CN106769633A - A kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked - Google Patents

A kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked Download PDF

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Publication number
CN106769633A
CN106769633A CN201710046215.0A CN201710046215A CN106769633A CN 106769633 A CN106769633 A CN 106769633A CN 201710046215 A CN201710046215 A CN 201710046215A CN 106769633 A CN106769633 A CN 106769633A
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yarn
sample
yarn group
high frequency
testing
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CN106769633B (en
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韩林
魏亚杰
万维维
王特
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JUSHI GROUP JIUJIANG CO Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N5/00Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid
    • G01N5/04Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder
    • G01N5/045Analysing materials by weighing, e.g. weighing small particles separated from a gas or liquid by removing a component, e.g. by evaporation, and weighing the remainder for determining moisture content

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  • General Health & Medical Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Chemical & Material Sciences (AREA)
  • Analytical Chemistry (AREA)
  • Biochemistry (AREA)
  • Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Treatment Of Fiber Materials (AREA)
  • Pathology (AREA)
  • Immunology (AREA)
  • Drying Of Solid Materials (AREA)
  • Reinforced Plastic Materials (AREA)
  • Investigating Strength Of Materials By Application Of Mechanical Stress (AREA)

Abstract

A kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked, the method for testing is carried out in the environment of 20 26 DEG C of temperature, humidity 55 75%, and method of testing is comprised the following steps:(1)Choose yarn group to be sampled;(2)Yarn group outer ring yarn removal to be sampled;(3)It is determined that digging sampling point position;(4)Take test sample;(5)Carry out water cut test;(6)Data analysis.Outfit of the present invention and equipment have cutting wire knife, stainless rule, signature pen, hermetic bag, electronic balance(It is accurate to 0.1mg), baking oven, planchet, drier, the method can in time measure the moisture content inside high frequency baking yarn group, quality problems caused by being prevented effectively from because baking not exclusively, contribute to promoting the use of for high frequency baking oven, the advantages of high frequency bakes that the product filoplume amount that has of technique is few, to bake speed fast can be given full play to, product quality and yield is effectively improved.

