CN106769759B - A kind of infiltrative device of test steel reinforced concrete protective layer and accelerated test method - Google Patents

A kind of infiltrative device of test steel reinforced concrete protective layer and accelerated test method Download PDF

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CN106769759B
CN106769759B CN201611126087.2A CN201611126087A CN106769759B CN 106769759 B CN106769759 B CN 106769759B CN 201611126087 A CN201611126087 A CN 201611126087A CN 106769759 B CN106769759 B CN 106769759B
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hermetically sealed
sample
flange
test
protective layer
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CN106769759A (en
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党玉栋
李昕成
李凯东
许国伟
赵勇
余明坤
赵宝生
郭清春
李东林
马晓杰
周学礼
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YUNNAN INSTITUTE OF BUILDING RESEARCH
Yunnan Construction and Investment Holding Group Co Ltd
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YUNNAN INSTITUTE OF BUILDING RESEARCH
Yunnan Construction and Investment Holding Group Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N1/00Sampling; Preparing specimens for investigation
    • G01N1/28Preparing specimens for investigation including physical details of (bio-)chemical methods covered elsewhere, e.g. G01N33/50, C12Q
    • G01N1/30Staining; Impregnating ; Fixation; Dehydration; Multistep processes for preparing samples of tissue, cell or nucleic acid material and the like for analysis
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/0806Details, e.g. sample holders, mounting samples for testing
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Immunology (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Physics & Mathematics (AREA)
  • Pathology (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Biomedical Technology (AREA)
  • Molecular Biology (AREA)
  • Testing Resistance To Weather, Investigating Materials By Mechanical Methods (AREA)
  • Sampling And Sample Adjustment (AREA)

Abstract

A kind of infiltrative device of test steel reinforced concrete protective layer and accelerated test method, it is related to a kind of infiltrative device and method of test steel reinforced concrete protective layer.The device includes: hermetically sealed can (1), permeating medium distilled water (1-1), gas-liquid separation net (1-2), air gauge (1-3), relief valve (1-4), sealing ring (1-5), clamping flange (1-6), electronic balance (2), fixed rack (2-1) weigh hook (2-2), steel wire (2-3), oil bath heating device (3), conduction oil (3-1) and oil bath pan (3-2) composition.Apparatus of the present invention and operating procedure are simple, can carry out quantitative assessment to the permeability of small size steel reinforced concrete protective layer sample, test time-consuming few, the testing inspection field suitable for concrete permeability.

