CN106811870A - A kind of super soft S/S solids double-component viscose non-woven material and preparation method thereof - Google Patents

A kind of super soft S/S solids double-component viscose non-woven material and preparation method thereof Download PDF

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Publication number
CN106811870A
CN106811870A CN201710088677.9A CN201710088677A CN106811870A CN 106811870 A CN106811870 A CN 106811870A CN 201710088677 A CN201710088677 A CN 201710088677A CN 106811870 A CN106811870 A CN 106811870A
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Prior art keywords
polypropylene
preparation
melt
masterbatch
softening agent
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CN201710088677.9A
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Chinese (zh)
Inventor
邓连华
张金秋
曹仁广
韩旭
肖其柏
张植民
付少辉
鲁海峰
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Hengtian Nonwoven Co Ltd Ka Wah
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Hengtian Nonwoven Co Ltd Ka Wah
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Priority to CN201710088677.9A priority Critical patent/CN106811870A/en
Publication of CN106811870A publication Critical patent/CN106811870A/en
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    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/005Synthetic yarns or filaments
    • D04H3/007Addition polymers
    • DTEXTILES; PAPER
    • D01NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
    • D01DMECHANICAL METHODS OR APPARATUS IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS
    • D01D5/00Formation of filaments, threads, or the like
    • D01D5/28Formation of filaments, threads, or the like while mixing different spinning solutions or melts during the spinning operation; Spinnerette packs therefor
    • D01D5/30Conjugate filaments; Spinnerette packs therefor
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/018Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the shape
    • DTEXTILES; PAPER
    • D04BRAIDING; LACE-MAKING; KNITTING; TRIMMINGS; NON-WOVEN FABRICS
    • D04HMAKING TEXTILE FABRICS, e.g. FROM FIBRES OR FILAMENTARY MATERIAL; FABRICS MADE BY SUCH PROCESSES OR APPARATUS, e.g. FELTS, NON-WOVEN FABRICS; COTTON-WOOL; WADDING ; NON-WOVEN FABRICS FROM STAPLE FIBRES, FILAMENTS OR YARNS, BONDED WITH AT LEAST ONE WEB-LIKE MATERIAL DURING THEIR CONSOLIDATION
    • D04H3/00Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length
    • D04H3/08Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating
    • D04H3/14Non-woven fabrics formed wholly or mainly of yarns or like filamentary material of substantial length characterised by the method of strengthening or consolidating with bonds between thermoplastic yarns or filaments produced by welding
    • D04H3/147Composite yarns or filaments
    • DTEXTILES; PAPER
    • D10INDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10BINDEXING SCHEME ASSOCIATED WITH SUBLASSES OF SECTION D, RELATING TO TEXTILES
    • D10B2321/00Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds
    • D10B2321/02Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polyolefins
    • D10B2321/022Fibres made from polymers obtained by reactions only involving carbon-to-carbon unsaturated bonds polyolefins polypropylene

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  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Nonwoven Fabrics (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)

Abstract

The invention provides the super soft S/S solids double-component viscose non-woven material of one kind, by polypropylene a and polypropylene b, and softening agent and Masterbatch are made, the features such as obtained non-woven fabrics of the invention has good hydrophilic property, pliability high, laminating skin, quality is closely knit, grammes per square metre is small, the 80g/m of surface density 30 of the material280 240N/5cm of longitudinal strength, longitudinal elongation at break rate 90 120%, the 800cNcm of longitudinal bending stiffness 200, the 4cm of buckling length 2,50 180N/5cm of horizontal strength, transverse breakage elongation 60 100%, the 480cNcm of transverse curvature rigidity 160, the 7cm of transverse curvature length 3, the three-dimensional thickness of material is 0.5 2mm.