Description

A kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked
Technical field
A kind of method of testing of the glass fiber yarn ball internal moisture baked the present invention relates to high frequency.
Background technology
The market demand of glass fiber direct roving is growing, and client is required also increasingly product quality Height, bakes whether technique well has vital effect to glass fiber product quality.High frequency baking oven by its baking speed it is fast, The advantages of product produces filoplume amount few, is increasingly becoming the baking equipment of some high-end glass fiber products.But high frequency is also because of its own The characteristics of in the presence of certain baking blind spot, easily there is the internal phenomenon do not dried completely of yarn group.Surpass to avoid the occurrence of moisture content Target quality problems, it is necessary to which the glass fibre yarn group inner aqueous rate baked to high frequency baking oven is measured.
" the enhanced article test method part 1s of GB/T 9914.1:Content disclosed in the measure of moisture content " is current The water cut test method general for conventional glass fibers roving, the method summary that the standard is related to is as follows:From yarn group Oven for drying is put on surface into after taking the yarn of certain length, yarn is weighed, and is re-weighed after taking-up, calculates moisture content.From taking Quadrat method understand the standard can only in test yarns group certain length yarn moisture content, i.e., the water-bearing survey of conventional yarn group, without The internal blind spot region water-bearing survey of yarn group under technique is baked suitable for high frequency.
The content of the invention
Its purpose of the invention is that the glass that a kind of high frequency provided to overcome the shortcomings of prior art to exist is baked Glass silvalin rolls into a ball the method for testing of internal moisture.
The technical scheme realized above-mentioned purpose and take, a kind of test of the glass fiber yarn ball internal moisture that high frequency is baked Method, described method of testing is carried out in the environment of 20-26 DEG C of temperature, humidity 55-75%, and method of testing includes following step Suddenly:(1)Choose yarn group to be sampled:In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, existed with signature pen The position end face that yarn group contacts with support creel plate makes marks, and be shaped as and the yarn of the mark roll into a ball the straight line that diameter is essentially coincided, and use Pyrocondensation bag installs yarn group to be removed from creel, delivers to doff area conditioning temperature;(2)Yarn group outer ring yarn removal to be sampled:To adjust Manage to the yarn group of room temperature and be positioned on creel, remove pyrocondensation bag, mark is carried out in the end face rolled into a ball apart from yarn at the 1cm of outer ring with signature pen Note, starts to remove outer ring yarn with winder, untill the 1cm marks of end face;(3)It is determined that digging sampling point position:From step (1)In the end face mark that does start, along yarn group end face, every 90 ° determine point position, then four point positions altogether, with end face each Draw the rectangle frame of 10cm*5cm on corresponding yarn group surface centered on point position, by four points position opsition dependents numberings be 1#, 2#, 3#, 4#, and indicated on the label of counter sample hermetic bag, in case obscuring;(4)Take test sample:With cutting wire knife along 1# The inner edge of point bit length square box is exerted oneself to draw, it is ensured that each edge is all drawn to depth 1cm, has thus been obtained volume profiles and has been The glass filoselle of 10cm*5cm*1cm, rapidly digs out filoselle, is put into sealing in 1# hermetic bags;Dig out successively as stated above The sample of 2#, 3#, 4# rectangle frame, is put into correspondence hermetic bag, and sample is delivered into physical property sensing chamber moisture content to be measured rapidly;(5) Carry out water cut test:Four planchets are taken out from drier, with scales/electronic balance weighing, M is recorded as;Again from four hermetic bags Take out sample segment respectively to be sequentially placed into four planchets, record claims to obtain gross weight M1;Sample is put into together with planchet Temperature is set as in 105 DEG C of baking oven that dry more than one hour, taking-up is weighed and carries out being recorded as M2, then moisture content H=(M2- M)/(M1-M);(6)Data analysis:Contrast four moisture content of sample and index of dispatching from the factory, it is known that this test data is as good as Often, judge that the product bakes working well property.
Beneficial effect
The present invention has advantages below compared with prior art.
1st, the moisture content inside high frequency baking yarn group can be in time measured, quality is asked caused by being prevented effectively from because baking not exclusively Topic;
2nd, contribute to promoting the use of for high frequency baking oven, high frequency can be given full play to and baked that the product filoplume amount that has of technique is few, baked The advantages of speed is fast, effectively improves product quality and yield.
Specific embodiment
