CN106822241A - A kind of smoked bar of clearing damp Chinese mugwort and preparation method thereof - Google Patents

A kind of smoked bar of clearing damp Chinese mugwort and preparation method thereof Download PDF

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Publication number
CN106822241A
CN106822241A CN201611243387.9A CN201611243387A CN106822241A CN 106822241 A CN106822241 A CN 106822241A CN 201611243387 A CN201611243387 A CN 201611243387A CN 106822241 A CN106822241 A CN 106822241A
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moxa
chinese mugwort
residue
extract solution
bar
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赵路通
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Henan Zhong Yi Ai Porcelain Culture Development Co Ltd
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Henan Zhong Yi Ai Porcelain Culture Development Co Ltd
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    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/282Artemisia, e.g. wormwood or sagebrush
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/28Asteraceae or Compositae (Aster or Sunflower family), e.g. chamomile, feverfew, yarrow or echinacea
    • A61K36/284Atractylodes
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K36/00Medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicines
    • A61K36/18Magnoliophyta (angiosperms)
    • A61K36/185Magnoliopsida (dicotyledons)
    • A61K36/54Lauraceae (Laurel family), e.g. cinnamon or sassafras
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K9/00Medicinal preparations characterised by special physical form
    • A61K9/0002Galenical forms characterised by the drug release technique; Application systems commanded by energy
    • A61K9/0004Osmotic delivery systems; Sustained release driven by osmosis, thermal energy or gas
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/10Preparation or pretreatment of starting material
    • A61K2236/15Preparation or pretreatment of starting material involving mechanical treatment, e.g. chopping up, cutting or grinding
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/331Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using water, e.g. cold water, infusion, tea, steam distillation, decoction
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/33Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones
    • A61K2236/333Extraction of the material involving extraction with hydrophilic solvents, e.g. lower alcohols, esters or ketones using mixed solvents, e.g. 70% EtOH
    • AHUMAN NECESSITIES
    • A61MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61KPREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K2236/00Isolation or extraction methods of medicinal preparations of undetermined constitution containing material from algae, lichens, fungi or plants, or derivatives thereof, e.g. traditional herbal medicine
    • A61K2236/30Extraction of the material
    • A61K2236/39Complex extraction schemes, e.g. fractionation or repeated extraction steps

Abstract

The present invention relates to smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort is made up of 100 150 portions of folium artemisiae argyis, 15 25 portions of eupatoriums, 25 40 parts of rhizoma atractylodis and 10 30 portions of Chinese cassia trees;Smoked bar of a kind of clearing damp Chinese mugwort of the present invention and preparation method thereof, the smoked bar of clearing damp Chinese mugwort can effective damp-clearing pain-relieving, expelling wind and clearing away cold, moxa-moxibustion is convenient, and the medication for alleviating patient is painful, easy to use, saves expense, it is adaptable to the patient of all age group.