Description

A kind of super soft S/S solids double-component viscose non-woven material and preparation method thereof
Technical field
The invention belongs to non-woven fabrics field, more particularly to a kind of super soft S/S solid double-component viscose non-woven materials and Its preparation method.
Background technology
Non-woven fabrics (non-weaving cloth) is a kind of fabric that need not be spinned cotton and woven cloth and be formed, simply by textile staple or Long filament is oriented or support is arranged at random, forms fibre net structure, is then reinforced using the method such as mechanical, hot sticky or chemical and formed.Letter Single saying be exactly:It is not by one one yarns interwoven, woollen yarn knitting together, but by fiber directly by the side of physics What method was bonded together, so, when the viscous title in you take your clothes, it finds that, it is that can not take out the end of a thread one by one. Non-weaving cloth breaches traditional weaving principle, and with technological process is short, speed of production is fast, yield is high, low cost, purposes Extensively, the features such as raw material sources are more, have a wide range of applications in daily production and life.
Spun-bond process increasingly occupies an important position as nonwoven production technology with the fastest developing speed at present.It is Using synthetic fiber spinning principle, continuous filament fibers are made to lay into net during polymer spinning, fibre web is through machinery, chemistry or warm Method is reinforced and forms non-weaving cloth.Spunbond production technology is applied to terylene, nonwoven polypropylene fabric history for many years.
The technological process of polypropylene spun-bonded non-woven fabrics is as follows:Polypropylene chip-melt spinning-air drawing-pendulum wire - winding is reinforced into net-hot rolling.
But current non-weaving cloth cannot also meet some specific demands in pliability, particularly with medical and health use Cloth, such as sanitary napkin, can make human body sensory uncomfortable.But this fiber or long filament can produce quiet because of friction in process Electricity, obstacle and trouble are brought to subsequent handling, are unfavorable in the carrying out of production, while in use, as electrostatic, Inconvenience is brought to user.Generally requiring carries out soft treatment, and its soft treatment is typically added or rear whole by master batch The method of reason is carried out, and causes that the pliability of non-woven fabrics is improved by reducing interfibrous coefficient of friction.But obtained in the method Material feel is not especially smooth, and not water-fastness, and the time that softness is maintained when using is not high.Chinese patent CN201110412625.5 also discloses that a kind of super soft non-weaving cloth and its manufacture method, and the method is using changing material Formal structure makes material become soft, and this preparation method can also influence the strength of material, reduce its service life.
The pliability of spun-bonded non-woven fabrics how is improved, how the pliability of spun-bonded non-woven fabrics softness as silk is brought up into Degree, as the technical barrier that non-woven fabrics industry is commonly encountered.In addition, though formula use in the industry at present plus soft can be in certain journey The pliability of product is improved on degree, but pliability is limited, additionally, to take into account the intensity of product, pliability, smooth degree and criticize Amount steady production is even more in the industry cannot be while the problem for solving.
The content of the invention
The technical problems to be solved by the invention be to provide a kind of super soft S/S solid double-component viscose non-woven materials and its Preparation method, prepared material has splendid comfort level and pliability, and its third dimension is stronger, and deformation behavior is small, breathes freely Property is more preferable.
To solve the above problems, the technical solution adopted by the present invention is:
A kind of super soft S/S solids double-component viscose non-woven material, by polypropylene a and polypropylene b, and softening agent and color Master batch is made;Wherein, the melt index of the polypropylene a is 20-50g/10min, and the melt index of polypropylene b is 10-30g/ 10min, and polypropylene a melt index higher than polypropylene b melt index;The polypropylene a, polypropylene b, softening agent and color The weight ratio of master batch is:70-90:10-30:2-6:1-2;The surface density 30-80g/m of the material2, longitudinal strength 80-240N/ 5cm, longitudinal elongation at break rate 90-120%, longitudinal bending stiffness 200-800cNcm, buckling length 2-4cm are laterally strong Power 50-180N/5cm, transverse breakage elongation 60-100%, transverse curvature rigidity 160-480cNcm, transverse curvature length 3- 7cm, the three-dimensional thickness of material is 0.5-2mm.
Wherein, the preparation method of the non-woven fabric composite material, comprises the following steps:
(1) Masterbatch for taking polypropylene a, the softening agent of half amount and half amount respectively in proportion is stirred by whisking machines Form mixed material A;The Masterbatch of polypropylene b, the softening agent of second half amount and second half amount is taken respectively in proportion by stirring Machine stirs to form mixed material B;
