
A kind of conventional storage method of thiazole, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must be pure without remaining impurity；
2., the thiazole of above-mentioned collection tentatively cleared up, be placed in multiple containers, be then placed in container respectively
In freezer, regulation storehouse temperature is 2 DEG C；
3., by humidity regulation in above-mentioned freezer to 20%, then regulation of carbon dioxide content is 24%；
4., clear water will be filled in the container of filling thiazole, clear water is to be higher by thiazole liquid level 3cm, then slight wobble
Afterwards, stand；
5., take a hermetically sealed can, hermetically sealed can is glass jar and glass is dark-brown glass, and seal pot bottom lay one layer
Quick lime, one layer of soft cloth is then laid on quick lime, be then one group by every 6 of said vesse, be placed in hermetically sealed can, it is close
Envelope；
6., air humidity in above-mentioned hermetically sealed can is adjusted to 25%, after being then evacuated to vacuum, seal, and sealing
Tank tank mouth smears sealing using wax oil；
7., air humidity in humiture and hermetically sealed can in examinations occur every other week freezer, and check hermetically sealed can
Interior vacuum, the clear water content in container, used until taking out.
The general principle and principal character and advantages of the present invention of the present invention has been shown and described above.The technology of the industry
Personnel are it should be appreciated that the present invention is not limited to the above embodiments, and the simply explanation described in above-described embodiment and specification is originally
The principle of invention, without departing from the spirit and scope of the present invention, various changes and modifications of the present invention are possible, these changes
Change and improvement all fall within the protetion scope of the claimed invention.The claimed scope of the invention by appended claims and its
Equivalent thereof.
Claims (2)
1. a kind of conventional storage method of thiazole, it is characterised in that comprise the following steps：
1., collect or newly configure thiazole, the thiazole of collection is no more than 5h, and thiazole must be pure without remaining impurity；
2., the thiazole of above-mentioned collection tentatively cleared up, be placed in respectively in multiple containers, container be then placed in freezer
In, regulation storehouse temperature is 2-5 DEG C；
3., by humidity regulation in above-mentioned freezer to 20-30%, then regulation of carbon dioxide content is 24-35%；
4., clear water will be filled in the container of filling thiazole, clear water is to be higher by thiazole liquid level 3-5cm, then after slight wobble,
Stand；
5., take a hermetically sealed can, hermetically sealed can is glass jar and glass is dark-brown glass, and seal pot bottom lay one layer of raw stone
Ash, one layer of soft cloth is then laid on quick lime, be then one group per 6-8 by said vesse, be placed in hermetically sealed can, it is close
Envelope；
6., air humidity in above-mentioned hermetically sealed can is adjusted to 25-30%, after being then evacuated to vacuum, seal, and in hermetically sealed can
Tank mouth smears sealing using wax oil；
7., air humidity in humiture and hermetically sealed can in examinations occur every other week freezer, and check in hermetically sealed can
Vacuum, the clear water content in container, used until taking out.
A kind of 2. conventional storage method of thiazole according to claim 1, it is characterised in that：Described container is capping
Conical flask.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611233091.9A CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201611233091.9A CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106829219A CN106829219A (en) | 2017-06-13 |
| CN106829219B true CN106829219B (en) | 2018-02-27 |
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201611233091.9A Active CN106829219B (en) | 2016-12-28 | 2016-12-28 | A kind of safe storage method of thiazole |
Country Status (1)
| Country | Link |
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| CN (1) | CN106829219B (en) |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10307138A1 (en) * | 2003-02-20 | 2004-09-02 | Bayer Ag | Process for the preparation of storage-stable benzothiazolylsulfenamides |
| WO2016042980A1 (en) * | 2014-09-16 | 2016-03-24 | 株式会社サクラクレパス | Ink composition for plasma treatment detection, and plasma treatment detection indicator |
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2016
- 2016-12-28 CN CN201611233091.9A patent/CN106829219B/en active Active
Also Published As
| Publication number | Publication date |
|---|---|
| CN106829219A (en) | 2017-06-13 |
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Effective date of registration: 20191202 Address after: 264200 Qingdao middle road-132f-09009, Weihai Economic and Technological Development Zone, Shandong Province Patentee after: Weihai Houpu Biotechnology Co.,Ltd. Address before: 233700 Guzhen Economic Development Zone, Bengbu, Anhui Patentee before: ANHUI HONGSHENG BIOLOGICAL CO.,LTD. |
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Effective date of registration: 20220228 Address after: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee after: Chenghong Pharmaceutical (Weihai) Co.,Ltd. Address before: 264200-132f-09009, Qingdao Middle Road, Weihai Economic and Technological Development Zone, Shandong Province Patentee before: Weihai Houpu Biotechnology Co.,Ltd. |
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Effective date of registration: 20230724 Address after: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee after: Chenghong Pharmaceutical (Weihai) Co.,Ltd. Patentee after: Weihai Houpu Biotechnology Co.,Ltd. Address before: 264400 Zhuhai Road North Jiaochang Road East, economic development zone, Wendeng District, Weihai City, Shandong Province Patentee before: Chenghong Pharmaceutical (Weihai) Co.,Ltd. |
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