Testing tool and equipment have cutting wire knife, stainless rule, signature pen, hermetic bag, electronic balance needed for of the invention(Accurately To 0.1mg), baking oven, planchet, drier.
A kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked, described method of testing is in temperature 20- 26 DEG C, carry out in the environment of humidity 55-75%, method of testing is comprised the following steps:
(1)Choose yarn group to be sampled:
In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, rolled into a ball in yarn with signature pen and contacted with support creel plate Position end face make marks, the mark is shaped as and the yarn group straight line that essentially coincides of diameter, with pyrocondensation bag by yarn group install from Creel is removed, and delivers to doff area conditioning temperature;
(2)Yarn group outer ring yarn removal to be sampled:
It is positioned over nursing one's health to the yarn group of room temperature on creel, removes pyrocondensation bag, the end at the 1cm of outer ring is being rolled into a ball apart from yarn with signature pen Mark is carried out in face, starts to remove outer ring yarn with winder, untill the 1cm marks of end face;
(3)It is determined that digging sampling point position:
From step(1)In the end face mark that does start, along yarn group end face, every 90 ° determine point position, then four point positions altogether, The rectangle frame of 10cm*5cm is drawn on corresponding yarn group surface centered on each point position of end face, four point position opsition dependents are compiled Number be 1#, 2#, 3#, 4#, and on the label of counter sample hermetic bag indicate, in case obscuring;
(4)Take test sample:
Exerted oneself to draw along the inner edge of 1# point bit length square boxs with cutting wire knife, it is ensured that each edge is all drawn to depth 1cm, thus The glass filoselle that volume profiles are 10cm*5cm*1cm has been arrived, rapidly filoselle has been dug out, sealing in 1# hermetic bags has been put into;By above-mentioned Method digs out the sample of 2#, 3#, 4# rectangle frame successively, is put into correspondence hermetic bag, sample is delivered into physical property sensing chamber rapidly and is treated Survey moisture content;
(5)Carry out water cut test:
Four planchets are taken out from drier, with scales/electronic balance weighing, M is recorded as;Again from four hermetic bags taking-up portion respectively Sample is divided to be sequentially placed into four planchets, record claims to obtain gross weight M1;Sample is put into temperature together with planchet to be set as In 105 DEG C of baking oven, dry more than one hour, taking-up is weighed and carries out being recorded as M2, then moisture content H=(M2-M)/(M1-M);
(6)Data analysis:
Contrast four moisture content of sample and index of dispatching from the factory, it is known that this test data has without exception, judge that the product bakes effect Fruit formedness.
Embodiment 1
Test sample:Glass fiber direct roving;
Test condition:23 DEG C of temperature, humidity 60%.
Method of testing step is:
(1)Choose yarn group to be sampled:In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, existed with signature pen The position end face that yarn group contacts with support creel plate makes marks, and be shaped as and the yarn of the mark roll into a ball the straight line that diameter is essentially coincided, and use Pyrocondensation bag installs yarn group to be removed from creel, delivers to doff area conditioning temperature.
(2)Yarn group outer ring yarn removal to be sampled:It is positioned over nursing one's health to the yarn group of room temperature on creel, removes pyrocondensation bag, With signature pen mark is carried out in the end face rolled into a ball apart from yarn at the 1cm of outer ring.Start to remove outer ring yarn with winder, until end face Untill 1cm marks.
(3)It is determined that digging sampling point position:From step(1)In do end face mark start, along yarn group end face it is every 90 ° determine one Individual point position, then four point positions altogether, the rectangular of 10cm*5cm is drawn centered on each point position of end face on corresponding yarn group surface Four point position opsition dependent numberings are 1#, 2#, 3#, 4# by shape frame, and are indicated on the label of counter sample hermetic bag, in case mixed Confuse.
(4)Take test sample:Exerted oneself to draw along the inner edge of 1# point bit length square boxs with cutting wire knife, it is ensured that each edge is all drawn To depth 1cm, the glass filoselle that volume profiles are 10cm*5cm*1cm is thus obtained, rapidly dug out filoselle, be put into Sealed in 1# hermetic bags, dig out the sample of 2#, 3#, 4# rectangle frame successively as stated above, be put into correspondence hermetic bag.Rapidly will Sample delivers to physical property sensing chamber moisture content to be measured.
(5)Carry out water cut test:Four planchets are taken out from drier, is weighed with a ten thousandth balance, recorded;From Hermetic bag is taken out at least 5g samples and is sequentially placed into planchet respectively, claims to obtain gross weight, record;Sample is put together with planchet Enter temperature to be set as in 105 DEG C of baking oven, dry more than one hour, taking-up is weighed and recorded.Moisture content is calculated, specific data are shown in Table 1:
Table 1 digs sample water cut test data