(2) mixed material component A is fed into a screw extruder, is melted at 240-290 DEG C;By mixed material B component is fed into an other screw extruder, is melted at 220-270 DEG C;By two melts of screw extruder extrusion Fondant filter filtering is transported to respectively through melt pipe, measuring pump is sent into afterwards, entered into through the accurate measurement of measuring pump Subsequently into spinning die head, spinneret is carried out by the die head of block form, side-by-side bicomponent fiber is sprayed, when by cooling box Be cooled after the cooling of wind carries out air drawing and forms helical fiber by pipe type air flow drawing device, and then fiber passes through Distributor is evenly distributed on spinneret, fluffy fleece is formed, by being transported to hot rolling after the preliminary reinforcing of pressure network roller Technique is shaped by hot-rolling mill hot rolling, is then cooled down by chill roll, and heat is carried out by blancher, and finally winding cutting is coiled i.e. Can.
The temperature of the hot rolling is 130-180 DEG C, and pressure is 0.4-0.6Mpa.
Melt pressure is 5MPa, and the melt-stoichiometry revolution speed on melt extruder is 15 revs/min -25 revs/min.
The pressure of the air drawing is 0.4-0.9Mpa, and air drawing speed is 5000m/min, and winding speed is 8.0- 15.0m/min。
The aperture of the spinneret is 200-300 μm.
The spinning speed is controlled to 300 ms/min to 600 ms/min,
Technique effect of the invention is:(1) viscose non-woven material prepared by the present invention can solve current non-woven fabrics The problem of hard sense and harsh feeling, pliability and comfort level are high;(2) present invention essentially consists in the different melt index of two kinds of use Polypropylene material forms bicomponent fibers according to certain proportioning by double-component spinneret, due to gathering for different melt index The shrinkage factor of propylene is different, and fiber can form the fiber of helical structure, while being reinforced using the hot roll that particular design is rolled a little Fibre web, makes to be obtained non-woven material with three-dimensional structure and super soft style;(3) present invention is by adding softening agent and color masterbatch Grain, obtained non-woven fabrics has good hydrophilic property, pliability high, laminating skin, the features such as quality is closely knit, grammes per square metre is small;(4) present invention The performance of prepared non-woven fabrics is very excellent, its surface density 30-80g/m2, longitudinal strength 80-240N/5cm, longitudinal fracture stretches Rate 90-120% long, longitudinal bending stiffness 200-800cNcm, buckling length 2-4cm, horizontal strength 50-180N/5cm, Transverse breakage elongation 60-100%, transverse curvature rigidity 160-480cNcm, transverse curvature length 3-7cm, the solid of material Thickness is 0.5-2mm, is superior to prior art correlation non-woven fabrics.
Specific embodiment
Technical scheme is further elaborated with reference to embodiment:
Embodiment 1
A kind of preparation method of non-woven fabric composite material, it is characterised in that comprise the following steps:
(1) melt index is taken respectively by weight proportion for 70 parts of 50g/10min polypropylene a, 2 parts of the softening agent of half amount 1 part of the Masterbatch with half amount stirs to form mixed material A by whisking machines;Taking melt index respectively by weight proportion is 1 part of the Masterbatch of 15 parts of 30g/10min polypropylene b, 2 parts of the softening agent of second half amount and second half amount is stirred by whisking machines Mix to form mixed material B;
(2) mixed material component A is fed into a screw extruder, is melted at 260 DEG C;By mixed material B groups Divide and be fed into an other screw extruder, melted at 230 DEG C;By the melts of two screw extruders extrusion respectively through Melt pipe is transported to fondant filter filtering, and the melt pressure is 5MPa, measuring pump is sent into afterwards, through the accurate of measuring pump Metering is entered into subsequently into spinning die head, and spinneret is carried out by the die head of block form, sprays side-by-side bicomponent fiber, the spray Silk speed control is 400 ms/min, is cooled after the cooling of wind to be entered by pipe type air flow drawing device when by cooling box Row air drawing forms helical fiber, and the pressure of the air drawing is 0.5Mpa, and air drawing speed is 5000m/min, Then fiber is evenly distributed on spinneret by distributor, fluffy fleece is formed, in the preliminary reinforcing by pressure network roller After be transported to hot rolling technology and shaped by hot-rolling mill hot rolling, the temperature of the hot rolling is 140 DEG C, and pressure is 0.4Mpa, Ran Houjing Supercooling roller is cooled down, and heat is carried out by blancher, and finally winding cutting is coiled, and the winding speed is 10.0m/min;
Wherein, the surface density 50g/m of prepared material2, longitudinal strength 160N/5cm, longitudinal elongation at break rate 110%, indulge To bending stiffness 600cNcm, buckling length 2cm, horizontal strength 120N/5cm, transverse breakage elongation 90% is horizontal Bending stiffness 320cNcm, transverse curvature length 4cm, the three-dimensional thickness of material is 1mm.
