CN106810114A - A kind of quartz and preparation method thereof - Google Patents

A kind of quartz and preparation method thereof Download PDF

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Publication number
CN106810114A
CN106810114A CN201510858468.9A CN201510858468A CN106810114A CN 106810114 A CN106810114 A CN 106810114A CN 201510858468 A CN201510858468 A CN 201510858468A CN 106810114 A CN106810114 A CN 106810114A
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CN
China
Prior art keywords
weight portions
quartz
dispersant
antioxidant
curing agent
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN201510858468.9A
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Chinese (zh)
Inventor
傅仁丰
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Hengyang Athena Quartz Stone Co Ltd
Original Assignee
Hengyang Athena Quartz Stone Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Hengyang Athena Quartz Stone Co Ltd filed Critical Hengyang Athena Quartz Stone Co Ltd
Priority to CN201510858468.9A priority Critical patent/CN106810114A/en
Publication of CN106810114A publication Critical patent/CN106810114A/en
Pending legal-status Critical Current

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Abstract

The present invention provides a kind of quartz and preparation method thereof, including step:1)Stirred after the toner of the quartz sand of 10~90 weight portions, the sea sand powder of 10~40 weight portions, the phenolic resin of 10~30 weight portions, the curing agent of 6~15 weight portions, the dispersant of 3~10 weight portions, the antioxidant of 2~7 weight portions, the adhesive of 2~7 weight portions, 3~10 weight portions is mixed;2)The above-mentioned raw material for mixing is evenly laid out in template;3)Template is compressing under -0.12~-0.06MPa;4)Sheet material after shaping is solidified 1~3 hour at 80~110 DEG C;5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz, can qualification rate batch production quartz high by technical solution of the present invention.