(6)Data analysis:Moisture content and index of dispatching from the factory in contrast table 1, it is known that this test data is without exception, the product are baked Work well.
Embodiment 2
Test sample:Glass fiber direct roving;
Test condition:25 DEG C of temperature, humidity 60%.
Method of testing step is:
(1)Choose yarn group to be sampled:In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, existed with signature pen The position end face that yarn group contacts with support creel plate makes marks, and be shaped as and the yarn of the mark roll into a ball the straight line that diameter is essentially coincided, and use Pyrocondensation bag installs yarn group to be removed from creel, delivers to doff area conditioning temperature.
(2)Yarn group outer ring yarn removal to be sampled:It is positioned over nursing one's health to the yarn group of room temperature on creel, removes pyrocondensation bag, With signature pen mark is carried out in the end face rolled into a ball apart from yarn at the 1cm of outer ring.Start to remove outer ring yarn with winder, until end face Untill 1cm marks.
(3)It is determined that digging sampling point position:From step(1)In do end face mark start, along yarn group end face it is every 90 ° determine one Individual point position, then four point positions altogether, the rectangular of 10cm*5cm is drawn centered on each point position of end face on corresponding yarn group surface Four point position opsition dependent numberings are 1#, 2#, 3#, 4# by shape frame, and are indicated on the label of counter sample hermetic bag, in case mixed Confuse.
(4)Take test sample:Exerted oneself to draw along the inner edge of 1# point bit length square boxs with cutting wire knife, it is ensured that each edge is all drawn To depth 1cm, the glass filoselle that volume profiles are 10cm*5cm*1cm is thus obtained, rapidly dug out filoselle, be put into Sealed in 1# hermetic bags, dig out the sample of 2#, 3#, 4# rectangle frame successively as stated above, be put into correspondence hermetic bag.Rapidly will Sample delivers to physical property sensing chamber moisture content to be measured.
(5)Carry out water cut test:Four planchets are taken out from drier, is weighed with a ten thousandth balance, recorded;From Hermetic bag is taken out at least 5g samples and is sequentially placed into planchet respectively, claims to obtain gross weight, record;Sample is put together with planchet Enter temperature to be set as in 105 DEG C of baking oven, dry more than one hour, taking-up is weighed and recorded.Moisture content is calculated, specific data are shown in Table 2:
Table 2 digs sample water cut test data
(6)Data analysis:Moisture content and index of dispatching from the factory in contrast table 2, it is known that this test data is without exception, the product are baked Work well.
Embodiment 3
Test sample:Glass fiber direct roving;
Test condition:25 DEG C of temperature, humidity 70%.
Method of testing step is:
(1)Choose yarn group to be sampled:In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, existed with signature pen The position end face that yarn group contacts with support creel plate makes marks, and be shaped as and the yarn of the mark roll into a ball the straight line that diameter is essentially coincided, and use Pyrocondensation bag installs yarn group to be removed from creel, delivers to doff area conditioning temperature.
(2)Yarn group outer ring yarn removal to be sampled:It is positioned over nursing one's health to the yarn group of room temperature on creel, removes pyrocondensation bag, With signature pen mark is carried out in the end face rolled into a ball apart from yarn at the 1cm of outer ring.Start to remove outer ring yarn with winder, until end face Untill 1cm marks.
(3)It is determined that digging sampling point position:From step(1)In do end face mark start, along yarn group end face it is every 90 ° determine one Individual point position, then four point positions altogether, the rectangular of 10cm*5cm is drawn centered on each point position of end face on corresponding yarn group surface Four point position opsition dependent numberings are 1#, 2#, 3#, 4# by shape frame, and are indicated on the label of counter sample hermetic bag, in case mixed Confuse.
(4)Take test sample:Exerted oneself to draw along the inner edge of 1# point bit length square boxs with cutting wire knife, it is ensured that each edge is all drawn To depth 1cm, the glass filoselle that volume profiles are 10cm*5cm*1cm is thus obtained, rapidly dug out filoselle, be put into Sealed in 1# hermetic bags, dig out the sample of 2#, 3#, 4# rectangle frame successively as stated above, be put into correspondence hermetic bag.Rapidly will Sample delivers to physical property sensing chamber moisture content to be measured.
(5)Carry out water cut test:Four planchets are taken out from drier, is weighed with a ten thousandth balance, recorded;From Hermetic bag is taken out at least 5g samples and is sequentially placed into planchet respectively, claims to obtain gross weight, record;Sample is put together with planchet Enter temperature to be set as in 105 DEG C of baking oven, dry more than one hour, taking-up is weighed and recorded.Moisture content is calculated, specific data are shown in Table 3:
Table 3 digs sample water cut test data
(6)Data analysis:Moisture content and index of dispatching from the factory in contrast table 3, it is known that this test data is without exception, the product are baked Work well.