Embodiment 2
A kind of preparation method of non-woven fabric composite material, comprises the following steps:
(1) it is 80 parts of 40g/10min polypropylene a, 2 parts of the softening agent of half amount and to take melt index respectively in proportion 1 part of the Masterbatch of half amount stirs to form mixed material A by whisking machines;Melt index is taken respectively in proportion for 20g/10min 1 part of the Masterbatch of 20 parts of polypropylene b, 2 parts of the softening agent of second half amount and second half amount stirs to form mixing by whisking machines Raw material B;
(2) mixed material component A is fed into a screw extruder, is melted at 270 DEG C;By mixed material B groups Divide and be fed into an other screw extruder, melted at 240 DEG C;By the melts of two screw extruders extrusion respectively through Melt pipe is transported to fondant filter filtering, and the melt pressure is 5MPa, measuring pump is sent into afterwards, through the accurate of measuring pump Metering is entered into subsequently into spinning die head, and spinneret is carried out by the die head of block form, sprays side-by-side bicomponent fiber, the spray Silk speed control is 500 ms/min, is cooled after the cooling of wind to be entered by pipe type air flow drawing device when by cooling box Row air drawing forms helical fiber, and the pressure of the air drawing is 0.7Mpa, and air drawing speed is 5000m/min, Then fiber is evenly distributed on spinneret by distributor, fluffy fleece is formed, in the preliminary reinforcing by pressure network roller After be transported to hot rolling technology and shaped by hot-rolling mill hot rolling, the temperature of the hot rolling is 150 DEG C, and pressure is 0.45Mpa, Ran Houjing Supercooling roller is cooled down, and heat is carried out by blancher, and finally winding cutting is coiled, and the winding speed is 11.0m/min,;
The surface density 65g/m of prepared material2, longitudinal strength 200N/5cm, longitudinal elongation at break rate 120%, longitudinal direction it is curved Stiffness 650cNcm, buckling length 4cm, horizontal strength 160N/5cm, transverse breakage elongation 100%, transverse curvature Rigidity 360cNcm, transverse curvature length 6cm, the three-dimensional thickness of material is 1.5mm.
Embodiment 3
A kind of preparation method of non-woven fabric composite material, comprises the following steps:
(1) it is 90 parts of 30g/10min polypropylene a, 2 parts of the softening agent of half amount and to take melt index respectively in proportion 1 part of the Masterbatch of half amount stirs to form mixed material A by whisking machines;Melt index is taken respectively in proportion for 10g/10min 1 part of the Masterbatch of 30 parts of polypropylene b, 2 parts of the softening agent of second half amount and second half amount stirs to form mixing by whisking machines Raw material B;
(2) mixed material component A is fed into a screw extruder, is melted at 290 DEG C;By mixed material B groups Divide and be fed into an other screw extruder, melted at 260 DEG C;By the melts of two screw extruders extrusion respectively through Melt pipe is transported to fondant filter filtering, and the melt pressure is 5MPa, measuring pump is sent into afterwards, through the accurate of measuring pump Metering is entered into subsequently into spinning die head, and spinneret is carried out by the die head of block form, sprays side-by-side bicomponent fiber, the spray Silk speed control is 600 ms/min, is cooled after the cooling of wind to be entered by pipe type air flow drawing device when by cooling box Row air drawing forms helical fiber, and the pressure of the air drawing is 0.8Mpa, and air drawing speed is 5000m/min, Then fiber is evenly distributed on spinneret by distributor, fluffy fleece is formed, in the preliminary reinforcing by pressure network roller After be transported to hot rolling technology and shaped by hot-rolling mill hot rolling, the temperature of the hot rolling is 140 DEG C, and pressure is 0.4Mpa, Ran Houjing Supercooling roller is cooled down, and heat is carried out by blancher, and finally winding cutting is coiled, and the winding speed is 12.0m/min;
The surface density 80g/m of prepared material2, longitudinal strength 220N/5cm, longitudinal elongation at break rate 120%, longitudinal direction it is curved Stiffness 500cNcm, buckling length 3cm, horizontal strength 90N/5cm, transverse breakage elongation 80%, transverse curvature is firm Degree 280cNcm, transverse curvature length 6cm, the three-dimensional thickness of material is 2mm.
Finally it should be noted that:The preferred embodiments of the present invention are the foregoing is only, are not intended to limit the invention, Although being described in detail to the present invention with reference to the foregoing embodiments, for a person skilled in the art, it still may be used Modified with to the technical scheme described in foregoing embodiments, or equivalent is carried out to which part technical characteristic. All any modification, equivalent substitution and improvements within the spirit and principles in the present invention, made etc., should be included in of the invention Within protection domain.