Description

A kind of quartz and preparation method thereof
Technical field
The invention belongs to building material technical field, a kind of quartz and preparation method thereof is specifically referred to.
Background technology
Artificial quartz stone plate is now widely used for furniture, ground, the metope of laying various buildings etc..Artificial quartz in lump lines decorative pattern series of products is typically produced using unsaturated polyester resin and quartz powder filler, but existing production technology is numerous and diverse and unstable, it is difficult to realize the batch production of stabilization, and the product fraction defective for obtaining is high, and production efficiency is low.
In current technology operation, major part is qualitative operation, such as not to wet feed precompressed, to the wet feed after stirring, directly sieving even directly spills toner, and process fails the quantitative control for realizing becoming more meticulous so that products appearance fluctuation is obvious, criticize often, fraction defective is high, it is impossible to realize splicing.
The content of the invention
The technical problem to be solved in the present invention is to provide a kind of quartz for being easy to qualification rate high to produce in batches.
Present disclosure includes:
A kind of quartz, is made from the following raw materials in parts by weight:
Quartz sand 10~90;
Sea sand powder 10~40;
Phenolic resin 10~30;
Curing agent 6~15;
Dispersant 3~10;
Antioxidant 2~7;
Adhesive 2~7
Toner 3~10.
Used as preferred technical scheme, the curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
Used as preferred technical scheme, the dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
Used as preferred technical scheme, the antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
Used as preferred technical scheme, described adhesive is one or more in polyurethane, polystyrene or polyacrylate.
Another technical problem to be solved by this invention is to provide a kind of method for preparing the above-mentioned quartz for being easy to qualification rate batch production high.
Present disclosure includes:
The method for preparing quartz, including step:
1)Stirred after the toner of the quartz sand of 10~90 weight portions, the sea sand powder of 10~40 weight portions, the phenolic resin of 10~30 weight portions, the curing agent of 6~15 weight portions, the dispersant of 3~10 weight portions, the antioxidant of 2~7 weight portions, the adhesive of 2~7 weight portions, 3~10 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.12~-0.06MPa;
4)Sheet material after shaping is solidified 1~3 hour at 80~110 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
Used as preferred technical scheme, the curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
Used as preferred technical scheme, the dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
Used as preferred technical scheme, the antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
Used as preferred technical scheme, described adhesive is one or more in polyurethane, polystyrene or polyacrylate.
Due to using above-mentioned technological means, a kind of quartz and preparation method thereof, including step:1)Stirred after the toner of the quartz sand of 10~90 weight portions, the sea sand powder of 10~40 weight portions, the phenolic resin of 10~30 weight portions, the curing agent of 6~15 weight portions, the dispersant of 3~10 weight portions, the antioxidant of 2~7 weight portions, the adhesive of 2~7 weight portions, 3~10 weight portions is mixed;2)The above-mentioned raw material for mixing is evenly laid out in template;3)Template is compressing under -0.12~-0.06MPa;4)Sheet material after shaping is solidified 1~3 hour at 80~110 DEG C;5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz, can qualification rate batch production quartz high by technical solution of the present invention.
Specific embodiment
In order that technological means, creation characteristic, reached purpose and effect that the present invention is realized are easy to understand, with reference to specific embodiment, the present invention is expanded on further.
A kind of quartz, is made from the following raw materials in parts by weight:
Quartz sand 10~90;
Sea sand powder 10~40;
Phenolic resin 10~30;
Curing agent 6~15;
Dispersant 3~10;
Antioxidant 2~7;
Adhesive 2~7
Toner 3~10.
The curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
The dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
The antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
Described adhesive is one or more in polyurethane, polystyrene or polyacrylate.
The method for preparing quartz, including step:
1)Stirred after the toner of the quartz sand of 10~90 weight portions, the sea sand powder of 10~40 weight portions, the phenolic resin of 10~30 weight portions, the curing agent of 6~15 weight portions, the dispersant of 3~10 weight portions, the antioxidant of 2~7 weight portions, the adhesive of 2~7 weight portions, 3~10 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.12~-0.06MPa;
4)Sheet material after shaping is solidified 1~3 hour at 80~110 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
The curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
The dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
The antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
Embodiment one
1)Stirred after the toner of the quartz sand of 10 weight portions, the sea sand powder of 10 weight portions, the phenolic resin of 10 weight portions, the curing agent of 6 weight portions, the dispersant of 3 weight portions, the antioxidant of 2 weight portions, the adhesive of 2 weight portions, 3 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.12MPa;
4)Sheet material after shaping is solidified 1 hour at 80 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
The curing agent is polyethylene polyamine.
The dispersant is hexenyl bis-stearamides.
The antioxidant is butylated hydroxy anisole.
Product percent of pass is 98.8%.
Embodiment two
1)Stirred after the toner of the quartz sand of 40 weight portions, the sea sand powder of 20 weight portions, the phenolic resin of 20 weight portions, the curing agent of 8 weight portions, the dispersant of 5 weight portions, the antioxidant of 4 weight portions, the adhesive of 4 weight portions, 5 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.10MPa;
4)Sheet material after shaping is solidified 2 hours at 100 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
The curing agent is DACH.
The dispersant is glyceryl monostearate.
The antioxidant is dibutyl hydroxy toluene.
Product percent of pass is 98.6%.
Embodiment three
1)Stirred after the toner of the quartz sand of 70 weight portions, the sea sand powder of 30 weight portions, the phenolic resin of 25 weight portions, the curing agent of 12 weight portions, the dispersant of 8 weight portions, the antioxidant of 6 weight portions, the adhesive of 6 weight portions, 7 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.08MPa;
4)Sheet material after shaping is solidified 2.5 hours at 105 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
The curing agent is diaminodiphenyl-methane.
The dispersant is polyethylene glycol.
The antioxidant is TBHQ.
Product percent of pass is 99.2%.
Example IV
1)Stirred after the toner of the quartz sand of 90 weight portions, the sea sand powder of 40 weight portions, the phenolic resin of 30 weight portions, the curing agent of 15 weight portions, the dispersant of 10 weight portions, the antioxidant of 7 weight portions, the adhesive of 7 weight portions, 10 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.06MPa;
4)Sheet material after shaping is solidified 3 hours at 110 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
The curing agent is the mixture of polyethylene polyamine, DACH and diaminodiphenyl-methane.
The dispersant is the mixture of hexenyl bis-stearamides, glyceryl monostearate and polyethylene glycol.
The antioxidant is the mixture of butylated hydroxy anisole, dibutyl hydroxy toluene and TBHQ.
Product percent of pass is 99.4%.
Using technical solutions according to the invention, or those skilled in the art is under the inspiration of technical solution of the present invention, designs similar technical scheme, and reaches above-mentioned technique effect, is to fall into protection scope of the present invention.