Description

A kind of smoked bar of clearing damp Chinese mugwort and preparation method thereof
Technical field
The invention belongs to Chinese medicine preparation field, specially a kind of smoked bar of clearing damp Chinese mugwort and preparation method thereof.
Background technology
Moxa-moxibustion originates from ancient Chinese as one of main treatment means of the traditional Chinese medical science, is the moxa-moxibustion material being made of folium artemisiae argyi The Ai heat of generation stimulates body surface point or specific position, by exciting the vein active physiology to adjust human disorder of ventilation Biochemical function, play promoting qi circulation and removing obstruction in the collateral, supporting YANG to cure collaps-syndrome as emergency treatment, it is promoting blood circulation and removing blood stasis, draw out pus by applying a plaster to the affected part expel the heat-evil, macrobiosis beauty the effects such as, so as to reach diseases prevention The purpose cured the disease.
But conventional moxa-moxibustion is in the preparation, is just processed using Chen Aiye more, because containing substantial amounts of folium artemisiae argyi in raw tarragon Oil, vigor is swift and violent during burning, and heating power is not persistently thorough enough, and it produces substantial amounts of volatile materials and Chinese mugwort tar in burning, These materials are sucked for a long time and easily suffers from tuberculosis, pollute Curing circumstance, be unfavorable for health, thus it is many using Chen Ai treatment, Blumea oil in the middle of Chen Ai is effectively volatilized so that the smoked bar of Chinese mugwort made can persistently burn and vigor is gentle, but Chen Ai Standing time is long, leverages the fabrication cycle of the smoked bar of Chinese mugwort, a large amount of productions of the smoked bar that is unfavorable for ending.When by folium artemisiae argyi during moxa-moxibustion Effect is treated, and curative effect is general, in addition it is also necessary to which the other medicines of auxiliary could play a role well, increase the pain of patient Hardship, increases expense, therefore needs badly and a kind of can merge other drugs curative effect and the smoked bar of Chinese mugwort with short production cycle.
The content of the invention
In order to solve that the Chinese mugwort smoked bar production cycle at present is long, curative effect is general, therapeutic process it is more painful and costly etc. Problem, the purpose of the present invention is to propose to smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of clearing damp Chinese mugwort being capable of effectively clearing damp Analgesic, expelling wind and clearing away cold, moxa-moxibustion is convenient, alleviates the medication pain of patient, easy to use, saves expense, it is adaptable to each year The patient of age section.
The technical scheme is that:A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 100-150 portions of folium artemisiae argyi, 15-25 portions of eupatorium, 25-40 parts of rhizoma atractylodis and 10-30 parts of Chinese cassia tree composition;
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, evaporation, Spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then will worn Blue and rhizoma atractylodis carry out ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, are afterwards sprayed to the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after evaporation process;
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued to crush Until level of residue is less than 5%, then smash into moxa to pieces;
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and is crushed Mixture is obtained to 40-50 mesh, is then the ethanol of 75-95% to the mass fraction of 20-30 times of mixture weight of addition in mixture Mix immersion 1-2h, 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, backward residue I in Add the mass fraction of 20-30 times of residue I weight carries out ultrasonic extraction for the ethanol of 75-95% at 35-40 DEG C, obtains extract solution II and residue II, then be the ethanol of 75-95% at 35-40 DEG C to the mass fraction of 20-30 times of II weight of residue is added in residue II Under carry out ultrasonic extraction, obtain extract solution III, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and be concentrated into The 20% of the volume of mixed liquor obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25- 30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight 5-10 after Chinese cassia tree is cleaned into dries pulverizing Water immersion 2-3h again, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is finished, And be cooled to room temperature drying can be prepared by Chinese cassia tree moxa;
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, is freezed afterwards dry It is dry, and compressing can be prepared by the clearing damp smoked bar of Chinese mugwort.
Beneficial effects of the present invention:
1st, smoked bar of clearing damp Chinese mugwort of the present invention and preparation method thereof, for arthralgia pain due to rheumatism, waist Teng's crymodynia etc. symptoms include effect are rapid, its Middle folium artemisiae argyi has warming channel for arresting bleeding, the effect of eliminating cold to stop pain, and eupatorium has removes dampness by means of aromatics, and appetizing of being amusing delivers the effect of relieving summer-heat, grey Art has eliminating dampness Jian spleens, and expelling wind and clearing away cold, the effect of improving eyesight, Chinese cassia tree has mends fire supporing yang, and guiding fire to origin, eliminating cold to stop pain, temperature is stimulated the menstrual flow The effect of arteries and veins, this several drugs are shared with folium artemisiae argyi, can reach warming channel for arresting bleeding during moxa-moxibustion, the effect of eliminating cold to stop pain, be used in conjunction two to Arthralgia pain due to rheumatism can be alleviated within three days, the situation of waist Teng's crymodynia can be relieved according to after state of an illness moxa-moxibustion two weeks, and pain subtracts Gently, moisture is dispelled by consolidating after moxa-moxibustion March, pain is little, effect is significant, it is adaptable to the patient of all age group, conveniently makes With alleviating the pain of patient's oral drugs;
2nd, it is of the invention by being evaporated extraction to Chinese cassia tree, and because the main component cinnamic acid in Chinese cassia tree is volatile, by Chinese cassia tree Evaporation when steam be passed into treated moxa so that cinnamic acid is attached on moxa, simultaneously because the effect of steam, also A part of Blumea oil can be taken away, the amount of Blumea oil is reduced, the burning endurance of the smoked bar of Chinese mugwort is improved, vigor is gentle, end tar Pollution is few, greatly reduces the production cycle of the smoked bar of Chinese mugwort, is easy to mass production to promote.
3rd, the present invention is by by the extract solution spray of eupatorium and rhizoma atractylodis to moxa, then using the side of freeze-drying Formula, effectively saves the active ingredient of eupatorium, rhizoma atractylodis and Chinese cassia tree, and this several drugs and moxa are shared, then is aided with suitably Moxibustion on Acupoints, clearing damp effect is good.
Specific embodiment
With reference to specific examples below, the present invention is described in further detail, and protection scope of the present invention is not limited to In following examples.Implement process of the invention, condition, reagent, experimental technique etc., in addition to the following special content for referring to, The universal knowledege and common knowledge of this area are, the present invention is not particularly limited content.
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort is by 100-150 parts of folium artemisiae argyi, 15-25 Part eupatorium, 25-40 parts of rhizoma atractylodis and 10-30 parts of Chinese cassia tree composition.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Described folium artemisiae argyi, acrid, bitter, warm is slightly poisonous.Return liver, spleen, kidney channel.Indication warming channel for arresting bleeding, eliminating cold to stop pain;Outward Use removing dampness to stop itchin.For spitting blood, bleeding from five sense organs or subcutaneous tissue, uterine bleeding, menorrhalgia, blood under threatened abortion, few abdomen crymodynia, through uncomfortable, uterus cold infertile of trembling with fear.
Described eupatorium, it is pungent, put down.Returns spleen, stomach, lung channel.Indication is removed dampness by means of aromatics, appetizing of being amusing, delivers relieving summer-heat.For Turbi damp obstructing in middle-JIAO, gastral cavity ruffian evil of vomitting, sweet in mouth, halitosis, polysialia, summer-heat and damp table card, damp-warm syndrome is from the beginning of burnout of generating heat is uncomfortable in chest not relax.
Described rhizoma atractylodis, pungent, hardship, temperature.Returns spleen, stomach, Liver Channel.Indication eliminating dampness Jian spleens, expelling wind and clearing away cold, improving eyesight.For Damp retention in middle-jiao, abdominal fullness and distention, diarrhea, oedema, tinea pedis Wei jiu, arthralgia pain due to rheumatism, anemofrigid cold, yctalopia, eyes dusk is puckery.
Described Chinese cassia tree, mends fire supporing yang, guiding fire to origin, eliminating cold to stop pain, warming meridian, for positive fistula Gong Leng, waist Teng's crymodynia, Kidney Virtual is breathed heavily, deficient yang with upper manifestation, dizziness hot eyes , Xin Peep crymodynias, cold of insufficiency type vomiting and diarrhea, and pain of trembling with fear is suffered from abdominal pain, dysmenorrhoea Amenorrhea.
Embodiment 1
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 100 portions of folium artemisiae argyis, 15 portions of eupatoriums, 25 parts Rhizoma atractylodis and 10 parts of Chinese cassia tree compositions.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Embodiment 2