Claims (7)

1. a kind of super soft S/S solids double-component viscose non-woven material, it is characterised in that by polypropylene a and polypropylene b, and Softening agent and Masterbatch are made;Wherein, the melt index of the polypropylene a is 20-50g/10min, the melt index of polypropylene b Be 10-30g/10min, and polypropylene a melt index of the melt index higher than polypropylene b;The polypropylene a, polypropylene b, The weight ratio of softening agent and Masterbatch is:70-90:10-30:2-6:1-2;The surface density 30-80g/m of the material2, longitudinal direction strength 80-240N/5cm, longitudinal elongation at break rate 90-120%, longitudinal bending stiffness 200-800cNcm, buckling length 2- 4cm, horizontal strength 50-180N/5cm, transverse breakage elongation 60-100%, transverse curvature rigidity 160-480cNcm, laterally Bending length 3-7cm, the three-dimensional thickness of material is 0.5-2mm.
2. the preparation method of double-component viscose non-woven material described in a kind of claim 1, it is characterised in that including following step Suddenly:
(1) Masterbatch for taking polypropylene a, the softening agent of half amount and half amount respectively in proportion stirs to be formed by whisking machines Mixed material A;The Masterbatch of polypropylene b, the softening agent of second half amount and second half amount is taken respectively in proportion by whisking machines Stirring forms mixed material B;
(2) mixed material component A is fed into a screw extruder, is melted at 240-290 DEG C;By mixed material B groups Divide and be fed into an other screw extruder, melted at 220-270 DEG C;By two melt difference of screw extruder extrusion Fondant filter is transported to by melt pipe to filter, measuring pump is sent into afterwards, entered into then through the accurate measurement of measuring pump Into spinning die head, spinneret is carried out by the die head of block form, spray side-by-side bicomponent fiber, be subject to when by cooling box Air drawing is carried out by pipe type air flow drawing device after the cooling for cooling down wind and forms helical fiber, then fiber is by distribution Device is evenly distributed on spinneret, fluffy fleece is formed, by being transported to hot rolling technology after the preliminary reinforcing of pressure network roller Shaped by hot-rolling mill hot rolling, then cooled down by chill roll, heat is carried out by blancher, finally winding cutting is coiled.
3. preparation method according to claim 2, it is characterised in that the temperature of the hot rolling is 130-180 DEG C, pressure is 0.4-0.6Mpa。
4. preparation method according to claim 3, it is characterised in that melt pressure is 5MPa, it is molten on melt extruder Body metering revolution speed is 15 revs/min -25 revs/min.
5. the preparation method according to claim any one of 3-4, it is characterised in that the pressure of the air drawing is 0.4- 0.9Mpa, air drawing speed is 5000m/min, and winding speed is 8.0-15.0m/min.
6. the preparation method according to claim any one of 4-5, it is characterised in that the aperture of the spinneret is 200- 300μm。
7. the preparation method according to claim any one of 5-6, it is characterised in that the spinning speed be controlled to 300 meters/ Divide to 600 ms/min.
CN201710088677.9A 2017-02-20 2017-02-20 A kind of super soft S/S solids double-component viscose non-woven material and preparation method thereof Pending CN106811870A (en)

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CN107761254A (en) * 2017-10-27 2018-03-06 山东恒鹏卫生用品有限公司 Elastic non-woven cloth and its preparation method and application
CN108035073A (en) * 2018-01-08 2018-05-15 恒天嘉华非织造有限公司 A kind of production technology of put-down side-by-side bicomponent spun-bonded continuous yarn non-woven material
CN108035077A (en) * 2018-01-08 2018-05-15 恒天嘉华非织造有限公司 A kind of production technology of the molding non-woven material of two-component spun-bonded continuous yarn hot wind
CN108179549A (en) * 2018-03-13 2018-06-19 苏州多瑈新材料科技有限公司 A kind of elastic super soft non-woven material of polypropylene-base long filament and its production method
CN108532130A (en) * 2018-04-24 2018-09-14 浙江金三发非织造布有限公司 A kind of extremely soft non-woven fabrics and its production technology
CN108842307A (en) * 2018-07-12 2018-11-20 山东斯维特新材料科技有限公司 A kind of fluffy elastic non-woven cloth production process
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CN109294059A (en) * 2018-09-13 2019-02-01 上海彩艳实业有限公司 A kind of modified softening agent, modified master batch and modified master batch manufacturing method
CN109750418A (en) * 2019-01-30 2019-05-14 寿光市万虹无纺布有限公司 A kind of sliceable non-woven fabrics of ultra-wide and preparation method thereof
CN110965208A (en) * 2018-09-30 2020-04-07 俊富非织造材料有限公司 Preparation method for manufacturing polypropylene non-woven fabric by spinning and melting method and non-woven fabric product
CN110965206A (en) * 2018-09-30 2020-04-07 俊富非织造材料有限公司 Polypropylene spun-bonded non-woven fabric and preparation process thereof for improving softness of polypropylene spun-bonded non-woven fabric
CN115247288A (en) * 2021-12-22 2022-10-28 青岛大学 Parallel double-component crimped filament and preparation method thereof
CN116219639A (en) * 2023-02-21 2023-06-06 山东道恩斯维特科技有限公司 Preparation method of bi-component spunbonded wiping material with three-dimensional structure

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Application publication date: 20170609