Description

A kind of infiltrative device of test steel reinforced concrete protective layer and accelerated test method
Technical field
The invention belongs to the infiltrative device of test steel reinforced concrete protective layer in concrete material field and its users Method is related to steel reinforced concrete protective layer quality test detection technique field.
Background technique
Exclude Durability of Concrete caused by raw material quality, the deterioration of concrete durability be usually all by table and In gradually develop.For armored concrete, in the case where there is carbonization or erosion carbon dioxide, concrete reinforcement The integrality and anti-permeability performance of protective layer are to determine the key point of Service Life of Reinforced Concrete Structures.Practical Service Environment Under, although there is no problem for concrete substrate durability itself, once steel reinforced concrete protective layer occurs because external environment corrodes Degrade, corrosion, cracking when, it is likely that will lead to inside concrete reinforcement corrosion acceleration, and then seriously affect concrete structure Durability and service life.Therefore, the permeability of steel reinforced concrete protective layer is tested and analyzes for studying concrete durability Play a significant role.For the steel reinforced concrete protective layer within the scope of 0~50mm of surface layer, it is limited to the reasons such as sample size, mesh Before there is no mature testing standard or method to evaluate its permeability.The test steel reinforced concrete protective layer permeability being currently known Method have: patent document CN 101929937 discloses a kind of method of testing permeability of concrete on surface of reinforced bar, principle It is that hydrogen is quantitatively discharged into concrete using positioned at rebar surface, test Hydrogen Vapor Pressure decline curve in certain time comes Reflect the gas permeability of concrete.Since steel reinforced concrete protective layers most of in Practical Project destruction is all due to aggressivity What ion permeated under the action of water, only reflect the gas permeability of steel reinforced concrete protective layer in this way, cannot Reflect the permeability of concrete water resistant and erosion carbon dioxide;Patent document CN 101532941 discloses a kind of detection concrete The device of near-surface permeability, principle are by testing concrete internal and external humidity change procedure in the long period, thus indirectly Reflect the permeability of concrete.But practical steel reinforced concrete protective layer is usually changed, institute by the variation of extraneous temperature and humidity environment In this way can only qualitative characterization certain small inside concrete humidity affected by environment variation, and exist and take a long time Limitation.
Summary of the invention
The purpose of the invention is to overcome, the device of above-mentioned existing test concrete permeability is complicated, precision is low, can not Quantitative test, time-consuming, and is difficult to evaluate the technical problems such as the permeability of steel reinforced concrete protective layer, and the present invention provides one kind Test the device and its application method of concrete permeability.
The purpose of the present invention is achieved through the following technical solution.
The infiltrative device of a kind of test steel reinforced concrete protective layer, comprising: hermetically sealed can, electronic balance, oil bath heating dress It sets;The sealing pot bottom fills permeating medium distilled water, middle part is equipped with gas-liquid separation net, side is equipped with duct and connects air gauge And relief valve;Hollow at the top of hermetically sealed can, top flange flange is equipped with the groove of different-diameter for placing sealing ring, seals Tank top edge is equipped with hole makes it be connected with clamping device for placing bolt;The electronic balance is placed on fixed rack The weighing hook in face, electronic balance is allowed to connect with hermetically sealed can with steel wire;The oil bath heating device is by conduction oil and oil bath pan (3-2) composition, the lower part of hermetically sealed can is in conduction oil.
Hermetically sealed can of the present invention uses stainless steel material, and hermetically sealed can lower part tank diameter is 50~200mm, is highly 100~200mm, wall thickness are 5mm or more;Sealing pot bottom fills permeating medium distilled water, upper position setting inside hermetically sealed can There is one layer of gas-liquid separation net, separation net mesh size is 0.15~2.36mm;Hermetically sealed can top flange flange is provided with difference The groove of diameter can place the sealing ring of different-diameter, and it is close the concrete sample to be tested of different-diameter can be clamped flange It seals and is connected.