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 110 portions of folium artemisiae argyis, 18 portions of eupatoriums, 30 parts Rhizoma atractylodis and 15 parts of Chinese cassia tree compositions.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Embodiment 3
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 125 portions of folium artemisiae argyis, 20 portions of eupatoriums, 35 parts Rhizoma atractylodis and 20 parts of Chinese cassia tree compositions.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Embodiment 4
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 140 portions of folium artemisiae argyis, 23 portions of eupatoriums, 38 parts Rhizoma atractylodis and 25 parts of Chinese cassia tree compositions.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Embodiment 5
A kind of smoked bar of clearing damp Chinese mugwort, according to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort by 150 portions of folium artemisiae argyis, 25 portions of eupatoriums, 40 parts Rhizoma atractylodis and 30 parts of Chinese cassia tree compositions.
Smoked bar of a kind of clearing damp Chinese mugwort and preparation method thereof, the smoked bar of described Chinese mugwort is by getting the raw materials ready, pretreatment of raw material, extraction process, Evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:Folium artemisiae argyi is carried out into pretreatment first and is made moxa, then Eupatorium and rhizoma atractylodis are carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, afterwards spray the extract solution of ultrasonic extraction It is compressing after freeze-drying to prepare the smoked bar of clearing damp Chinese mugwort on moxa after mist to evaporation process.
The pretreatment of described raw material, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued Crush until level of residue is less than 5%, then smashs into moxa to pieces.
The concrete operations of described eupatorium and the ultrasonic extraction of rhizoma atractylodis are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and It is crushed to 40-50 mesh and obtains mixture, is then 75-95%'s to the mass fraction of 20-30 times of mixture weight of addition in mixture Ethanol mixes immersion 1-2h, and 35-40 DEG C is adjusted the temperature to afterwards carries out ultrasonic extraction, obtains extract solution I and residue I, it is backward residual Add the mass fraction of 20-30 times of residue I weight for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C in slag I, must carry Take liquid II and residue II, then be the ethanol of 75-95% in 35- to the mass fraction of 20-30 times of II weight of residue is added in residue II Ultrasonic extraction is carried out at 40 DEG C, extract solution III is obtained, merge afterwards extract solution I, extract solution II and extract solution III mixed liquor and dense Be reduced to the volume of mixed liquor 20% obtains extract solution IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, it is ultrasonic every time to be spaced 1-5min;Described evaporation process refers to add its weight after Chinese cassia tree is cleaned into dries pulverizing 5-10 times of water immersion 2-3h, is then evaporated treatment in a kettle., and steam is passed through in moxa, until water evaporation is complete Finish, and be cooled to room temperature drying and can be prepared by Chinese cassia tree moxa.
Described spraying treatment refers to be atomized extract solution IV, is then uniformly sprayed onto on Chinese cassia tree moxa, Zhi Houleng It is lyophilized dry, and compressing can be prepared by the smoked bar of clearing damp Chinese mugwort.
Clinical case:
Liu so-and-so, female, 36 years old, arthralgia pain due to rheumatism, morning stiffness was serious, 2-3 days of the present invention of moxa-moxibustion, once a day, each 25-30min, disease Shape is relieved, and morning stiffness mitigates, the stable disease acupuncture March that holds on again after.
King so-and-so, man, 65 years old, arthritis, morning stiffness was serious, arthralgia, 3-4 days of the present invention of moxa-moxibustion, once a day, every time 25-30min, symptom is relieved, and continues stable disease after moxa-moxibustion half a year, and pain is slight.
Week so-and-so, female 15 years old, suffers from cold, and moisture invades heresy, arthralgia, 2-3 days of the present invention of moxa-moxibustion, once a day, each 25- 30min, pain is relieved, and is fully recovered after continuing moxa-moxibustion March, does not recur so far.
Zhang, female, 40 years old, rheumatoid arthritis, arthralgia, 1-3 days of the present invention of moxa-moxibustion, once a day, every time 25-30min, symptom is relieved, and continues stable disease after moxa-moxibustion 1 year, and arthralgia is slight.
Gong so-and-so, man, 35 years old, arthritis, arthralgia, one meets cloudy pain more very, 3-5 days of the present invention of moxa-moxibustion, daily 1 Secondary, each 25-30min, symptom is relieved, and pain is slight after continuing moxa-moxibustion half a year, stable disease.