Claims (1)

1. a kind of method of testing of the glass fiber yarn ball internal moisture that high frequency is baked, it is characterised in that described method of testing Carried out in the environment of 20-26 DEG C of temperature, humidity 55-75%, method of testing is comprised the following steps:
(1)Choose yarn group to be sampled:
In the good glass fiber yarn ball of one outward appearance of high frequency baking oven egress selection, rolled into a ball in yarn with signature pen and contacted with support creel plate Position end face make marks, the mark is shaped as and the yarn group straight line that essentially coincides of diameter, with pyrocondensation bag by yarn group install from Creel is removed, and delivers to doff area conditioning temperature;
(2)Yarn group outer ring yarn removal to be sampled:
It is positioned over nursing one's health to the yarn group of room temperature on creel, removes pyrocondensation bag, the end at the 1cm of outer ring is being rolled into a ball apart from yarn with signature pen Mark is carried out in face, starts to remove outer ring yarn with winder, untill the 1cm marks of end face;
(3)It is determined that digging sampling point position:
From step(1)In the end face mark that does start, along yarn group end face, every 90 ° determine point position, then four point positions altogether, The rectangle frame of 10cm*5cm is drawn on corresponding yarn group surface centered on each point position of end face, four point position opsition dependents are compiled Number be 1#, 2#, 3#, 4#, and on the label of counter sample hermetic bag indicate, in case obscuring;
(4)Take test sample:
Exerted oneself to draw along the inner edge of 1# point bit length square boxs with cutting wire knife, it is ensured that each edge is all drawn to depth 1cm, thus The glass filoselle that volume profiles are 10cm*5cm*1cm has been arrived, rapidly filoselle has been dug out, sealing in 1# hermetic bags has been put into;By above-mentioned Method digs out the sample of 2#, 3#, 4# rectangle frame successively, is put into correspondence hermetic bag, sample is delivered into physical property sensing chamber rapidly and is treated Survey moisture content;
(5)Carry out water cut test:
Four planchets are taken out from drier, with scales/electronic balance weighing, M is recorded as;Again from four hermetic bags taking-up portion respectively Sample is divided to be sequentially placed into four planchets, record claims to obtain gross weight M1;Sample is put into temperature together with planchet to be set as In 105 DEG C of baking oven, dry more than one hour, taking-up is weighed and carries out being recorded as M2, then moisture content H=(M2-M)/(M1-M);
(6)Data analysis:
Contrast four moisture content of sample and index of dispatching from the factory, it is known that this test data has without exception, judge that the product bakes effect Fruit formedness.
CN201710046215.0A 2017-01-22 2017-01-22 Method for testing moisture in high-frequency baked glass fiber yarn cluster Active CN106769633B (en)

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Cited By (1)

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CN110274844A (en) * 2018-03-15 2019-09-24 中冶长天国际工程有限责任公司 The diagnostic method and device of drying process in sintering fuel granularmetric composition detection system

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CN102235958A (en) * 2010-04-26 2011-11-09 张保林 Simple detection of water-containing fiber (or fiber bundle)
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CN102235958A (en) * 2010-04-26 2011-11-09 张保林 Simple detection of water-containing fiber (or fiber bundle)
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CN110274844A (en) * 2018-03-15 2019-09-24 中冶长天国际工程有限责任公司 The diagnostic method and device of drying process in sintering fuel granularmetric composition detection system
CN110274844B (en) * 2018-03-15 2021-12-24 中冶长天国际工程有限责任公司 Method and device for diagnosing drying process in sintered fuel grain composition detection system

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