Clamping flange of the present invention is hollow disk, it is characterised in that stainless steel material is used, with a thickness of 5~ 10mm, clamping flange lower part are provided with the groove with hermetically sealed can top flange flange same shape and size;Clamp flange Edge is provided with the hole of size and number identical as hermetically sealed can top flange flange, makes it by concrete to be measured for placing bolt Sample sealing is fixed and closely coupled with hermetically sealed can.
A kind of infiltrative accelerated test method of test steel reinforced concrete protective layer of the invention, comprising the following steps:
The first step, sampling and sample preparation: the core boring sampling from concrete component, 50~200mm of core diameter, then according to need Certain thickness concrete sample is cut from core sample, thickness is desirable according to concrete strength and maximum size of coarse aggregate 10mm~50mm, sample upper and lower surface are parallel and smooth;The sample is put into saturated limewater and is impregnated no less than for 24 hours;Then, The specimen surface moisture finished will be impregnated to dry, then sealed sample side with sealant, stood to the sealing of sample side Glue is fully cured;
Second step, fixed sample to be tested: injected slurry volume is 1/4~1/2 infiltration for sealing tank volume inside to hermetically sealed can Medium distilled water;Then 1 outer diameter is respectively placed and sample to be tested is straight in hermetically sealed can top flange flange and clamping flange base Then hermetically sealed can, the ready sample to be tested of step 1 and clamping flange are tightly fastened by the equal sealing ring of diameter with bolt;
Electronic balance is stably placed at fixed rack by third step) on, then step 2 is installed and attached to together Hermetically sealed can, concrete sample to be measured and clamping flange three parts wire hanger are on the weighing hook of electronic balance;
4th step, oil bath heating device electrified regulation, makes thermally conductive oil temperature increase to the temperature of setting from room temperature;
The assembled device of step 3 is stably placed on oil bath heating device by the 5th step, and adjust steel wire length with Guarantee that 1/2 height of hermetically sealed can lower part is in inside conduction oil, but the bottom of hermetically sealed can and oil bath pot bottom at least 20mm distance;
6th step closes relief valve, opens balance and start recording data, reaches step 2 to whole device mass loss In initially to the 1/3 of the permeating medium distillation water quality injected inside hermetically sealed can when, off-test;Take device mass loss and when Half interval contour loss of improving quality increases rapidly and at the uniform velocity characterizes the permeability of sample in the slope of curve of near linear section, takes 3 The arithmetic average of sample is the permeability of the sample, unit kg/m2·h。
7th step after the test removes hermetically sealed can, disassembles after its temperature is cooled to room temperature;It repeats the above steps It can carry out the infiltrative test of next sample.
The invention has the advantages that being suitable for the infiltrative testing inspection field of steel reinforced concrete protective layer;Its principle It is to allow permeating medium distilled water to generate steam under sealing and hot conditions and penetrate concrete sample, passes through and monitor certain time The mass loss rate of the interior distilled water lost through concrete sample, and then quantitatively determine the infiltration of concrete sample Property;No pollution to the environment is used in the present invention and has the distilled water of preferable wellability as permeating medium with concrete, and sharp Concrete is passed it through with the pressure that vapor itself generates, therefore apparatus of the present invention are simple and environmentally-friendly, and tested time-consuming few;This Invention automatically records data using electronic balance, can effectively improve test efficiency, reduce test process manpower consumption and Human error.
Detailed description of the invention
Fig. 1 apparatus of the present invention schematic diagram;
The schematic diagram main view of Fig. 2-1 hermetically sealed can of the present invention (2);
The schematic diagram side view of Fig. 2-2 hermetically sealed can of the present invention (2);
The schematic diagram top view of Fig. 2-3 hermetically sealed can of the present invention (2);
Fig. 3-1 present invention clamping flange (1-6) and sealing ring (1-5) schematic diagram main view;
Fig. 3-2 present invention clamping flange (1-6) and sealing ring (1-5) schematic diagram side view;
Fig. 3-3 present invention clamping flange (1-6) and sealing ring (1-5) schematic diagram top view;