Claims (5)

1. a kind of clearing damp Chinese mugwort smokes bar, it is characterised in that:According to weight ratio, the preparing raw material of the smoked bar of described Chinese mugwort is by 100-150 parts Folium artemisiae argyi, 15-25 portion of eupatorium, 25-40 parts of rhizoma atractylodis and 10-30 parts of Chinese cassia tree composition.
2. a kind of clearing damp Chinese mugwort as claimed in claim 1 smokes the preparation method of bar, it is characterised in that:The smoked bar of described Chinese mugwort is by standby Material, pretreatment of raw material, extraction process, evaporation, spraying, freeze-drying and shaping are prepared from, and concrete operations are:First by folium artemisiae argyi Carry out pretreatment and be made moxa, eupatorium and rhizoma atractylodis are then carried out into ultrasonic extraction, then treatment is evaporated to moxa with Chinese cassia tree, it The extract solution of ultrasonic extraction is sprayed on the moxa after evaporation process afterwards, it is compressing after freeze-drying to prepare the clearing damp The smoked bar of Chinese mugwort.
3. a kind of clearing damp Chinese mugwort as claimed in claim 2 smokes the preparation method of bar, it is characterised in that:The pre- place of described raw material Reason, cleans dries pulverizing by folium artemisiae argyi first, then crosses 40-60 mesh sieves, and residue is continued to crush until level of residue is less than 5%, then smashes It is broken into moxa.
4. a kind of clearing damp Chinese mugwort as claimed in claim 2 smokes the preparation method of bar, it is characterised in that:Described eupatorium and rhizoma atractylodis The concrete operations of ultrasonic extraction are:Eupatorium and rhizoma atractylodis are first cleaned into drying first, and is crushed to 40-50 mesh and obtain mixture, then To adding the mass fraction of 20-30 times of mixture weight for the ethanol of 75-95% soaks 1-2h in mixture, temperature is adjusted afterwards Carry out ultrasonic extraction to 35-40 DEG C, obtain extract solution I and residue I, backward residue I in add the matter of 20-30 times of residue I weight Amount fraction carries out ultrasonic extraction for the ethanol of 75-95% at 35-40 DEG C, obtains extract solution II and residue II, then add in residue II Enter the mass fraction of 20-30 times of II weight of residue for the ethanol of 75-95% carries out ultrasonic extraction at 35-40 DEG C, obtain extract solution III, merging extract solution I, extract solution II and extract solution III obtain mixed liquor and are concentrated into the 20% of the volume of mixed liquor and carried afterwards Take liquid IV;The frequency of described ultrasonic extraction is 20-80KHz, and ultrasonic time is 25-30min, every time ultrasound interval 1-5min; Described evaporation process refers to add the water of 5-10 times of its weight to soak 2-3h after Chinese cassia tree is cleaned into dries pulverizing, is then steamed Hair treatment, and steam is passed through in moxa, until water evaporation is finished, and is cooled to room temperature drying and be can be prepared by Chinese cassia tree moxa.
5. a kind of clearing damp Chinese mugwort smokes the preparation method of bar as described in claim 4, it is characterised in that:Described spraying treatment is Be atomized for extract solution IV by finger, is then uniformly sprayed onto on Chinese cassia tree moxa, afterwards freeze-drying, and compressing be can be prepared by The smoked bar of clearing damp Chinese mugwort.
CN201611243387.9A 2016-12-29 2016-12-29 A kind of smoked bar of clearing damp Chinese mugwort and preparation method thereof Pending CN106822241A (en)

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CN1327801A (en) * 2000-06-14 2001-12-26 石学敏 Moxibustion stick for dispelling dampness, relieving pain and mourishing Qi and blood
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Publication number Priority date Publication date Assignee Title
CN1327801A (en) * 2000-06-14 2001-12-26 石学敏 Moxibustion stick for dispelling dampness, relieving pain and mourishing Qi and blood
CN102342969A (en) * 2011-11-24 2012-02-08 成都盛尔嘉科技有限公司 Production method for micro-smoke moxibustion

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