Claims (10)

1. a kind of quartz, it is characterised in that be made from the following raw materials in parts by weight:
Quartz sand 10~90;
Sea sand powder 10~40;
Phenolic resin 10~30;
Curing agent 6~15;
Dispersant 3~10;
Antioxidant 2~7;
Adhesive 2~7
Toner 3~10.
2. quartz as claimed in claim 1, it is characterised in that:The curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
3. quartz as claimed in claim 1, it is characterised in that:The dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
4. quartz as claimed in claim 1, it is characterised in that:The antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
5. quartz as claimed in claim 1, it is characterised in that:Described adhesive is one or more in polyurethane, polystyrene or polyacrylate.
6. a kind of method for preparing the quartz as described in claim 1 to 5 any claim, it is characterised in that including step:
1)Stirred after the toner of the quartz sand of 10~90 weight portions, the sea sand powder of 10~40 weight portions, the phenolic resin of 10~30 weight portions, the curing agent of 6~15 weight portions, the dispersant of 3~10 weight portions, the antioxidant of 2~7 weight portions, the adhesive of 2~7 weight portions, 3~10 weight portions is mixed;
2)The above-mentioned raw material for mixing is evenly laid out in template;
3)Template is compressing under -0.12~-0.06MPa;
4)Sheet material after shaping is solidified 1~3 hour at 80~110 DEG C;
5) sheet material after above-mentioned solidification is carried out into the demoulding, after stacking cooling, you can obtain quartz.
7. the method for preparing quartz as claimed in claim 6, it is characterised in that:The curing agent is one or more in polyethylene polyamine, DACH or diaminodiphenyl-methane.
8. the method for preparing quartz as claimed in claim 6, it is characterised in that:The dispersant is one or more in hexenyl bis-stearamides, glyceryl monostearate or polyethylene glycol.
9. the method for preparing quartz as claimed in claim 6, it is characterised in that:The antioxidant is one or more in butylated hydroxy anisole, dibutyl hydroxy toluene or TBHQ.
10. the method for preparing quartz as claimed in claim 6, it is characterised in that:Described adhesive is one or more in polyurethane, polystyrene or polyacrylate.
CN201510858468.9A 2015-11-30 2015-11-30 A kind of quartz and preparation method thereof Pending CN106810114A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201510858468.9A CN106810114A (en) 2015-11-30 2015-11-30 A kind of quartz and preparation method thereof

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201510858468.9A CN106810114A (en) 2015-11-30 2015-11-30 A kind of quartz and preparation method thereof

Publications (1)

Publication Number Publication Date
CN106810114A true CN106810114A (en) 2017-06-09

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CN201510858468.9A Pending CN106810114A (en) 2015-11-30 2015-11-30 A kind of quartz and preparation method thereof

Country Status (1)

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Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101456207A (en) * 2009-01-06 2009-06-17 冯文英 Production technique of plate material of quartz, river and sea sand
CN104496272A (en) * 2014-12-15 2015-04-08 田忠和 Anti-aging artificial quartzite plate and manufacturing method thereof
CN104496273A (en) * 2014-12-15 2015-04-08 田忠和 Artificial quartzite plate and manufacturing method thereof
CN104529244A (en) * 2014-12-15 2015-04-22 田忠和 Anti-aging and antibacterial artificial quartzite board and manufacturing method thereof

Patent Citations (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101456207A (en) * 2009-01-06 2009-06-17 冯文英 Production technique of plate material of quartz, river and sea sand
CN104496272A (en) * 2014-12-15 2015-04-08 田忠和 Anti-aging artificial quartzite plate and manufacturing method thereof
CN104496273A (en) * 2014-12-15 2015-04-08 田忠和 Artificial quartzite plate and manufacturing method thereof
CN104529244A (en) * 2014-12-15 2015-04-22 田忠和 Anti-aging and antibacterial artificial quartzite board and manufacturing method thereof

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Application publication date: 20170609

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