Fig. 3-4 present invention clamping flange (1-6) and sealing ring (1-5) schematic bottom view;
Fig. 4 verification test result figure of the present invention.
Specific embodiment
Referring to Fig.1, the infiltrative device preferred embodiment of test steel reinforced concrete protective layer of the present invention, it by Wall thickness is 5mm, total height is 200mm stainless steel hermetically sealed can 1, the electronic balance 2 that range is 5kg and precision is 0.1g, and most The oil bath heating device 3 that high-temperature can be heated to 200 DEG C is constituted.Wherein: it is 0.18mm's that mesh size is equipped in the middle part of hermetically sealed can 1 Copper gas-liquid separation net 1-2, side are equipped with the duct that diameter is 5mm, and for connecting, range is 20bar and precision is 0.2bar's Air gauge 1-3 and relief valve 1-4;1 top flange flange of hermetically sealed can is equipped with the groove that outer diameter is 50mm, placed 1 outer diameter The rubber seal 1-5 for being 3mm for 50mm, diameter of section, it is 5mm that 1 top flange flange plate edge of hermetically sealed can, which is equipped with 6 diameters, Circular hole, can place bolt make its with a thickness of 5mm stainless steel clamping flange 1-6 be connected;Electronic balance 2 is placed on solid Determine above rack 2-1, the weighing hook 2-2 of electronic balance 2 is allowed to connect with hermetically sealed can 1 with steel wire 2-3;Oil bath heating device 3 It is made of conduction oil 3-1 and oil bath pan 3-2, the lower part 80mm of hermetically sealed can 1 is in 130 DEG C of conduction oil 3-1.
Inventor has carried out field tests to concrete using this test device.Preferred implementation steps are as follows:
The first step, sample preparation.The cube concrete test specimen that test sample is 28 day age, side length is 200mm.The test block at It puts and conserves in dry environments to 28 day age after type 1 day.It is first in order to obtain the test sample that permeance property has significant difference First from the concrete formation Middle face drill core, core diameter 50mm, then from the forming surface of core sample 2mm and 100mm down The thin slice of 15mm thickness is cut respectively as final sample to be tested.After 2 preparation of samples are good, steeped in saturated limewater It 24 hours, then takes out and is dried the moisture on its surface with blotting paper, and sealed its side with silicone sealant, be placed on dry 6 hours in dry air, the silicone sealant of concrete sample side is fully hardened at this time;
Second step, fixed sample to be tested.40g distilled water 1-1 is injected inside to hermetically sealed can 1;Then in 1 top method of hermetically sealed can The rubber seal 1-5 that 1 outer diameter is 50mm is respectively placed in blue flange and the clamping bottom flange 1-6, then will be close with 6 bolts The ready sample to be tested of sealed cans 1, step 1 and clamping flange 1-6 are tightly fastened;
Electronic balance 2 is stably placed on fixed rack 2-1, step 2 is then installed and attached to one by third step Hermetically sealed can 1, concrete sample to be measured and the clamping flange 1-6 three parts risen are hung with the weighing that steel wire 2-3 is suspended on electronic balance 2 On hook 2-2;
4th step, 3 electrified regulation of oil bath heating device, makes conduction oil 3-1 temperature increase to 130 degrees Celsius from room temperature;
The assembled device of step 3 is stably placed on oil bath heating device 3, and adjusts steel wire 2-3 long by the 5th step Degree is to guarantee that 1 lower part of hermetically sealed can, 1/2 height is in inside conduction oil 3-1, and the bottom of hermetically sealed can 1 has with the bottom oil bath pan 3-2 The distance of 25mm;
6th step closes relief valve 1-4, opens balance and start recording data, and test period is under the experiment condition The relation curve of 2 samples corresponding device mass loss and time as shown in Figure 4 can be obtained in 18h, takes surface layer and inside mixed The slope for last 8 data points for increasing suddenly and at the uniform velocity changing on the solidifying corresponding mass loss curve of earth sample is respectively 8.72g/h and 3.46g/h is 0.001520m according to the practical vapor permeation area that the sample deducts sealing circuit covering2, therefore surface layer Infiltration rate corresponding with inner concrete sample is respectively 5.74kg/ (m2And 2.28kg/ (m h)2·h)。
7th step after the test removes hermetically sealed can 1 and its device being attached thereto, and is cooled to room temperature to its temperature After disassemble;The infiltrative test of next sample can be carried out by repeating the above steps.
Apparatus of the present invention and method have the following effects: device and method are simple and environmentally-friendly, it is time-consuming less, can quantitative test etc. it is excellent Point.

Claims (4)

1. a kind of infiltrative device of test steel reinforced concrete protective layer characterized by comprising hermetically sealed can (1), electronic balance (2), oil bath heating device (3);Hermetically sealed can (1) bottom fills permeating medium distilled water (1-1), middle part is isolated equipped with gas-liquid Net (1-2), side are equipped with duct connection air gauge (1-3) and relief valve (1-4);Hollow at the top of hermetically sealed can (1), top flange is convex Edge disk is equipped with the groove of different-diameter for placing sealing ring (1-5), and hermetically sealed can (1) top flange flange plate edge is equipped with hole Hole makes it be connected with clamping flange (1-6) for placing bolt;The electronic balance (2) is placed on fixed rack (2-1) above, The weighing hook (2-2) of electronic balance (2) is allowed to connect with hermetically sealed can (1) with steel wire (2-3);The oil bath heating device (3) It is made of conduction oil (3-1) and oil bath pan (3-2), the lower part of hermetically sealed can (1) is in conduction oil (3-1);Sample to be tested is put Enter and is impregnated in saturated limewater no less than for 24 hours.
2. a kind of infiltrative device of test steel reinforced concrete protective layer according to claim 1, which is characterized in that sealing Tank (1) uses stainless steel material, and it is highly 100~200mm, wall thickness is that hermetically sealed can (1) lower part tank diameter, which is 50~200mm, 5mm or more;Hermetically sealed can (1) bottom fills permeating medium distilled water (1-1), and the internal upper position of hermetically sealed can (1) is provided with one layer Gas-liquid separation net (1-2), separation net mesh size are 0.15~2.36mm;Hermetically sealed can (1) top flange flange is provided with not With the groove of diameter, the sealing ring (1-5) of different-diameter can be placed, and the concrete sample to be tested of different-diameter can be clamped Flange (1-6) seals and is connected.
3. a kind of infiltrative device of test steel reinforced concrete protective layer according to claim 1, which is characterized in that clamping Flange (1-6) is hollow disk, using stainless steel material, with a thickness of 5~10mm, clamp the lower part flange (1-6) be provided with The groove of hermetically sealed can (1) top flange flange same shape and size;Clamping edge flange (1-6) is provided with and hermetically sealed can (1) hole of the identical size and number of top flange flange makes it that concrete sample to be measured is sealed fixation for placing bolt And it is closely coupled with hermetically sealed can.
4. using a kind of accelerated test side for testing the infiltrative device of steel reinforced concrete protective layer according to claim 1 Method, which comprises the following steps:
The first step, sampling and sample preparation: the core boring sampling from concrete component, 50~200mm of core diameter, then as needed from Cut certain thickness concrete sample on core sample, thickness according to concrete strength and maximum size of coarse aggregate can use 10mm~ 50mm, sample upper and lower surface are parallel and smooth;Then, the specimen surface moisture finished will be impregnated to dry, it then will with sealant Sample side sealing, stands to the sealant of sample side and is fully cured;
Second step, fixed sample to be tested: being 1/4~1/2 infiltration of hermetically sealed can (1) volume to the internal injected slurry volume of hermetically sealed can (1) Saturating medium distilled water (1-1);Then it is respectively placed outside 1 in hermetically sealed can (1) top flange flange and clamping bottom flange (1-6) The diameter sealing ring equal with sample to be tested diameter (1-5), it is then with bolt that hermetically sealed can (1), step 1 is ready to test sample Product and clamping flange (1-6) are tightly fastened;
Electronic balance (2) is stably placed on fixed rack (2-1), step 2 is then installed and attached to one by third step Hermetically sealed can (1), concrete sample to be measured and clamping flange (1-6) three parts risen are suspended on electronic balance (2) with steel wire (2-3) Weighing hook (2-2) on;
4th step, oil bath heating device (3) electrified regulation, makes conduction oil (3-1) temperature increase to the temperature of setting from room temperature;
The assembled device of step 3 is stably placed on oil bath heating device (3) by the 5th step, and it is long to adjust steel wire (2-3) Degree is to guarantee that 1/2 height of hermetically sealed can (1) lower part is in conduction oil (3-1) inside, but the bottom of hermetically sealed can (1) and oil bath pan (3- 2) bottom at least 20mm distance;
6th step is closed relief valve (1-4), is opened balance and start recording data, is reached step to whole device mass loss In two initially to the 1/3 of the permeating medium distillation water quality injected inside hermetically sealed can (1) when, off-test;Device quality is taken to damage Lose the infiltration for improving quality with time graph and losing and increasing rapidly and at the uniform velocity characterize sample in the slope of curve of near linear section Property, take the arithmetic average of 3 samples for the permeability of the sample, unit is kg/ (m2·h);
7th step after the test removes hermetically sealed can (1), disassembles after its temperature is cooled to room temperature;It repeats the above steps i.e. It can carry out the infiltrative test of next sample.
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CN107589050A (en) * 2017-08-15 2018-01-16 哈尔滨工业大学 A kind of monitoring system and method for the Concrete Material of monitoring in real time infiltration water suction coupling coefficient
CN108918376B (en) * 2018-05-17 2021-01-05 云南省建筑科学研究院 Device and test method for detecting concrete surface permeability and maintenance effect
CN113466109B (en) * 2021-08-11 2022-05-27 龙游县万基建设工程检测有限公司 Device and method for detecting impermeability of concrete for building

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CN101482470B (en) * 2009-02-13 2010-12-08 西北农林科技大学 Test method for anti-permeability performance of fluid sealant and substrate bonding sample interface
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CN103776749B (en) * 2014-02-21 2016-11-02 哈尔滨工业大学 Asphalt mastic vapor permeation experimental technique under a kind of evaluation pressurized conditions
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CN205786227U (en) * 2016-05-24 2016-12-07 湖南建研信息技术股份有限公司 A kind of concrete impermeability test sensing device

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